Detail fatigue rating method based on bimodal Weibull distribution for DED Ti-6.5Al-2Zr-1Mo-1V titanium alloy

Previous studies have shown that the fatigue life distribution of metal materials fabricated with Additive Manufacturing(AM) methods, such as Direct Energy Deposited(DED) Ti-6.5Al-2Zr-1Mo-1V alloys, exhibits two peaks. To promote the application of AM in aerospace and other engineering fields, developing a fatigue strength evaluation method suitable for AM materials based on their unique fatigue behaviours and fatigue life distributions is necessary. In this paper, a novel Detail Fatigue Rating(...     

Ti-6.5Al-3.5Mo-1.5Zr-0.3Si合金绝热剪切和局部流动行为

在THERMECMASTOR-Z型热模拟机上对Ti-6.5Al-3.5Mo-1.5Zr-0.3Si合金在变形温度780～1 080 ℃,应变速率0.001～70.000 s^-1条件下的流动应力变化规律进行了研究,分析了变形工艺参数对Ti-6.5Al-3.5Mo-1.5Zr-0.3Si合金绝热剪切和局部流动行为的影响,并采用基于动态材料模型的功率耗散图分析了Ti-6.5Al-3.5Mo-1.5Zr-0.3Si合金易发生绝热剪切和局部流动的热力参数范围。结果表明:在所研究的热变形条件下,当温度较高、应变速率较低时,变形呈稳态流动特征,当温度较低、应变速率较高时,变形呈流动软化特征。通过功率耗散图分析及微观组织观察可知,在α+β两相区变形,应变速率高于0.100 s^-1时,功率耗散系数多数小于0.16,变形多处于流变失稳区域,其变形机制主要为绝热剪切和局部流动。     

扩散连接界面缺陷对Ti-6Al-4V合金力学性能的影响

研究了φ4mm与φ2mm的扩散连接界面缺陷对Ti-6Al-4V合金力学性能的影响。当拉伸载荷方向与缺陷平面平行时,材料的强度与塑性与无缺陷材料相当,这是由于此类缺陷对样品受力截面的面积几乎没有影响。含有φ4mm缺陷试样的拉压疲劳寿命展现出很大的分散性,界面缺陷并未成为裂纹萌生的唯一位置。从表面起裂的样品均处于高寿命区域,而绝大部分从缺陷处起裂的样品均落于低寿命区域。有限元分析表明,当缺陷位于中心位置时其引起的应力集中较小,应力分布梯度较小;缺陷位于边缘位置时,应力集中效应增大。     

Ti-6Al-2Zr-1M0-1V合金的热变形行为

在Gleeble-1500热模拟机上对Ti-6A1-2Zr-1Mo-1V钛合金铸态材料进行了恒温和恒应变速率下的热压缩变形实验，温度范围是700～1000℃，应变速率范围是5×10     

Electrochemical behavior of Ti-6.5Al-2Zr-1Mo-1V alloy under rotating condition with periodically fluctuating current density

Titanium alloy plays a crucial role in the electrochemical field due to its excellent corrosion resistance. The passivation and dissolution behaviors of Ti-6.5Al-2Zr-1Mo-1V（TA15） alloy in Na Cl solution were studied by simulating the electrochemical machining process in a rotating condition, which made the anode in a state with alternating high and low current density. Electron probe micro analysis, ultra-depth microscope, scanning electron microscope, and X-ray photoelectron spectrometer were u...     

湿喷丸处理Ti-6Al-4V合金微动磨损行为影响

采用湿喷丸技术对Ti-6Al-4V合金进行表面强化处理,研究了部分滑移、混合滑移和完全滑移等不同状态下钛合金样品的微动磨损行为,从微动状态角度探讨喷丸强化对钛合金微动磨损行为的影响规律。试验结果显示,喷丸处理对于完全滑移状态下Ti-6Al-4V合金的微动磨损行为影响较小;而在混合滑移状态时,喷丸处理使得微动磨痕的塑性变形积累区消失,有效抑制局部疲劳损伤造成的微裂纹萌生。这是因为喷丸引入加工硬化作用使材料表层局部强度提高,进而改善局部疲劳损伤。     

