空间微小碎片累积作用下材料光学性能退化预示模型适用性研究

航天器在轨服役期间会遭受到大量空间微小碎片和微流星体的撞击作用,其中的微米级粒子将在航天器表面产生大面积砂蚀现象,并使材料或器件功能衰退。文章介绍了NASA空间微小碎片累积损伤材料光学性能退化预示模型并推导了两个预示模型之间的关系。利用ORDEM2000碎片分布模型估算了K8玻璃累积损伤面积。以K8玻璃为例,对比研究了两个预示模型的适用性。结果表明,当航天器外表面损伤程度小于40%,可利用Canoon模型评价和预示材料光学性能退化规律;当航天器外表面损伤程度大于40%,需利用Mirtich模型评价和预示材料光学性能退化规律。     

接触角法测玄武岩及玻璃纤维表面能实验

通过Wilhelmy吊片法测试液体与玄武岩、玻璃纤维单丝的前进接触角,应用OWRK理论计算得到纤维表面能及其色散与极性分量.实验研究表明:未经表面处理的玄武岩纤维表面能高于S-2玻璃纤维,去除浸润剂后2种纤维表面能的极性分量均明显降低,并且测试液体的极性分量对纤维表面能的测试结果影响甚大.分析结果为纤维与树脂的表面张力合理匹配、形成良好界面浸润和粘接提供了理论依据.      

基于玻璃-硅复合基板的微系统圆片级三维封装

随着微系统追求更小的尺寸、更高的集成度，圆片级三维封装技术已成为未来微系统封装的发展趋势。基于玻璃回流工艺，提出了一种新型圆片级三维封装技术。设计了用于实现单模光纤阵列与玻璃基板上平面光波导之间耦合封装的U型槽阵列，采用高导硅作为垂直电引出，制备了玻璃-硅复合基板，并用玻璃帽实现了封装。玻璃-硅复合基板技术在三维微系统和光电子封装领域中具有重要的应用前景。     

A wall-thickness compensation strategy for wax pattern of hollow turbine blade

As an important index affecting the aerodynamic performance and the structural strength of hollow turbine blades, the wall-thickness precision of the blade is mainly inherited from the positional relationship between the corresponding wax pattern and the internal ceramic core. However, due to locating errors, the actual position of ceramic core is always deviated from the ideal position, which makes it difficult to guarantee the wall-thickness precision of the wax pattern. To solve this problem, a wall-thickness compensation strategy is proposed in this paper. Firstly, based on the industrial computed tomography (ICT) technique and curve matching algorithms, a model reconstruction method is developed, with which the 3D model of a trial wax pattern can be easily constructed. After that, focusing on eliminating the wall-thickness errors of the trial wax pattern, an optimization method for the pose of the ceramic core in the wax pattern is proposed. Then, by mapping the optimal pose of the ceramic core to length adjustments of the locating rods, the wall-thickness errors of the wax pattern can be greatly reduced. A case study is also given to illustrate the effectiveness of the proposed compensation strategy.     

SiCO陶瓷隔热复合材料TaSi2-MoSi2硼硅酸盐玻璃涂层制备与性能

为了提高SiCO陶瓷隔热复合材料的抗氧化抗热震性能,通过刷涂法制备SiCO陶瓷隔热复合材料TaSi_2-MoSi_2硼硅酸盐玻璃涂层,借助扫描电镜、X射线衍射等手段对硼硅酸盐玻璃含量分别占23%、31%、38%、41%的涂层进行微观形貌和相组成分析,对不同含量的涂层进行1 500℃氧化5 min,取出后冷却至室温的重复循环试验。结果表明:在循环次数达到25次,氧化总时间达到125 min后,硼硅酸盐玻璃含量占38%的TaSi_2-MoSi_2硼硅酸盐玻璃涂层表面具有最少的孔洞和裂纹,涂层的失重率为-2.1%,说明该涂层具有最好的抗氧化和抗热震性能。。     

