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1.
CuO/CNTs复合催化剂的制备及对FOX-12热分解的催化性能 总被引:3,自引:0,他引:3
以醋酸铜和碳纳米管为原料,采用溶胶浸渍法在常压低温(100℃)下制备出CuO/CNTs复合催化剂,采用XRD、TEM、ICP等对催化剂进行表征,并用DSC研究催化剂对FOX-12热分解特性的影响。TEM结果表明,纳米CuO以8~10 nm的椭球形粒子和宽度为5 nm、长度为50 nm的棒状粒子2种形态附着在碳纳米管表面。催化剂使FOX-12分解峰温降低、放热量增加、表观活化能降低,表现出良好的催化性能。当FOX-12与催化剂以质量比5:1混合时,FOX-12热分解峰温降低了20.3℃,ΔH增加了332 J/g。 相似文献
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对LY12CZ铝合金室温和高温下的单轴循环变形行为及其时间相关特性进行了实验研究,重点讨论了环境温度、应力水平、加载波形和峰值保持对材料棘轮行为的影响。结果表明:室温和高温下,LY12CZ铝合金体现出循环硬化特性,并具有明显的应变幅值依赖性;材料的棘轮行为不仅依赖于当前的平均应力和应力幅值大小,还与加载历史密切相关。尽管LY12CZ铝合金在单调拉伸时对应变率的变化不敏感,但其循环棘轮行为具有明显的时间相关特性:有峰值保持时产生的棘轮应变明显大于没有保持时的值,并随保持时间的增加而增大;正弦波形下的棘轮应变大于三角波形下的棘轮应变。 相似文献
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利用从飞机长桁上截取的LY12CZ材料作出的试件分别在三种腐蚀环境下作了腐蚀实验.实验结果证明在加工时的挤压变形程度、腐蚀液的浓度对LY12CZ的腐蚀都有影响;SO2对LY12CZ的腐蚀现象主要是点蚀. 相似文献
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采用电子束焊接对10mm TA12钛合金进行了焊接,焊缝表面形成良好.对TA12钛合金电子束焊接试样进行了金相分析和静力试验、冲击试验和扫描电镜(SEM)分析.结果表明,焊接接头熔合区、热影响区和母材区的微观组织差别明显;随着等轴α相体积分数的减少,接头塑性和冲击韧性值降低,但是拉伸强度变化不大. 相似文献
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Yingtai Chen Yumin Li Hong Zhang Yi Xie Xuezhong Chen Jinyu Ren Xiaowei Zhang Zijiang Zhu Hongliang Liu Yawei Zhang 《Advances in Space Research (includes Cospar's Information Bulletin, Space Research Today)》2010
The aim of this study was to estimate the acute effects of low dose 12C6+ ions or X-ray radiation on human immune function. The human peripheral blood lymphocytes (HPBL) of seven healthy donors were exposed to 0.05 Gy 12C6+ ions or X-ray radiation and cell responses were measured at 24 h after exposure. The cytotoxic activities of HPBL were determined by 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyl tetrazolium bromide (MTT); the percentages of T and NK cells subsets were detected by flow cytometry; mRNA expression of interleukin (IL)-2, tumor necrosis factor (TNF)-α and interferon (IFN)-γ were examined by real time quantitative RT-PCR (qRT-PCR); and these cytokines protein levels in supernatant of cultured cells were assayed by enzyme-linked immunosorbent assays (ELISA). The results showed that the cytotoxic activity of HPBL, mRNA expression of IL-2, IFN-γ and TNF-α in HPBL and their protein levels in supernatant were significantly increased at 24 h after exposure to 0.05 Gy 12C6+ ions radiation and the effects were stronger than observed for X-ray exposure. However, there was no significant change in the percentage of T and NK cells subsets of HPBL. These results suggested that 0.05 Gy high linear energy transfer (LET) 12C6+ radiation was a more effective approach to host immune enhancement than that of low LET X-ray. We conclude that cytokines production might be used as sensitive indicators of acute response to LDI. 相似文献
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浮空器结构件如吊舱、过渡架及推进支架等多采用金属管材连接。目前,浮空器管材结构连接缺乏使用工况下极限值实测数据,材料及连接方式选择的理论支撑尚有不足。据此,对常用管材的不同连接方式进行比较及断裂分析。研究中铝合金和钛合金管材分别采用螺接及焊接的方式进行连接,测试样品的力学性能并结合仿真分析验证其断裂原因。结果表明:TA1钛合金管材采用焊接连接方式,相对螺接方式连接强度提高 87.9%;6061铝合金管材采用螺接连接方式,相对焊接方式连接强度提高 39.3%。2A12铝合金管材焊接连接强度优于螺接连接强度。同时,分析断裂原因发现,管材形变是影响焊缝连接强度的重要因素;应力集中易发生在管材端部连接处,导致端部焊缝发生断裂;管材形变会使母材断裂时伴有撕裂现象,进一步降低管材的最大连接强度。 相似文献
9.
Demet Cilden-Guler Zerefsan Kaymaz Chingiz Hajiyev 《Advances in Space Research (includes Cospar's Information Bulletin, Space Research Today)》2018,61(1):513-529
In this study, different geomagnetic field models are compared in order to study the errors resulting from the representation of magnetic fields that affect the satellite attitude system. For this purpose, we used magnetometer data from two Low Earth Orbit (LEO) spacecraft and the geomagnetic models IGRF-12 (Thébault et al., 2015) and T89 (Tsyganenko, 1989) models to study the differences between the magnetic field components, strength and the angle between the predicted and observed vector magnetic fields. The comparisons were made during geomagnetically active and quiet days to see the effects of the geomagnetic storms and sub-storms on the predicted and observed magnetic fields and angles. The angles, in turn, are used to estimate the spacecraft attitude and hence, the differences between model and observations as well as between two models become important to determine and reduce the errors associated with the models under different space environment conditions. We show that the models differ from the observations even during the geomagnetically quiet times but the associated errors during the geomagnetically active times increase. We find that the T89 model gives closer predictions to the observations, especially during active times and the errors are smaller compared to the IGRF-12 model. The magnitude of the error in the angle under both environmental conditions was found to be less than 1°. For the first time, the geomagnetic models were used to address the effects of the near Earth space environment on the satellite attitude. 相似文献
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针对某航空发动机在试车过程中多次出现加力筒体尾端局部区域异常变色现象,为了分析其故障原因,利用外观检查、材质分析和温色模拟试验等失效分析方法,确定了故障加力筒体变色部位经历了最高850℃左右的超温。为进一步评价故障加力筒体的可靠性,对其基体材料力学性能及组织演变规律开展研究。在TA12钛合金板材空冷状态下,从加热温度与组织及力学性能的关系分析结果表明:其力学性能随加热温度的升高呈先降低再提高的趋势,在800℃左右达到最低值,且力学性能变化趋势与组织形态演变呈明显的对应关系。根据加力筒体故障部位力学性能及可靠性明显降低的试验结果,判断该加力筒体不再适合继续参与服役试车,建议更换该故障件,并对替换件进行监控。 相似文献