激光沉积Ti-6Al-2Zr-Mo-V钛合金高周疲劳性能

 疲劳失效是钛合金工业应用中最重要的失效方式,疲劳强度是钛合金应用的关键性指标。为了研究激光沉积Ti-6Al-2Zr-Mo-V钛合金的疲劳性能和行为,在625 MPa到900 MPa不同应力水平下进行了室温高周疲劳(HCF)测试(应力比R=0.1,加载频率f=120~130 Hz),完成了疲劳断口表面分析。研究了气孔存在及分布对激光沉积Ti-6Al-2Zr-Mo-V钛合金疲劳性能的影响。激光沉积钛合金具有细小α/β片层组织。分析结果显示,虽然疲劳源区有气孔存在,激光沉积Ti-6Al-2Zr-Mo-V钛合金仍然具有优异的疲劳性能。取向丰富细小的α/β片层组织能有效减小疲劳源区滑移长度。分析结果还表明,应力水平对疲劳行为有一定影响。     

Experimental study of effect of post processing on fracture toughness and fatigue crack growth performance of selective laser melting Ti-6Al-4V

For Ti-6Al-4V, a titanium alloy increasingly used in aerospace structure, selective laser melting (SLM) is an attractive additive manufacturing technology, which is attributed to its complex construction capability with high accuracy and good surface quality. In order to obtain qualified mechanical properties, SLM parameters and post processing should be tailored for diverse service conditions. Fracture toughness and fatigue crack growth (FCG) behavior are critical characteristics for damage tolerance evaluation of such metallic structures, and they are affected by post processing technologies significantly. The objective of this study is to obtain the fracture toughness and fatigue crack growth behavior of Ti-6Al-4V manufactured by SLM, and to evaluate the influence of post-SLM thermomechanical treatment and surface machining. Fracture toughness and FCG tests were performed for SLM Ti-6Al-4V in three types of post processing status: as-built, heat treated and hot isostatically pressed (HIPed), respectively. Specimens with as-built and machined surface were tested. The microstructure and fractography were analyzed as well in order to investigate the relevance among manufacture process, microstructure and mechanical properties. The results demonstrate that as-built SLM Ti-6Al-4V presents poor ductility and FCG behavior due to martensitic microstructure and residual stresses. Both heat treatment and hot isostatic pressing improve the plane-stress fracture toughness and FCG performance considerably, while surface machining shows slight effect.     

TC11钛合金焊接接头低周疲劳分形损伤演化研究

基于损伤力学和分形理论,在金属材料疲劳断口的形貌特征具有统计自相似性的基础上建立了表征焊接接头断口损伤的面分形损伤演化模型.利用TC11合金低周疲劳试验后所得到的断口测得其面分维数,结合试验数据拟合获得该材料损伤演化方程参数;从而建立了TC11合金焊接接头三级载荷下的疲劳损伤演化方程;同时将该模型与基于断口表面裂纹扩展的线分形损伤演化模型加以比较.      

铸造钛合金的氢处理细化晶粒的研究

本文研究了氢处理（渗氢+共析处理+真空除氢）对铸造Ti-6Al-4V合金微观组织的影响。发现Ti-6A1-4V合金渗氢后析出片状的面心立方结构的TiH₂相。随含氢量的增加,TiH₂相趋于球化。渗氢试样经共析处理后,原晶界α消失,组织转变为α+TiH₂共析组织及少量残余β相。真空除氢后,组织变为细小的等轴组织。氢处理提供了一种细化铸造Ti-6Al-4V组织的有效途径。     

Ti-6Al-4V合金氢致塑性效应与应用

利用光学显微镜研究了置氢处理后Ti-6A1-4V合金的微观组织,通过X射线衍射分析试验研究了置氢处理过程中的相转变过程;采用室温压缩试验研究了置氢处理后Ti-6Al-4V合金的变形行为,并进行了冷镦试验.结果表明,氢促进了α"马氏体与亚稳β相的形成,亚稳β相的形成与转变是Ti-6Al-4V合金变形性能提高的主要因素;在...     