Silver Film Growth on Glass Ceramic by Radio Frequency Magnetron Sputtering

Thin silver films are deposited by radio frequency magnetron sputtering on glass ceramic at room temperature.Variations of sputtering power,bios voltage and power density are carried out for each deposition,then parts of as-deposited samples are subjected to annealing at 600 ℃ within a vacuum chamber.Structural properties are studied by X-ray diffraction(XRD),scanning electron microscope(SEM)and laser scanning confocal microscope(LSCM).It is shown that structural properties have a strong dependency on sputtering power and annealing temperature.Electrical contact resistance measured by a four point probe instrument is directly affected by the thickness of films.It is also found that the film conductivity,especially in thinner films,is improved by the increasing grain size.Finally,the film adhesion is observed by scratch tests.And the adhesive ability deposited by radio frequency magnetron sputtering shows a better performance than that produced by traditional methods.     

玻璃基环形振动微陀螺谐振子的设计与制造工艺

针对传统单晶硅材料热胀系数不稳定引起的硅基环形振动微陀螺的温度漂移问题，开展了玻璃基环形振动微陀螺谐振子的设计，并提出了一种新型的玻璃基准三维微结构制造工艺，借助微型电子机械系统（MEMS）工艺中成熟的深硅刻蚀、阳极键合、化学机械抛光等通用加工技术，融合玻璃熔融工艺，解决了玻璃基准三维微结构的制造工艺难题，同时保证了高的加工精度，实现了玻璃基环形振动微陀螺谐振子的高精度批量制造。     

耐候钢活性MAG 焊接接头组织及冲击断口特征

针对焊枪可达性差等难熔合焊接结构,提出了活性熔化极气体保护焊焊接新方法。该方法可增加焊接熔深,改善难熔焊接结构的熔合不良,获得高质量的焊接接头。采用活性熔化极气体保护焊接对耐候钢进行了工艺试验,对焊接接头组织、冲击韧性及断口形貌进行分析。结果表明,相对熔化极气体保护焊,活性熔化极气体保护焊在同等焊接热输入下熔深显著增加,焊缝表面及焊接接头内部质量高,接头组织更为细化,过热区析出碳化物相也更加细小弥散,冲击韧性提高,冲击断口韧性特征更明显。     

空心石英纤维增强聚芳基乙炔树脂基透波复合材料的制备及其性能

以空心石英纤维(HSF)和聚芳基乙炔(PAA)树脂为原料采用RTM工艺制备了空心石英纤维增强聚芳基乙炔树脂基复合材料(HSF/PAA),比较了HSF/PAA与实心石英纤维增强聚芳基乙炔树脂基复合材料(SF/PAA)的力学性能、介电性能及不同纤维增强体形式对材料力学性能的影响。结果表明,HSF/PAA具有较好的高温力学性能和优异的介电性能,使用温度可达450℃,而且通过对纤维增强体形式的优化有望进一步提高该类材料的综合性能。尽管HSF/PAA的高温力学性能仅有同结构SF/PAA的55%~75%,但其在较宽的温度和频率范围内均具有更低的介电常数(3.1)和介质损耗角正切值(0.004),在实际应用中可以获得更高的传输系数和更宽的壁厚容差,有望在耐高温透波材料在航空航天等诸多领域获得应用。     

添加微量铜对FeCoNbSiB合金非晶形成能力及磁性的影响

采用工业用硼铁为主要原料制备一种FeCoNbSiBCu大块非晶合金.采用差示扫描量热分析、X射线衍射分析、扫描电镜及能谱分析对合金的非晶形成能力进行研究.结果表明,通过添加微量Cu可以显著提高FeCoNbSiB合金玻璃形成能力,当添加Cu的原子比含量为0.5at%～0.7at%时,合金的非晶形成能力明显提高.采用振动样品磁强计对铸态样品的软磁性能进行研究.结果表明,当Cu的加入量为0.5at%时,非晶合金的软磁性能得到提高.