TC11钛合金钨极氩弧焊工艺试验研究

针对TC11钛合金材料进行了自动钨极氩孤焊接工艺试验,获得了成形良好的焊缝,焊接质量符合航空Ⅰ级焊缝标准.采用金相试验方法和力学性能试验对不同焊接填充材料下的显微组织和性能进行对比.结果表明,采用TC11同质焊丝可获得与母材抗拉强度相当的焊接接头,略高于采用TA2纯钛焊丝的接头,但采用TA2焊丝时的集中塑性接近母材.     

TC18钛合金焊接接头应用性能研究

采用氩弧焊和电子束焊2种焊接工艺对TC18锻坯进行焊接,按焊接接头试验方法进行了拉伸和冲击试验,获得了焊接接头的强度系数和冲击韧性。试验结果表明,TC18钛合金焊接接头具有良好的焊接性,同时,对于飞机焊接结构设计应优先选用电子束焊。     

TC4/TA18钛合金蜂窝夹层结构钎焊工艺研究

针对TC4/TA18钛合金蜂窝夹层结构,采用Ti-37.5Zr-15Cu-10Ni非晶箔带钎料,研究钎焊温度和保温时间对TC4/TA18钛合金蜂窝夹层结构接头微观组织及力学性能的影响,优化出TC4/TA18钛合金蜂窝夹层结构较优的钎焊工艺为920℃/保温90min和钎料添加量80μm,该工艺参数下钎焊接头的室温拉脱强度平均值最高,可达19.82MPa,破坏部位为TA18钛合金蜂窝芯。     

激光熔化沉积快速成形TC4钛合金的焊接性能

为了探索激光熔化沉积快速成形技术制备TC4钛合金的焊接性能,分别采用电子束焊、激光焊两种方法制备接头试样,并借助金相、硬度试验等方法获得接头力学性能、显微组织及硬度。结果表明:两种焊接方法得到的接头抗拉强度最高达953 MPa,焊接系数均0.9;激光和电子束焊接焊缝为网篮状α'相马氏体组织,热影响区为α相和针状马氏体组织组成。激光熔化沉积快速成形TC4钛合金和传统工艺制造的TC4钛合金在焊接特性方面表现相当。     

钛合金薄板对接及锐角接电子束焊接

针对TC4钛合金薄板对接接头和TC1钛合金薄板锐角接头进行电子束焊接工艺研究,得到TC4及TC1钛合金薄板的电子束焊接工艺参数.通过常规力学性能测试和X射线检查,TC4钛合金对接焊缝的拉伸强度平均为1050MPa,达到了母材强度的95％以上.试验结果证明,上述工艺参数得到的焊缝,满足设计及相关文件的要求.     

异种状态TC4钛合金电子束焊接性能分析北大核心CSCD

针对相对疏松的铸造钛合金和相对密实的锻造钛合金的焊接问题,开展了两种状态的TC4钛合金电子束焊接工艺研究,对比了不同焊接参数对焊接质量的影响。研究结果表明,采用方波扫描可以较好地实现铸造钛合金与锻造钛合金的连接,焊缝成形良好,内部无缺陷;焊接接头力学性能分析表明,拉伸断裂位置全部在铸件母材区一侧。实焊结果证明,电子束焊接可以实现异种状态TC4钛合金焊接的工程化应用。     

异种状态TC4 钛合金电子束焊接性能分析

针对相对疏松的铸造钛合金和相对密实的锻造钛合金的焊接问题,开展了两种状态的TC4钛合金电子束焊接工艺研究,对比了不同焊接参数对焊接质量的影响。研究结果表明,采用方波扫描可以较好地实现铸造钛合金与锻造钛合金的连接,焊缝成形良好,内部无缺陷;焊接接头力学性能分析表明,拉伸断裂位置全部在铸件母材区一侧。实焊结果证明,电子束焊接可以实现异种状态TC4钛合金焊接的工程化应用。     

TC18钛合金焊接接头力学性能试验研究

氩弧焊和电子束焊是钛合金加工中两类常见的工艺方法,对比研究两种工艺对焊接接头力学性能的影响对其在工程中的合理选用具有重要的参考价值。完成了TC18钛合金氩弧焊接头和电子束焊接头的静力拉伸及旋转弯曲疲劳试验,并根据试验结果对两类焊接接头的力学性能进行了对比分析,采用统计学方法给出了二者的中值疲劳寿命SN曲线及疲劳极限。研究结果表明：氩弧焊接头焊缝区内晶粒粗大,使得材料的力学性能明显劣化;电子柬焊接头具有更高的抗拉强度与更好的高周疲劳性能,更有利于工程应用。     