粉末耐热钛合金组织性能及成形技术

采用热等静压技术及旋转电极粉,采用预合金粉粉末冶金工艺开展了粉末耐热钛合金TC11(Ti-6.5AJ-3.5Mo-1.5Zr-0.3Si)制备技术研究,研制出了全致密粉末TC11合金,通过热处理工艺研究优化粉末TC11材料的组织和性能.利用光学显微镜,对其组织进行了分析,用SEM观察了旋转电极粉末形貌,对室温及高温(550℃)拉伸性能及弹性模量等进行了测试分析.粉末TC11合金的组织和性能与同批次TC11锻棒材料进行了对比研究.利用特殊模具成形,开展了粉末TC11构件近净成形技术的研究,实现了整体大尺寸、带网格加强筋的薄壁粉末TC11合金航天飞行器舱体件近净成形,且未检测出内部缺陷.研究结果表明,粉末TC11合金具有与锻造材料相当的拉伸性能,而弹性模量更优,其金相组织均匀细致,形成了网篮组织,并有围绕其分布的等轴α.粉末TC11合金及合适的近净成形技术可在高性价比、高可靠性的轻质耐热航天飞行器构件制备中得到应用.     

变形工艺对Ti-3Al-5Mo-5V动态压缩变形的影响

采用显微组织分析和工艺试验相结合的方法系统分析了变形工艺对Ti-3A l-5Mo-5V钛合金动态压缩变形行为的影响规律。结果表明,变形速率和变形量影响着合金动态变形局部化的程度(剪切带的宽度)和变形过程中出现的剪切带的类型,动态变形后剪切带区域的硬度与其他位置的硬度差异较大,这种差异可以通过变形后适当的后续退火处理来消除。     

Grinding behavior and surface appearance of（TiC_p＋ TiB_w）/Ti-6Al-4V titanium matrix composites

（TiCp＋ TiBw）/Ti-6Al-4V titanium matrix composites（PTMCs） have broad application prospects in the aviation and nuclear field. However, it is a typical difficult-to-cut material due to high hardness of the reinforcements, high strength and low thermal conductivity of Ti-6Al-4V alloy matrix. Grinding experiments with vitrified CBN wheels were conducted to analyze comparatively the grinding performance of PTMCs and Ti-6Al-4V alloy. Grinding force and force ratios, specific grinding energy, grinding temperature, surface roughness, ground surface appearance were discussed. The results show that the normal grinding force and the force ratios of PTMCs are much larger than that of Ti-6Al-4V alloy. Low depth of cut and high workpiece speed are generally beneficial to achieve the precision ground surface for PTMCs. The hard reinforcements of PTMCs are mainly removed in the ductile mode during grinding. However, the removal phenomenon of the reinforcements due to brittle fracture still exists, which contributes to the lower specific grinding energy and grinding temperature of PTMCs than Ti-6Al-4V alloy.     

Tool Life and Surface Integrity in High-speed Milling of Titanium Alloy TA15 with PCD/PCBN Tools

Titanium alloys are widely used in aeronautics that demand a good combination of high strength, good corrosion resistance and low mass. The mechanical properties lead to challenges in machining operations such as high process temperature as well as rapidly increasing tool wear. The conventional tool materials are not able to maintain their hardness and other mechanical properties at higher cutting temperatures encountered in high speed machining. In this work, the new material tools, which are polycrystalline diamond (PCD) and polycrystalline cubic boron nitride (PCBN) tools, are used in high-speed milling of Ti-6.5Al-2Zr-1Mo-1V (TA15) alloy. The performance and wear mechanism of the tools are investigated. Compared to PCBN tool, PCD tool has a much longer tool life, especially at higher cutting speeds. Analyses based on the SEM and EDX suggest that attrition, adhesion and diffusion are the main wear mechanisms of PCD and PCBN tools in high-speed milling of TA15. Oxidation wear is also observed at PCBN tool/workpiece interface. Roughness, defects, micro-hardness and microstructure of the machined surface are investigated. The recorded surface roughness values with PCD/PCBN tools are bellow 0.3 μm at initial and steady cutting stage. Micro-hardness analysis shows that the machined surface hardening depth with PCD and PCBN tools is small. There is no evidence of sub-surface defects with PCD and PCBN tools. It is concluded that for TA15 alloy, high-speed milling can be carried out with PCD/PCBN tools.     

