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PIP工艺制备SiC晶须增强SiCf/SiC复合材料的性能
引用本文:姜卓钰,吕晓旭,周怡然,齐哲,高晔,赵文青,焦健. PIP工艺制备SiC晶须增强SiCf/SiC复合材料的性能[J]. 航空材料学报, 2021, 0(2)
作者姓名:姜卓钰  吕晓旭  周怡然  齐哲  高晔  赵文青  焦健
作者单位:中国航发北京航空材料研究院先进复合材料国防科技重点实验室;中国航发北京航空材料研究院表面工程研究所;北京理工大学材料学院
基金项目:国家科技重大专项(2017-VI-0007-0077)。
摘    要:以不同界面层厚度的SiC纤维为增强相,采用先驱体浸渍裂解工艺(PIP)制备SiCf(PyC)/SiC复合材料,并在复合材料基体中引入SiC晶须,对其性能进行研究。结果表明:热解碳(PyC)界面层厚度约为230 nm时,SiC纤维拔出明显,SiCf/SiC复合材料拉伸强度、弯曲强度和断裂韧度分别达到192.3 MPa、446.9 MPa和11.4 MPa?m1/2;在SiCf/SiC复合材料基体中引入SiC晶须后,晶须的拔出、桥连及裂纹偏转等增韧机制增加了裂纹在基体中传递时的能量消耗,使复合材料的断裂韧度和弯曲强度分别提高了22.9%和9.1%。

关 键 词:碳化硅  复合材料  SIC晶须  力学性能

Performance of SiC whisker reinforced SiCf/SiC composites fabricated by PIP
JIANG Zhuoyu,LYU Xiaoxu,ZHOU Yiran,QI Zhe,GAO Ye,ZHAO Wenqing,JIAO Jian. Performance of SiC whisker reinforced SiCf/SiC composites fabricated by PIP[J]. Journal of Aeronautical Materials, 2021, 0(2)
Authors:JIANG Zhuoyu  LYU Xiaoxu  ZHOU Yiran  QI Zhe  GAO Ye  ZHAO Wenqing  JIAO Jian
Affiliation:(National Key Laboratory of Advanced Composites,AECC Beijing Institute of Aeronautical Materials,Beijing 100095,China;Surface Engineering Division,AECC Beijing Institute of Aeronautical Materials,Beijing 100095,China;School of Materials Science&Engineering,Beijing Institute of Technology,Beijing 100081,China)
Abstract:SiCf/SiC composites with the polycarbosilane and silicon carbide fiber of different pyrolytic carbon(PyC)interphase thicknesses as the reinforcement phase were fabricated by a polymer impregnation and pyrolysis(PIP)method.And SiC whisker was introduced into the SiCf/SiC composites to further improve its performance.It is found that the mechanical properties of SiCf/SiC composites have outstanding tensile strength,fracture toughness and flexural strength of 192.3 MPa,446.9 MPa and 11.4 MPa?m1/2,when the PyC interphase thickness is about 230 nm.After the introduction of SiC whisker,into the SiCf/SiC composite matrix,the toughening mechanisms such as whisker pull-out,whisker bridging and crack deflection increase the energy consumption when the crack is transferred in the matrix,and the fracture toughness and bending strength of the composite are increased by 22.9%and 9.1%respectively.
Keywords:silicon carbide  composite  SiC whisker  mechanical properties
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