大厚度TC4-DT钛合金电子束焊接接头微观组织和力学性能研究

对60mm厚TC4-DT钛合金锻件进行电子束焊接。通过对焊接接头显微组织观察,拉伸、冲击、断裂韧性测试,研究了该合金电子束焊接接头的力学性能。结果表明:TC4-DT钛合金具有良好的焊接工艺性能。焊缝为α相网篮组织,该合金电子束焊接接头的拉伸强度与基材相当,但冲击韧性与锻件相比略低。同时,该合金焊接接头也具有良好的损伤容限性能,与锻件相比焊接接头的断裂韧性下降约20%。     

TC17钛合金在TIG焊接方法下的焊接性研究

利用填充TA2焊丝的TIG焊接方法,研究了焊接接头组织和性能特点,并利用焊前涂覆活性剂和焊后进行热处理的正交试验,讨论了焊前和焊后处理方法对焊接接头性能的影响。试验结果表明,TC17钛合金TIG焊接接头明显可见焊缝、熔合线和热影响区等区域,焊缝区柱状晶特点明显并且存在一定量的小气孔,热影响区晶粒较大;焊接接头组织较母材有软化的倾向。焊后接头强度达到母材的85%,热处理后接头强度可达到母材的90%以上,并且热处理后的焊接接头具有良好的高温拉伸、持久性能,显示出TC17钛合金具有良好的焊接性。     

TC21细晶钛合金TIG焊接接头组织及力学性能研究

开展了不同晶粒尺寸的细晶粒TC21钛合金的TIG焊接实验,研究了母材及接头组织和力学性能。结果表明：细晶粒TC21钛合金TIG焊接接头抗拉强度达到母材的95％左右,焊接性较好;但是焊接接头脆化严重,伸长率和断面收缩率均较低。焊缝中心和热影响区组织相似,为α’马氏体组织。相同焊接规范下,21μm的细晶TC21合金焊缝及热影响区为片状或长粒状α’组织;而7μm的细晶TC21合金接头中α’丛的尺寸较小且相互交错,形成针状或短粒状α’组织。硬度测试表明：靠近母材的热影响区细晶区存在一个软化区,该区域硬度最低,而焊缝中心与热影响区粗晶区分界处（细晶过渡区（FTZ））也存在硬度的下降,不过此区域下降幅度不大。常温拉伸断口呈准解理断裂特征,随着母材晶粒度的增大,焊接接头解理特征越明显。     

TC18钛合金普通退火工艺研究

研究了普通退火工艺参数对TC18（Ti-5A1-5Mo-5V-1Cr-1Fe）钛合金显微组织和力学性能的影响。结果表明,合金强度随退火温度升高先降低后上升,900％及以上温度退火后合金强度可达到1100MPa以上。a相形状、数量及尺寸等方面的变化是影响合金强度和塑性的关键因素。     

Joining of SiO2 ceramic and TC4 alloy by nanoparticles modified brazing filler metal

Nano-Al₂O₃ particles modified AgCuNi filler was adopted to braze the SiO₂ ceramic and TC4. The effects of filler size as well as the brazing temperature on the interfacial microstructure and mechanical property of the joints were investigated. Nanoscale filler reduced the phases dimension and promoted the homogeneous distribution of microstructure, obtaining a higher joint strength when compared to microscale filler. The increase of brazing temperature made the accelerating dissolution and diffusion of Ti, which promoted the increase of thickness of Ti₄O₇ + TiSi₂ layer adjacent to SiO₂ ceramic and diffusion layer zone nearby TC4 alloy. The hypoeutectic structure was produced in the brazing seam due to the high Ti content. The maximum shear strength of ∼40 MPa was obtained at 950 °C for 10 min.     

