Ti2SnC的合成及其反应机制的研究

采用常压烧结技术,分别对Ti/Sn/C和Ti/Sn/TiC两种配料,在950～1250℃温度范围、保温15～360 min,真空条件下进行烧结.结果表明,两种配料均在1200℃短时间内合成了高纯度Ti2SnC粉.利用X射线衍射(XRD),能量色散谱仪(EDS)及扫描电镜(SEM)对Ti2SnC粉末进行了表征,并对Ti2SnC的形成机制进行了分析.所制备的Ti2SnC为片状颗粒,表面光滑,颗粒尺寸小于10 μm,厚度约为1～2 μm.Ti2SnC的形成机制是,在Ti-Sn-C反应系统中,Ti和Sn先反应形成Ti-Sn化合物;然后是Ti和C反应形成TiC;最后,Ti-Sn化合物和TiC反应形成Ti2SnC.此反应机制进一步由Ti-Sn-TiC反应系统验证.     

无人机进气道设计中的隐身技术

无人机在现代战争中发挥着越来越大的作用,但也呈现出易受攻击和易被摧毁的弱点,因此迫切需要采取有效的措施来提高无人机在复杂战场环境中的生存能力.阐述了进气道隐身设计对无人机隐身的重要性,并从进气道气动隐身设计和吸波材料在进气道隐身中的应用方面对改善无人机的隐身性能进行了详细分析.     

风云二号B星原始云图中频模拟器

为了配合风云二号B星原始云图调解器的研制，制作了相关的卫星信号的中频模拟设备。该中频模拟器由突发数据源，噪声源和调制器三部分组成，介绍了其系统原理和各单元实现。     

Orbital phase spectroscopy of X-ray pulsars to study the stellar wind of the companion

High Mass X-ray Binary Pulsars (HMXBP), in which the companion star is a source of supersonic stellar wind, provide a laboratory to probe the velocity and density profile of such winds. Here, we have measured the variation of the absorption column density along with other spectral parameters over the binary orbit for two HMXBP in elliptical orbits, as observed with the Rossi X-ray Timing Explorer (RXTE) and the BeppoSAX satellites. A spherically symmetric wind profile was used as a model to compare the observed column density variations. In 4U 1538-52, we find the model corroborating the observations; whereas in GX 301-2, the stellar wind appears to be very clumpy and a smooth symmetric wind model seems to be inadequate in explaining the variation in column density.     

Characterizing slope correction methods applied to satellite radar altimetry data: A case study around Dome Argus in East Antarctica

Slope correction is important to improve the accuracy of satellite radar elevation measurements by mitigating the slope-induced error (SE), especially over uneven ground surfaces. Although several slope correction methods have been proposed, guidance in the form of stepwise algorithm on how to implement these methods in processing radar altimetric data at the coding level, and the differences among these methods need to be presented and discussed systematically. In this paper, three existing types of slope correction methods—the direct method (DM), intermediate method (IM), and relocation method (RM, further divided into RM1 and RM2)—are described in detail. In addition, their main differences and features for various scientific applications are analyzed. We conduct a systematic experiment with CryoSat-2 Low Resolution Mode (LRM) data in a physically stable area around Dome Argus in East Antarctica, where in-situ measurements were available for comparison. The slope correction is implemented separately using the three methods, with the latest high-accuracy Reference Elevation Model of Antarctica (REMA) as the a-priori topography model. The bias and precision of the slope-corrected CryoSat-2 data results from the RM2 is ?0.18 ± 0.86 m based on the comparison with the field Global Navigation Satellite System (GNSS) data. The results from the RM2 indicate higher precision compared to those from the RM1. According to the correlation analysis of the slope-corrected CryoSat-2 data results (RM1 and RM2), the bias enlarges and the precision becomes worse when the surface slope increases from 0 to 0.85°. After a comprehensively comparative analysis, we find that the results from the RM1 and RM2 are superior in precision (0.93 m and 0.86 m) with respect to the GNSS data. The relatively low precision (1.22 m) from the IM is due to the potential error from the a-priori digital elevation model (DEM). The DM has the lowest precision (2.66 m). Another experiment over rough topography in West Antarctica is carried out for comparison, especially between the RM1 (precision of 15.27 m) and RM2 (precision of 16.25 m). In general, the RM is recommended for the SE elimination among the three methods. Moreover, the RM2 is firstly considered over smooth topography due to the superior performance in bias and precision, while the RM1 is more suggested over the rough topography because of the slightly smaller bias and better precision. The IM relies much on the accuracy of the a-prior DEM and is not usually recommended, because of the strict requirement in the sampling time between the radar altimetry data and the a-priori DEM to avoid any surface change over time.     

