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创新地采用基于螺杆挤出和颗粒喂料的熔融沉积模型制备了致密氮化硅陶瓷。研究了喂料的打印性能、脱脂工艺,以及典型的打印缺陷的存在形式。结果表明,氮化硅颗粒喂料具有优异的打印性能,适合打印无支撑的小倾角、薄壁和复杂曲面的部件。本文研究开发的有机黏结剂体系结合溶剂+热两步脱脂工艺在厚截面部件制备中有突出优势,可以实现9 mm厚度的坯体安全脱脂。研究发现FDM的典型工艺缺陷有层间裂隙和路径间孔隙两种。结合气压烧结,制备了抗弯强度(774.5±70) MPa、密度3.25 g/cm3的致密氮化硅陶瓷,并成功制备了形状复杂和维形良好的氮化硅陶瓷零件。 相似文献
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YANG Yong-zhen ZHANG Chun-yi JI Wei-yun LIU Xu-guang XU Bing-she 《中国航空学报》2006,19(B12):228-231
The deoiled asphalt as the carbon source and the ferrocene as the metal source and the catalyst precursor were chosen to synthesize iron-containing carbon microparticles through co-carbonization at the temperature of about 450℃ for 3 h. The resulting products were treated at 2 000 ℃ for 2 h. All samples were examined by high resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD). The results show that the iron particles in the heat-treated material are completely coated by carbon. In addition to the fully filled carbon microparticles as well as hollow carbon ones, also form carbon fibers with hollow centers. The formation mechanism of the as-prepared products was discussed briefly. 相似文献
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陶瓷材料因其强度高、密度低、耐高温及耐腐蚀等特点在航空航天领域具有广阔的应用前景。针对传统成型方式的局限性,对羟基磷灰石陶瓷材料的光固化3D打印工艺进行了研究。使用微米级羟基磷灰石粉末和光敏树脂,配制出可供3D打印的羟基磷灰石陶瓷浆料,成型出羟基磷灰石陶瓷坯体。根据TG–DSC热分析法,确定了陶瓷坯体的脱脂工艺参数,烧结出羟基磷灰石陶瓷样件。使用SEM扫面电镜观察样件表面形貌,通过X射线衍射分析物相组成,并通过阿基米德排水法测得其致密度,使用万能材料试验仪测量样件的抗弯强度。试验结果证明,利用光固化3D打印技术可以成型出致密度为94.9%,抗弯强度约为41.3MPa的羟基磷灰石陶瓷样件。 相似文献
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