激光增材制造钛合金构件的化学抛光工艺研究

采用HNO3-HF抛光液对激光选区熔化钛合金制件进行化学抛光,以试样表面粗糙度、减薄及失重变化为指标探究了抛光过程中不同温度和时间对钛合金增材制件抛光效果的影响。通过电化学测量、拉伸试验、残余应力测试等方法对比分析了化学抛光前后钛合金试样的电化学和力学性能。结果表明在温度30℃、反应时间10min下抛光钛合金可以取得较理想的抛光效果,试样表面粗糙度减小、耐腐蚀性能提高。化学抛光后钛合金的强度出现小幅下降,内部原有的残余应力由拉应力转变为压应力。     

Biaxial tensile behavior of Ti-6Al-4V under proportional loading

The biaxial tensile behavior of isotropic Ti-6Al-4 V is characterized in this paper. A novel cruciform specimen was designed and optimized to achieve uniform stress and strain distribution within the gauge area. Biaxial tensile tests were conducted at three different loading ratios by the biaxial testing machine. The Digital Image Correlation (DIC) technique was applied to determine strain distribution, and a high-speed camera was employed to record the fracture process. An Inverse Analysis (IA) approach with a combined experimental and numerical method was proposed to determine the true stresses at the gauge section of the specimen during biaxial tensile tests. The results indicate that the initial yield locus can be described by the Cazacu criterion accurately, whereas the Mises criterion can predict better the strengthening behavior of Ti-6Al-4 V in the first quadrant in the principal stress space.     

飞机结构材料疲劳裂纹的扩展机制及其工程应用

 本文简要地评述了铝合金、钛合金和高强度钢的疲劳裂纹扩展机制及其工程应用;提出了预测疲劳裂纹扩展门槛值的一个普遍关系式;评价了现有四种超载模型对Ti-6A1-4V合金在拉伸超载下的延缓效应和预测寿命能力。对Willenborg和Maarse模型作了改进,并应用于A1和Ti合金的寿命预测。改进后的Maarse模型明显地提高了预测拉伸超载下和谱载下寿命的精度。文中还讨论了显微组织、应力比和表面状态等对材料疲劳裂纹扩展行为的影响。     

超声振动载荷下合金的疲劳寿命性能研究

 应用超声共振试验技术研究了三种工程常用合金(Ｕｄｉｍｅｔ５００,１７４ＰＨ和Ｔｉ－６Ａｌ－４Ｖ)在超声振动载荷(ｆ＝２０ｋＨｚ,Ｒ＝－１)下的疲劳寿命性能,并与常规疲劳载荷(ｆ＝２０－５０Ｈｚ,Ｒ＝－１)下材料的有关性能做了对比分析。研究结果表明,材料的超声疲劳寿命性能与其动态振动特性、机械响应以及载荷体制有关。     

Cr在Ti-Al-Cr合金抗高温氧化过程中的作用研究

研究了 Ti-50 Al,Ti-50 Al-1 5Cr,Ti-4 5Al-1 5Cr和 Ti-67Al-8Cr(原子百分数 )合金在 90 0～ 1 0 0 0℃下的高温氧化性能。结果表明 :Ti-50 Al-1 5Cr,Ti-4 5Al-1 5Cr和 Ti-67Al-8Cr均表现出优良的抗氧化性能,氧化后表面主要是 α-Al₂O₃及少量的 TiO₂ 组成。Ti-50 Al-1 5Cr,Ti-67Al-8Cr和 Ti-4 5Al-1 5Cr合金良好的抗高温氧化性能归于 Cr在合金抗氧化过程中起到了吸氧效应的作用。另外发现对于 Ti-50 Al-1 5Cr和 Ti-67Al-8Cr均发生了 950℃时的氧化增重比 1 0 0 0℃时的氧化增重大,这是由于 Cr的加入使 Ti的活性降低的缘故。