TC4-DT钛合金线性摩擦焊接头组织和力学性能分析

针对飞机用典型的TC4-DT钛合金线性摩擦焊接头,开展组织及接头的拉伸、冲击和低周疲劳等力学性能测试。结果表明:TC4-DT钛合金线性摩擦焊接头经过700℃+保温3h的热处理后,接头的室温和高温抗拉强度达到母材的97%以上,室温和低温冲击性能略高于母材,室温低周疲劳性能与母材相当,具有良好的综合力学性能。     

BT20钛合金激光焊技术研究

针对2.5 mm厚BT20钛合金进行了CO2激光焊和YAG激光焊研究,结果表明由于激光特性不同,形成的焊缝几何特征不同,当焊接工艺适当,可保证焊接过程的稳定性和焊接接头的质量.在激光自熔焊时主要的焊缝缺陷是咬边,这是由于钛合金物理性能和激光高能束流焊特性所致.这种咬边缺陷不利于焊接接头性能,尤其是接头的疲劳性能和断裂韧性.采用活性剂和填丝焊,以及激光旋扫焊可以改善焊缝咬边缺陷,提高钛合金激光焊接头的力学性能.     

TC4钛合金线性摩擦焊接头的冲击韧性及断口特征

在自制的XMH-160型线性摩擦焊机上利用先期试验优化的规范参数进行TC4线性摩擦焊接试验.对焊后试件进行冲击试验研究,冲击试件基本沿母材断裂.观察冲击试件的宏观和微观断口,并分析接头的金相组织.结果表明,焊缝超细晶组织所具有的高断裂应力是焊接接头冲击韧性值高于母材的主要原因.     

Hot deformation behavior and strain compensation constitutive model of equiaxed fine grain diffusion-welded micro-duplex TC4 titanium alloy

In this work, two-stage diffusion bonding of micro-duplex TC4 titanium alloy was carried out to study the flow behavior and constitutive models of the bonding joint and the base metal after the same thermal cycling during the hot forming process. Microstructure and mechanical properties test were used to verify the good quality of the equiaxed fine grain diffusion-welded TC4 alloy. Quasi-static tensile experiment was carried out at temperatures ranging from 750–900 °C and strain rates of 0.0001–0.1 s⁻¹. The joint showed the weak dynamic recovery at strain rates of 0.01–0.1 s⁻¹ and temperatures of 750–850 °C. At strain rates of 0.0001–0.001 s⁻¹ and temperatures of 850–900 °C, the flow stress of joint presented steady-state characteristics. Different deformation conditions lead to the remarkable difference of dynamic softening performance between the joint and heat-treated base metal, but the flow stress in elastic and strain hardening stages exhibited similar behavior. The strain compensated Arrhenius-type constitutive models of TC4 joint and heat-treated base metal were developed respectively. The fifth-order polynomial functions between the material property correlation coefficients and strain were obtained. The models have shown good correlation, with correlation coefficient values of 0.984 and 0.99. The percentage average absolute relative error for the models were found to be 10% and 9.46%, respectively.     

Substructure evolution in two phases based constitutive model for hot deformation of TC18 in α + β phase region

The α + β dual phase titanium alloys are key structural materials in aviation and aerospace industries, and the complicated flow behavior of these titanium alloys during hot deformation requires to establish a constitutive model incorporating physical mechanism for optimizing processing parameters and designing forming tools. This work aims to establish a constitutive model incorporating physical mechanism for hot deformation of TC18 in α + β phase region. Firstly, the flow behavior and microstructure evolution for hot deformation of TC18 in α + β phase region are characterized. The TC18 shows significant strain hardening rate and negative strain hardening exponent around and after peak flow stress, respectively. After peak flow stress, Dynamic Recovery (DRV) mechanism dominates the evolution of α and β phases according to the results of substructure evolution. Then, the internal state variables method is applied to establish a constitutive model incorporating physical mechanism for hot deformation of dual phase titanium alloys. The variation of dislocation density during the hot deformation of titanium alloys is modeled by considering the accumulation of dislocation due to the impediment to dislocation movement by substructure obstacles and the annihilation of dislocation due to the dynamic restoration effect. The interaction between dislocations, the subgrain boundaries and the grain/phase boundaries obstruct the dislocation movement in the α phase, and the first two obstructs the dislocation movement in the β phase during the hot deformation of TC18. The dislocation annihilation process in the α and β phases during the hot deformation of TC18 is dominated by DRV. Finally, the substructure evolution in the two phases based constitutive model for hot deformation of TC18 in α + β phase region is presented. This model is well applied to predict the flow stress and quantitively analyze the role of DRV effect in the evolution of α and β phases during the hot deformation of TC18.