NiCrAlYSi涂层/DD6单晶高温合金界面再结晶和互扩散行为

采用电子束物理气相沉积(EB-PVD)在单晶高温合金DD6基体上沉积NiCrAlYSi涂层.利用X射线衍射(XRD)、扫描电镜(SEM)、能谱仪(EDS)以及透射电镜(TEM)等研究了高温扩散过程中NiCrAlYSi/DD6的界面再结晶和互扩散行为.研究结果表明合金表面喷砂处理后的涂层试样经1 323 K真空热处理4 ...     

原位合成TiB_2/6351复合材料热压缩变形特性

采用Gleeble-1500D热模拟试验机对原位合成TiB2(质量分数,8%)/6351复合材料在不同变形温度和不同应变速率条件下的热变形特性进行了研究,利用透射电镜(TEM)和光学显微镜分析了压缩后试样的微观组织.结果表明, 材料的流变应力随变形温度的升高而降低,随应变速率的提高而增大;材料的流变行为主要表现为加工硬化、动态回复和动态再结晶;相应的显微组织特征为:位错网络、混乱的位错团和胞状结构,亚晶及等轴晶.在应变速率和变形温度均较低时,增强体颗粒周围的基体中形成高密度位错区,但随变形温度的升高而减少;在应变速率较高时,增强体颗粒和基体的界面处开裂甚至增强体颗粒本身发生破碎.     

Surface Recrystallization in Nickel Base Single Crystal Superalloy DD6

The samples of single crystal superalloy DD6 are grit blasted and then heat treated either with the standard heat treatment procedure or in the temperature range of 1 000-1 250 °C for 4-16 h at vacuum atmosphere, then the recrystallization behavior of DD6 alloy is investigated. The results show that the equiaxed recrystallization grains form in the γ phase region where the as-cast γ′ phases have been dissolved completely, and cellular recrystallization forms in the region where the as-cast γ′ phases have been dissolved partially. The cellular recrystallization area consists of cellular grains, and the cellular grain consists of cubic γ′ phase, lamellar γ′ phase and γ+γ′ The coexistence of the equiaxed recrystallization zones and cellular recrystallization zones is a recrystallized characteristic of the cold worked single crystal samples which are heat treated at a temperature lower than the solution temperature. When the heating temperature is higher than 1 150 °C, with the increase of heat treating temperature, the equiaxed recrystallization zone expands, whereas the cellular recrystallization zone shrinks. All the deformed regions are consumed by equiaxed recrystallization after annealing at solution temperature.     

高纯α—Fe热压缩动态复原机制的研究

用高纯α-Fe在GLEEBLE-1500热模拟机上率进行了热压缩试验。变形温度分别为550℃,700℃,800℃和900℃,应变速率分别为0.001s~(-1),0.01s~(-1),0.1s~(-1),1s~(-1)和10s~(-1)。对其热压缩过程中的显微结构变化及真应力-真应变曲线进行的研究结果表明,形变温度的增加和应变速率降低有利于动态再结晶的进行;对动态再结晶与Z参数关系的研究结果表明,在一定的Z参数范围内即25<1nZ<37,高纯α-Fe可以发生动态再结晶,并给出动态再结晶图。     

锆元素在铝合金中的应用

概述了锆元素在铝合金中的存在形式,重点讨论其对铝合金各项性能的作用机理,包括对合金的再结晶行为,淬火敏感性,时效行为以及合金综合性能(强度、断裂韧性、抗应力腐蚀性能等)的影响变化。简要介绍了锆元素在铝合金,尤其在高强铝合金中的典型应用,并结合当前锆元素研究发展的新趋势,指出对锆元素的研究认识需进一步深入和突破。     

表面再结晶对定向凝固高温合金高周疲劳行为的影响

采用悬臂旋转弯曲试验,研究定向凝固DZ4合金在喷丸预变形及热处理后产生的再结晶层对高周疲劳寿命的影响.结果表明,DZ4合金经过一定程度的预变形,在随后的高温热处理后表面会产生一定厚度的再结晶;再结晶层对DZ4合金高周疲劳寿命有一定影响;在一定喷丸强度范围内,随喷丸强度增加,疲劳寿命先减小后增大.     

