曲面不锈钢/微晶玻璃层状复合材料的设计制备

设计制备了与1Cr17和0Cr18Ni9不锈钢匹配的CaO-Al2O3-SiO2(CAS)系和BaO-Al2O3-SiO2(BAS)系微晶玻璃,研究了微晶玻璃的各项理化性能。利用流延法制备微晶玻璃生带,以此制备符合曲面不锈钢/微晶玻璃层状复合材料,并对复合材料相关性能进行测试。结果表明,所设计制备的玻璃经850℃、30min热处理后可形成线胀系数与对应不锈钢匹配的微晶玻璃,且具有适宜弯曲强度和较低介电常数、介质损耗;由此制备的曲面不锈钢/微晶玻璃层状复合材料具有良好的绝缘性能、结合强度和抗热冲击性能。     

含硼富燃料推进剂燃烧机理研究

分析了AP包覆硼对含硼富燃料推进剂低压燃烧的影响。通过微热电偶测温和火焰单幅照相技术分别测试含硼富燃料推进剂燃烧波温度分布及燃烧火焰结构；根据气相温度变化的趋势，把该推进剂的气相区燃烧又分为三个子区，并给出了三个子区的厚度，分析了各区温度变化趋势不同的原因。用扫描电镜对熄火表面形貌进行观察，并通过能谱仪进行局部元素分析；该推进剂中断燃烧熄火纵向剖面的实验表明，该推进剂的燃烧表面存在“沉积层”；分析认为该“沉积层”由硼、积炭和少量的三氧化二硼组成，且基本惰性。燃面上“沉积层”的厚度与温度分布曲线中燃面上气相区的厚度基本一致，认为该推进剂的气相反应在燃面上的惰性“沉积层”中进行。     

316不锈钢/WC-Co涂层在锌液中的腐蚀

研究了经高速火焰喷涂(HVOF)的316不锈钢WC-Co涂层在锌液中的腐蚀行为,包括腐蚀速度、界面组织形貌和成分的变化.结果表明,WC-Co涂层在锌液中的腐蚀表现为沿裂纹的腐蚀.涂层中的缺陷造成裂纹源,在锌液和热喷涂过程留下的残余热应力的作用下,发生裂纹扩展,形成沿裂纹的腐蚀.铬和铝的扩散能力都比锌强,在产生裂纹的初期,铬和铝将优先锌扩散到裂纹中.如果适当改善喷涂工艺,增加涂层的致密度,可以延长涂层的使用寿命.     

基于Euler／N—S方程的跨音速非线性静气动弹性问题研究

在C-H网格的基础上,采用Jameson的中心差分有限体积法求解Euler/N-S方程,采用结构影响系数法计算结构的弹性变形,用三角元面积加权法和常体积转换法(CVT)实现流固耦合,计算了弹性后掠机翼在跨音速状态的静气动弹性问题     

Effect of Counterface Material on Friction and Wear Behavior of Ni-Cr-W-Al-Ti-MoS_2 Composites

Ni-Cr-W-Al-Ti-MoS2 self-lubricating composites were prepared through the powder metallurgy (P/M) method. Their friction properties were investigated by a pin-on-disk tribometer in the range from the room temperature to 600 ℃. Alumina, silicon nitride and nickel-iron-sulfide alloys were selected as the counterface materials. Results indicate that the lowest friction coefficients under 0.22 can be obtained at 600 ℃ when rubbed against alumina. When rubbed against nickel-iron-sulfide alloys, are presented the lowest wear rates in the magnitude of 10-6 mm3/N·m, one order of magnitude lower than those when rubbed against ceramics. In the case of three rubbing pairs, the wear rates of the composite containing MoS2 present themselves inversely proportional to friction coefficients. With alumina ceramics used as a counterface, transfer films and glaze layers will form on the contact surface playing a main role in lubrication at high temperatures. However, when silicon nitride and nickel-iron-sulfide alloy are used, the lubricating transfer films appear not to be promi-nent.     

Preparation,Growth Mechanisms and Characterizations of ZnSe Films via the Solvothermal Method

With diethylamine as a solvent, ZnSe films were formed on the Si substrate directly from zinc and selenium through the modified solvothermal method. The effects of holding temperature, deposition time and substrate surface treatment on the quality and morpholo-gies of the ZnSe films were investigated. The growth mechanism of ZnSe films was proved to be a layer-nucleation growth process, which was tied in with the Stranski-Krastanov (SK) model. ZnSe films were identified by the X-ray diffraction pattern (XRD), the scan-ning electron microscope (SEM), the X-ray photoelectron spectroscope (XPS) and the photoluminescence (PL) techniques. The results indicate that the modified solvothermal method with diethylamine as a solvent is suitable to prepare high quality ZnSe films.     

三通管复合胀形过程模拟

建立了三通管复合胀形的三维弹塑性有限元模型,研究了三通管液压复合胀形中,反压大小、加载路径以及加载时间等对胀形成形的影响。     

MOCVI制备Nextel 720/SiO2复合材

研究了MOCVI(MetalOrganicChemicalVaporInfiltration)方法制备Nextel720/SiO     

金属基复合材料热循环损伤的共振检测方法研究

本文叙述了金属基复合材料热循环损伤的动态共振检测方法，利用该方法对Ｂ／Ａｌ、ＳｉＣｆ／Ａｌ和Ｃ／Ｍｇ等单向排列金属基复合热循环损伤进行了检测，得出一些结果，并进行了讨论。     

TC6钛合金棒材热处理工艺研究

对TC6钛合金φ20mm～φ120mm不同规格棒材进行了普通退火、双重退火、等温退火、固溶时效等热处理方法和热处理制度研究,并对比分析了热处理制度和组织、性能之间的影响关系,结果表明,TC6钛合金的组织和性能对热处理工艺敏感,应根据半成品规格、类型、截面形状、使用温度、受力情况以及设备条件等诸多因素选择合适的热处理方法和制度,才能达到强度、塑性和韧性的最佳匹配。研究结果证实普通退火是一种简单易行的退火制度,适用于飞机结构用中等规格棒材等半成品的退火,进一步提出了TC6钛合金棒材的热处理工艺选择原则。