Photoluminescence Properties of Nanocrystalline 3C-SiC Films

Nanocrystalline (nc) 3C-SiC films on the Si substrate were prepared by the helicon wave plasma enhanced chemical vapor deposi-tion (HW-PECVD) technique. With the SiH4-CH4 gas flow ratio changing, the films exhibit different photoluminescence (PL) character-istics. Under the stoichiometric condition, the PL peak redshift from 470 nm to 515 nm is detected with the increase of excitation wave-length, which can be attributed to the quantum confinement effect radiation of 3C-SiC nanocrystals of different sizes. However, the ap-pearance of an additional PL band at 436 nm in Si-rich film might be sourced back to the excess of Si defect centers in it. This is also the case for C-rich film for its PL band lying at 570 nm. The results above quoted indicate an important influence of gas flow ratio on the PL properties of the SiC films providing an effective guidance for analyzing the luminescence mechanism and exploring the high-efficiency light emission of the SiC films.     

渗透检测中渗透深度与其它参数动态关系的理论研究

本文以圆孔状缺陷作为计算模型，推导了渗透检验过程中渗透深度与其它参数之间的动态关系，并对结果进行了分析和讨论。     

低应变基桩缺陷量化分析软件系统

目前,在基桩缺陷低应变分析方面,对基桩缺陷仅能给出定性评价,没有量化指标。主要研究的是在均匀土质中,在基桩单一缺陷量化分析模型及多缺陷量化分析模型的基础上应用计算机语言建立一个数据完整的低应变基桩单缺陷及多缺陷量化分析的软件系统,解决了基桩量化分析领域没有分析程序的难题。     

固体火箭发动机装药缺陷失效判定研究的发展和展望

阐述了近年来固体火箭发动机装药缺陷失效判定研究的一些进展,目前世界各国还未发现统一而完善的缺陷失效判定方法。根据最近相关领域新技术的出现与军事斗争的需要,展望了这一研究领域未来的发展趋势。     

某涡轮后机匣裂纹失效机理分析

为排除某航空发动机斜支板涡轮后机匣在试车后出现裂纹的故障,进行了裂纹宏观检查、断口宏观和微观形貌分析、材质检查、细晶层成因及其对疲劳特性影响分析,并对裂纹性质进行了判定,分析了产生裂纹故障的原因。结果表明:斜支板涡轮后机匣裂纹为疲劳性质,原始铸造冷隔缺陷、热等静压工艺产生的细小再结晶层、基体晶粒粗大是促使涡轮后机匣过早疲劳开裂的主要原因。为避免该类故障再次发生,建议提高浇注温度以增强浇注液流动性,从而排除冷隔缺陷;防止热等静压时产生表面细小再结晶;添加细化剂使基体晶粒细化。     

某型发动机三齿Ⅱ级涡轮叶片断裂故障浅析

某型发动机Ⅱ级涡轮叶断裂故障，是长期困扰该型发动机承制厂的重大技术质量问题。通过对故障的研究，提出了解决断裂故障的改进措施。     

某端燃固体火箭发动机脱粘面临界尺寸的研究

建立了含脱粘面的某固体火箭发动机工作过程的数学模型，根据脱粘面不扩展条件下得到的发动机工作过程中压力变化仿真曲线，进行了装药应力应变场的三维粘弹性有限元计算，并采用J积分断裂判据，预估了在发动机工作过程中脱粘面可能发生扩展时的临界尺寸。     

固体火箭发动机喷管粘接界面的超声检测

介绍了超声纵波多次反射法在固体火箭发动机喷管金属与非金属复合构件粘接界面无损检测中的应用原理，设计制做了对比试块用来考查方法的探伤灵敏度，并对实际样品进行了检测，证明该方法适用于现场检测和阵地探伤。     

基于微结构识别的单向复合材料导热系数预估

以T300碳纤维/环氧树脂基单向复合材料为例,考虑纤维周围间隙缺陷的影响,建立了基于微观图像识别的等效导热系数预估方法.首先利用图像识别技术处理材料微观电镜照片,然后依据纤维体积分数稳定性判据应用几何重构技术建立了代表性单元,并通过在代表性单元（RVE）内部交界面处添加接触热阻的方法引入间隙缺陷的影响,最终利用有限元方法模拟得到等效导热系数（ETC）.研究发现:间隙的位置对等效导热系数影响微弱;随着间隙缺陷占比和厚度的增加,等效导热系数显著降低;间隙缺陷占比大于0.8,无量纲间隙缺陷厚度小于0.15时,单向纤维增韧复合材料的等效导热系数受间隙影响最突出;相对于纤维和基体理想接触的情况,考虑间隙缺陷后,等效导热系数最大降幅可达52.1%.      

Characteristics of Disorder and Defect in Hydrogenated Amorphous Silicon Nitride Thin Films Containing Silicon Nanograins

The hydrogenated amorphous silicon nitride （SiNx） thin films embedded with nano-structural silicon were prepared and the micro- structures at the interface of silicon nano-grains/SiNx were identified by the optical absorption and Raman scattering measurements. Characterized by the exponential tail of optical absorption and the band-width of the Raman scattering TO mode, the disorder in the interface region increases with the gas flow ratio increasing. Besides, as reflected by the sub-gap absorption coefficients, the density of interface defect states decreases, which can be attributed to the structural mismatch in the interface region and also the changes of hydrogen content in the deposited films. Additional annealing treatment results in a significant increase of defects and degree of disorder, for which the hydrogen out-diffusion in the annealing process would be responsible.