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Al2O3(YAG)/LaPO4层状陶瓷复合材料研究 总被引:2,自引:0,他引:2
选择Al2O3(YAG)作为基体片层材料,LaPO4作为界面层材料,采用凝胶注模成型技术制备出基体层材料的坯片,然后在基体层坯片上采用浸渍或喷涂工艺附着界面层材料,最后将坯片叠置于模具中热压烧结.制备的陶瓷复合材料微观结构均匀,基体片层厚度为110-150μm,界面层厚度为10~30μm,实测层厚比为11.重点研究工艺参数及界面层成分对层状陶瓷复合材料室温性能的影响.结果表明,氧化物基层状陶瓷复合材料的抗弯强度比基体材料略有下降,但室温断裂韧性达到了13.52MPa·m1/2,是基体材料断裂韧性的3倍.对比氧化物基层状陶瓷复合材料与基体材料在断裂过程中裂纹扩展路径的差异. 相似文献
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以Al(NO3)3乙醇溶液为电解液,利用阴极微弧电沉积技术在纯钛表面制备了较厚的氧化铝涂层.分析了涂层的形貌、成分和相组成,测试了涂层的抗高温氧化、电化学腐蚀及抗热震性能,并探讨了阴极微弧沉积氧化铝涂层的机理.涂层由γ-Al2O3和少量的α-Al2O3组成.涂层中含有少量的钛元素,表明涂层/钛界面附近的钛基体在微弧放电作用下也参与氧化铝涂层的沉积和烧结过程.涂层经过100次(700 ℃水淬)热循环后仍与钛基体结合良好.700 ℃恒温氧化结果表明,具有氧化铝涂层的钛氧化速率降低了4倍. 相似文献
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陶瓷超材料吸波器具有耐高温、高强度、可完美吸波的特点,其结构复杂且具有周期性,是一种新兴的吸波器件.但传统成形方式在复杂结构制造上存在一定的局限性.本文提出一种基于光固化增材制造氧化铝陶瓷表面镀铁氧体的方法实现周期性复杂结构的陶瓷超材料吸波器.使用氧化铝粉末和光敏树脂,配制出可供3D打印的氧化铝陶瓷浆料,利用3D打印机... 相似文献
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JING Mao-xianga * SHEN Xiang-qiana ZHOU Jian-xina LI Dong-hongb LI Wang-xingb aSchool of Materials Science Engineering Jiangsu University Zhenjiang China bZhengzhou Research Institute of Chalco Henan Zhengzhou China 《中国航空学报》2006,19(Z1)
Alumina-based composites containing 0-15wt% Ni metallic phase were produced by hot press-sintering Ni-coated alumina pow-ders. The Ni-coated alumina powders were prepared by the aqueous heterogeneous precipitation of alumina micro-powders and nickel sulfate salt followed by reduction process. The microstructural features and dispersion of Ni phase in Ni-coated alumina powders and the subsequent alumina-Ni cermets were investigated using scanning electron microscope (SEM), X-ray diffractometer (XRD), and trans-mission electron microscope (TEM). The relative density of the hot press-sintered composites was measured with the Archimedes’ method while the fracture strength and the fracture toughness were defined with the three-point bending method and the mi-cro-indentation fracture method. In the formation of alumina-Ni cermets from sintered Ni-coated alumina powders, Ni phase to some extent limits the densification rate and stifles the coarsening and growing process of alumina grains. The Ni phase is found to be located at the interfaces and the triple-joint junctions of alumina grains which results into alteration of the fracture mode of alumina and its in-creased fracture strength and fracture toughness if compared with monolithic alumina. 相似文献
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为了确保星载微波电路用高纯氧化铝基板的国产化可靠替代,本文通过全面分析星载产品用高纯氧化铝基板的工艺适用性验证需求,研究建立了星载微波电路用高纯氧化铝基板的工艺适用性验证指标体系,确定了验证试验项目,利用微波电路工艺件试验和组件产品环境适应性考核等试验验证手段,示范性地阐释了陶瓷基板类材料工艺适用性验证方法。研究表明,基于验证需求分析确定验证项目,通过试验与工艺实践获得各类验证数据进行多维度综合评价,可以给出客观完整、科学有效的工艺适用性验证结论。 相似文献
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