己二酸酯类增塑剂向橄榄油中迁移量的测定方法

采用精馏橄榄油为模拟物,对PVC食品接触材料中四种己二酸酯类增塑剂向脂类食品模拟物的迁移量进行了检测,并对萃取条件和萃取试剂进行了优化,采用GC—MS技术,通过外标法进行迁移量的检测。研究表明,此方法具有方法简便,重现性好,灵敏度高,定性、定量准确可靠的特点,最低检测限可达5mg／kg,回收率为83．20％～106．13％,标准偏差为1．60％～3．34％,可实际应用于PVC食品接触材料己二酸酯类增塑剂迁移量的检测。     

Fundamentals of Design and Technology of Rolling Element Bearings

This article presents an overview of fundamentals of rolling element bearing designs and technologies. The aim is to outline the complex interrelation of all fundamentals with the rolling contact fatigue and the attainable bearing life. Such fundamentals include, amongst others, bearing stressing and life capability. The article shows the different types of rolling bearing stressing and the analysis of the stress distribution (principal stresses and equivalent stresses) in the material under the rolling contact area. It becomes obvious that the contamination of the bearing with foreign particles leads to a drastic reduction in bearing life. Furthermore, it demonstrates the impact of the bearing lubrication and coating as well as the effect of additives on the attainable life and wear. Further fundamentals of rolling element bearing design are the materials, the material cleanliness and the heat treatment. The article reveals the importance of the cleanliness of bearing steels as well as different types of inclusions and their effect on rolling contact fatigue. Additionally the article describes how to optimize the material properties (strength, toughness and residual stress) by the heat treatment processes. The outcome of these investigations is that endurance life of a rolling element bearing can be achieved if specific operating conditions, an adequate lubrication, good system cleanliness and specific bearing stressing are met. The article provides a guideline for bearing engineers on how designs and technologies can be applied to optimizing a bearing for a particular industry or aerospace application.     

航材管理中的成本控制与保障率组合研究

从系统角度考察航材成本与保障率的关系，研究影响保障率的动因，并将各种因素同成本对应起来，旨在实现以最合适的成本保证公司运营效率最大化的目标，以及从需求出发制定确实有效的成本改进方法。     

航天钐钴永磁直流电动机

阐述了导弹用高功率／重量比直流电动机的电磁设计和结构设计。电磁设计的重点在于电磁参数的确定和分级优化确定转子及磁钢的尺寸；结构设计的重点在于磁钢的固定和绕组端部的固定，经样机和小批生产均取得极为满意的结果。     

用微分法推导拉压静不定变形谐调方程

材料力学中，解决桥架拉压静不定问题时，推导变形谐调方程是其关键，以往都是用图解法近似导出变形谐调方程，本文作者提出用微分法导出普遍适用的变形谐调方程：△ｌ１＋△ｌ２＝２△３ｃｏｓα。     

PIP 法制备SiBN 纤维增强氮化物陶瓷基复合材料Ⅰ———纤维和先驱体性能分析

利用先驱体聚合物浸渍-裂解(PIP)技术制备SiBN纤维增强氮化物陶瓷基复合材料,对SiBN纤维、聚硅硼氮烷有机先驱体裂解以及SiBN纤维增强氮化物陶瓷基复合材料性能进行了分析。研究表明:聚硅硼氮烷先驱体在氨气气氛下裂解得到的陶瓷产物碳含量较低,其裂解产物介电常数在3.0左右,介电损耗小于0.01;SiBN纤维中C和O元素含量均较高,碳的存在对材料介电性能影响明显;制备的氮化物陶瓷基复合材料弯曲强度为88.52 MPa,弹性模量为20.03 GPa。     

石墨烯基吸波材料研究新进展

吸波材料的性能是影响雷达隐身的关键因素,其研究对军用和民用都具有非常重要的意义。石墨烯由于其独特的吸波性能,成为吸波材料研究的一大热点。本文综述了石墨烯/铁氧体、石墨烯/金属微粉、石墨烯/磁性金属、石墨烯/导电聚合物和石墨烯/磁性材料/导电聚合物等复合吸波材料在吸波领域的最新研究应用现状,并展望了吸波材料未来发展趋势。     

SiC尺寸和含量对MB2/SiC复合材料超塑性的影响

在应变速率为 2 .0 8× 10 - 3 s- 1 ～ 5 .2 1× 10 - 1 s- 1 的范围内 ,测试了四种镁基复合材料的超塑性。结果表明 ,颗粒百分含量增加 ,复合材料的延伸率和应变速率敏感性指数增加 ,颗粒尺寸增大则导致复合材料超塑性能的下降。     

Synthesis of Iron-containing Carbon Microparticles from Deoiled Asphalt and Ferrocene

The deoiled asphalt as the carbon source and the ferrocene as the metal source and the catalyst precursor were chosen to synthesize iron-containing carbon microparticles through co-carbonization at the temperature of about 450℃ for 3 h. The resulting products were treated at 2 000 ℃ for 2 h. All samples were examined by high resolution transmission electron microscopy （HRTEM） and X-ray diffraction （XRD）. The results show that the iron particles in the heat-treated material are completely coated by carbon. In addition to the fully filled carbon microparticles as well as hollow carbon ones, also form carbon fibers with hollow centers. The formation mechanism of the as-prepared products was discussed briefly.     

Mission STS-134: Results of Shape Memory Foam Experiment

Shape memory epoxy foams were used for an experiment aboard the International Space Station (ISS) to evaluate the feasibility of their use for building light actuators and expandable/deployable structures. The experiment named I-FOAM was performed by an autonomous device contained in the BIOKON container (by Kayser Italia) which was in turn composed of control and heating system, battery pack and data acquisition system. To simulate the actuation of simple devices in micro-gravity conditions, three different configurations (compression, bending and torsion) were chosen during the memory step of the foams so as to produce their recovery on ISS. Micro-gravity does not affect the ability of the foams to recover their shape but it poses limits for the heating system design because of the difference in heat transfer on Earth and in orbit. A recovery about 70% was measured at a temperature of 110 °C for the bending and torsion configuration whereas poor recovery was observed for the compression case. Thanks to these results, a new experiment has been developed for a future mission by the same device: for the first time a shape memory composite will be recovered, and the actuation load during time will be measured during the recovery of an epoxy foam sample.