GH4169高温合金惯性摩擦焊接头动态再结晶过程

当温度、应变、应变速率达到一定条件时 ,GH4 16 9镍基高温合金在惯性摩擦焊接过程中易发生动态再结晶。本文研究结果表明 ,由于GH4 16 9合金惯性摩擦焊接时间很短 ,动态再结晶进行得相当充分 ,而动态回复不足 ,在动态再结晶的过程中还可以看到有些结晶过程还处于形核阶段 ,这是惯性摩擦焊接头产生细晶乃至超细晶的根本原因     

镍基单晶叶片制造技术及再结晶研究进展

针对航空发动机单晶涡轮叶片的制造技术以及再结晶缺陷进行分析,结合国内外研究现状,从单晶空心涡轮叶片铸造技术、单晶空心涡轮叶片再结晶缺陷及单晶叶片再结晶控制方法等方面,对单晶叶片制造技术及再结晶控制方法取得的研究成果进行总结和分析。重点介绍了叶片制造技术和再结晶控制技术的方法及研究。对我国单晶空心涡轮叶片制造技术及再结晶缺陷的进一步研究重点进行分析。     

SiC_P/Al-Cu复合材料动态再结晶行为及临界条件

利用Gleeble-1500D热模拟试验机对40%SiC_P/Al-Cu复合材料进行压缩实验,研究其在温度为350~500℃、应变速率为0.01~10 s~(-1)条件下的高温塑性变形行为。由实验得出变形过程中的应力-应变曲线,采用加工硬化率处理方法对应力-应变数据进行处理,结合lnθ-ε曲线的拐点和(-α(lnθ)/αε)-ε曲线最小值的判据,研究该复合材料动态再结晶临界条件。结果表明:40%SiC_P/Al-Cu复合材料的应力-应变曲线主要以动态再结晶软化机制为特征,峰值应力(σ_p)随变形温度的降低或应变速率的升高而增加;该材料的lnθ-ε曲线出现拐点,(-α(lnθ)/αε)-ε曲线出现最小值;临界应变(ε_c)随变形温度的升高与应变速率的降低而减小,且临界应变与峰值应变(εp)之间具有相关性,即ε_c=0.528εp;临界应变与Zener-Hollomon参数(Z)之间的函数关系为ε_c=4.58×10~(-3)Z~(0.09)。透射电镜观察显示应变为0.06时(变形温度为400℃,应变速率为10 s~(-1))已经发生动态再结晶,应变为0.2时,动态再结晶晶粒充分长大。     

A step deformation method for superplasticity improvement of coarse-grained Ti–15V–3Cr-3Sn-3Al

Ti–15V–3Cr–3Sn–3Al(Ti–15–3), a kind of metastable beta titanium which has high specific strength and good cold-formability, is highlighted for applications in the aerospace manufacture industry. However, the technique for improving its formability at elevated temperatures is still a challenge at present. In this work, a step deformation method is proposed for superplasticity improvement of coarse grained Ti–15–3 plates at temperatures around its beta transus. The effects of the strain rate and the strain at the first stage on the superplasticity are investigated. The results show an increase of the strain rate sensitivity and a decrease of the flow stress under the step deformation mode compared to those obtained under constant strain rates at 780℃. The maximum strain to failure obtained in the step mode is 93% higher than that deformed in the constant strain rate mode. Strain rates, strains at the first stage, and temperatures have influences on the superplasticity improvement. The deformation mechanism is concluded as subgrain formation accommodated by grain boundary sliding rate-controlled by dislocation climb. The improved m value in the step deformation is accounted to the extra dislocation density produced during the strain rate reduction.