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WANG Jing-ping* LIU Ying HU Min ZHANG Mi-lin College of Materials Science Chemical Engineering Harbin Engineering University Harbin China 《中国航空学报》2006,19(Z1)
Hexagonal-plate BaFe12O19 nano-particles were prepared by combining the co-precipitation and molten-salt method. The effects of molten-salt NaCl on the products have been compared with those of KCl. The X-ray diffraction analysis,the environment scanning electron microscopy and the vibrating sample magnetometer were used to measure their characteristics. The results show that the mol-ten-salt KCl is helpful to obtain pure phase while the molten-salt NaCl will prompt the crystallinity of particles to increase. It is also found that, given the molten-salt of NaCl and that of KCl of the same quantity, the particles formed are also the same size. The size of particles slightly increases as the quantity of the salt increases. Moreover, the sample prepared under 200% NaCl salt system has mag-netization of 71.5 emu/g. 相似文献
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通过合成新型改性剂--(γ-苯乙炔亚胺基)丙基三乙氧基硅烷(PEIPTES)实现对SiO2前驱体的原位改性,制备新型异构聚酰亚胺/SiO2杂化浆料,利用元素分析、FT-IR、热重分析等对PEIPTES的结构和性能以及新型杂化浆料的结构进行表征与分析.结果表明,杂化浆料中有机相与无机相之间形成化学键.利用该杂化浆料对碳纤维表面进行改性.AFM分析表明,改性后碳纤维表面覆盖一层有纳米级颗粒状突起的物质,增加表面粗糙度,有利于改善复合材料界面性能.复合材料力学性能研究表明,杂化浆料可提高碳纤维/异构聚酰亚胺复合材料的层间剪切强度,当SiO2含量为5wt%时层间剪切强度达到最大值,此时冲击性能和界面耐热性能均有显著提高. 相似文献
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