A review of long drop tubes as a supplement/alternative to space experiments

The 100 meter high drop tube at the Marshall Space Flight Center has proven to be a viable facility for studies of containerless solidification. Advantages are that experiments are inexpensive and large numbers of specimens can be processed rapidly. It would not be unusual to run ten specimens in a day. Another significant advantage is that the undercooling behavior can be followed with sufficient sensitivity to easily detect the onset of recalescence and subsequent events.Disadvantages are the restrictions on specimen sizes and types of alloys that can be run in a microgravity environment. Practical specimen sizes range between 50 mg and 500 mg depending on the type of furnace being used. Refractory alloys can be processed in a vacuum (about 10^?5 torr) and therefore at microgravity. Non-refractory alloys demand an atmosphere (about 200 torr) to obtain appreciable undercooling before impact at the bottom of the tube. Under these conditions significant g forces result.Because of the present limitations of the 100 meter drop tube, the most definitive work has been done on niobium based alloys. Large amounts of undercooling have been observed routinely and the effects of undercooling on microstructure have been characterized in detail. X-ray diffraction, scanning electron microscopy, and transmission electron microscopy have been used to determine types of phases, amounts of phases, and compositions of phases. It is clear, as would be expected, that the results bear some resemblance to rapid solidification processing by quenching. However, there are dissimilarities due to the uniqueness of solidification by deep undercooling without quenching in long drop tubes and accompanying recalescence effects.     

Undercooling studies on Nb-Pt and Nb-Si alloys using the 105 meter drop tube

Niobium-platinum samples of compositions ranging from 16 to 32 at. % have been undercooled to as much as 540 K in the low gravity, containerless environment of the 105 meter drop tube located at the George C. Marshall Space Flight Center. Undercooling was terminated in the Nb-Pt samples by the nucleation and growth of the Nb₃Pt phase. In the 16–18 at. % Pt samples, this resulted in samples which are completely Nb₃Pt, in contrast to both the equilibrium phase diagram and the non-undercooled samples which formed with Nb dendrites and interdendritic Nb₃Pt. Undercoolings for the Nb-Si samples were up to 670 K, which corresponds to 27% of the liquidus temperature or 80% of the estimated hypercooling limit. In the Nb-Si system, a coupled zone was identified as well as a metastable extension of the solubility limit of Si in Nb due to deep undercooling.     

用分级淬火油来控制工件变形

用分级淬火油来控制工件变形好富顿国际公司Ｒ．Ｊ．ＢＲＥＮＮＡＮ分级淬火油这个名词是１９４２年首先提出来的。它是指将钢件由奥氏体状态放到温度比Ｍｓ略高一点的介质中进行淬火。钢件放在其中的时间恰好使各部分温度平衡，随后放在空气中冷却，从而减少表面和芯部转...