Higher order ionospheric error correction in BDS precise orbit determination

The ionospheric error affects the accuracy of the Global Navigation Satellite Systems observation and precise orbit determination. Usually, only the first order ionospheric error is considered, which can be eliminated by the ionospheric-free linear combination observation. But the remaining higher order ionospheric error will affect the accuracy of observations and their applications. In this paper, the influence of the higher order ionospheric error have been studied by using the International Geomagnetic Reference Field 13 and the Global Ionosphere Maps model produced by the Center for Orbit Determination in Europe. Focus on ionospheric error, the experiment of paper at doy 302 in 2019, which show that the second order ionospheric error impacting BeiDou Navigation Satellite System (BDS) B1I and B3I observation is 6.3569 mm and 11.8484 mm, respectively. Whereas, the third order ionospheric error impacting BDS B1I and B3I observation is 0.1734 mm and 0.3977 mm, respectively. Due to the current measurement accuracy of BDS carrier-phase observation can reach 2 mm, the influence of high order ionospheric error on observation should be considered. For BDS precise orbit determination, the orbit overlapping results are indicated that its orbit accuracy can be improved approximately 5 mm with the higher order ionospheric error correction, which is also in agreement with the results of Satellite Laser Ranging in this work.     

Fe_2O_3/石墨烯复合物的制备及催化性能研究

以氧化石墨烯和硝酸铁为原料,采用水热法制备Fe_2O_3/石墨烯复合物。采用XRD、FTIR、RAMAN、SEM等对其结构和形貌进行表征,并通过不同升温速率的TG-DSC研究Fe_2O_3/石墨烯复合物对HMX热分解催化作用。结果表明,在氧化石墨烯被还原为石墨烯过程中,同时Fe_2O_3纳米粒子负载于石墨烯片层上;Fe_2O_3/石墨烯复合物可使HMX热分解活化能降低51.13 kJ·mol~(-1),对HMX有较好的催化作用。     

全方向长期伴飞卫星集群轨道设计与仿真

主要研究在J2摄动的影响下，在中心卫星周围全方向上部署长期相对有界伴飞卫星的轨道设计方法。首先，利用J2不变的条件，由已知中心卫星轨道根数建立伴飞卫星的半长轴、偏心率及轨道倾角之间关系。然后，通过对伴飞卫星和中心卫星之间初始相对位置及轨道根数之间关系的分析，得到伴飞卫星的全部初始轨道根数，使其能够部署到中心卫星周围的任意方向上，从而能实现卫星集群在中心卫星的周围全方向长期有界伴飞。最后，通过轨道仿真验证了该方法的有效性。     

衬底温度对共溅射法制备的Cu2ZnSnS4薄膜晶粒生长的影响

研究了衬底温度对采用Cu2ZnSnS4靶和Cu靶共溅射制备的Cu2ZnSnS4薄膜晶粒生长的影响。采用拉曼光谱、X射线能量色散谱仪、扫描电子显微镜和紫外 可见 近红外分光光度计对在不同衬底温度条件下制备的Cu2ZnSnS4薄膜 的元素比例、形貌以及光学带隙进行了表征与分析。结果表明制备的Cu2ZnSnS4薄膜晶粒生长遵循不同规律。室温衬底条件下制备的Cu2ZnSnS4薄膜晶粒生长遵循两步法，导致颗粒尺寸和元素分布不均；而在120~200 ℃衬底温度条件下制备的Cu-Zn-Sn-S预置层在溅射过程中已有Cu2ZnSnS4晶粒形成，这些晶粒在后续硫化生长过程中起到形核点的作用， 促进了Cu2ZnSnS4晶粒的长大与元素的均匀分布。随着衬底温度的升高，Cu-Zn-Sn-S预置层及由此制备出的Cu2ZnSnS4薄膜的结晶性变好，Cu2ZnSnS4薄膜的带隙先升高后减小至1.55 eV。     

Two-Dimensional Modal Curvature for Damage Detection in Plates

Mode shape has become a hotspot of vibration-based damage detection in plates.Two-dimensional(2D)modal curvature(MC2D),derived from mode shapes,is a prevailing physical quantity used to indicate damage.Unfortunately,the physical mechanism of MC2 Dfor characterizing damage in plates has not been clarified to date.In contrast,one-dimensional(1D)modal curvature(MC1D)has explicit physical mechanism to portray damage in beams.Unresolved physical mechanism of MC2 Dseverely hampers its applications for damage identification in plates.To address this deficiency,the clarification mechanism of MC2 Dis investigated to identify damage.With the clarified mechanism,numerical and experimental cases are used to demonstrate the effectiveness of MC2 Din detecting damage in plates.