Comparative Study on Super Fine Mesophase Powder and MCMB Used to Manufacture High-Density Isotropic Carbon Bulks

Mesocarbon microbeads (MCMB) and super fine mesophase powder (SFMP) were prepared firstly from a coal tar pitch and then hot-condensed into high-density isotropic carbon (HDIC) bulks under 160 MPa and finally sintered at 1 000 ℃ . By analyzing the ther-mogravimetric behavior of the MCMB and SFMP powders, their volume shrinkage and weight loss during sintering and the bulk density and flexural strengths of their sintered bulks, it was found that the smaller sizes and the richer β-resin contents of SFMP have facilitated formation of sintered bulks with more compact isotropic structure and higher flexural strengths than MCMB. Because of the filling and bonding effects of SFMP on MCMB bulks, addition of SFMP, albeit a little, can greatly increase the flexural strengths of sintered bulks of MCMB. However, adding MCMB, even a slight amount, into SFMP can severely impair the flexural strength of sintered bulks. This might be attributed to both the crack initiation along the boundaries between MCMB and SFMP and the formation of layered texture of MCMB sphere.     

Preparation and Mechanical Properties of Glass Coats with High Temperature Radar Absorber

BaO-La2O3-B2O3 （BLB） glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the absorbing coat because it is considered to be a good high temperature absorber. The effect of the coating temperature and coating time on the tensile strength of the glass coat was investigated and the proper coating parameters to get good mechanical properties were determined. In addition, the effects of the SiCN content on the tensile strength of the absorbing coat were also discussed. Results show that it is possible to prepare the glass coat using the BLB glass as a binder. That the coat formed at 730℃ for 30 min has the best tensile strength witnesses 730 ℃, 30 min to be the proper parameter to prepare the glass coat. The BLB glass coat without SiCN powder possesses good tensile strength and the introduction of the SiCN absorber into the glass coat will lower the tensile strength. As the SiCN content increases, the tensile strength of the absorbing coat decreases, which could be attributed to the aggregation of SiCN in the coats.     

橡胶软油箱材料对铝合金腐蚀的影响研究

选择橡胶软油箱外层的橡胶材料及防老化涂层材料与7A04 T6包铝及去包铝、7B04 T6包铝及去包铝合金进行接触腐蚀试验。试验结果表明软油箱中对铝合金腐蚀产生直接影响的非金属材料为橡胶防老化涂层,并确定了四种橡胶防老化涂层材料的腐蚀敏感性顺序;通过对橡胶防老化涂层进行的EDS分析以及涂层浸泡液的pH值变化及氯离子含量研究,认为橡胶防老化涂层中对铝合金腐蚀产生影响的主要成分为氯离子和金属氧化物。     

粉末粒度对快速凝固／粉末冶金Al-Fe-Mo-Si／Zn-Al复合材料组织与性能的影响

研究不同粉末粒度Al-9.0?-1.8%Mo-1.7%Si/5%(Zn-30%Al)金属/金属复合材料的组织、拉伸性能和阻尼性能.快速凝固粉末由气体雾化制备,选取平均粒度d50分别为27.3,36.2,41.6μm粉末装入包套,经除气,再热挤压制成棒材.结果表明,粉末粒径越粗,强化相越粗大,呈团聚体存在,且有偏聚现象,材料的强度明显下降,室温下粉末较细材料的阻尼性能较好,高于100℃时粉末粒度较粗材料的阻尼性能好.     

2D12铝合金腐蚀性能研究

对不同规格2D12铝合金进行晶间腐蚀、剥蚀和应力腐蚀性能测定.研究表明,2D12铝合金自然时效(T4)状态具有晶间腐蚀和剥落腐蚀倾向,2D12铝合金S-L方向比S-T方向的抗应力腐蚀的性能低,应力腐蚀开裂门槛应力强度因子分别为22.6和27.1 MPa·m1/2,这与C环应力腐蚀结果一致,断口呈现典型的沿晶断裂特征.     

LY12铝合金的拉扭复合加载疲劳

对LY12铝合金的拉扭复合加载疲劳性能进行了研究,并用扫描电镜对疲劳试样的断口进行了观察.试验选用单轴轴向、0°同相拉扭复合、45°非同相拉扭复合、90°非同相拉扭复合和纯扭转五种加载路径,并使试样在不同加载路径下的最大等效应变值相等.结果表明,LY12铝合金试样在五种加载条件下,均出现循环硬化和饱和现象.LY12铝合金试样在纯扭转加载时的寿命最长,在90°非同相拉扭复合加载时的寿命最短.用Wang-Brown模型的损伤参量,可以较好解释不同加载条件的疲劳寿命差异.单轴轴向加载和0°同相拉扭复合加载试样的断口均出现疲劳条纹,纯扭转加载和90°非同相拉扭复合加载断口形貌以裂纹面间相互摩擦的痕迹为主.     

波导器件铝合金双十字轴整体铸造工艺研究

在严格控制型芯尺寸精度、表面粗糙度的条件下,采用普通砂型铸造的方法来制造铝合金双十字轴这类铝合金波导器件是可行的。     

TC4钛合金和7475铝合金的长裂纹和小裂纹扩展特性的研究

研究了TC4钛合金和7475铝合金在应力比R=0.5,0和-1恒幅载荷下的长裂纹和小裂纹的扩展行为。小裂纹试验采用单边缺口拉伸试样,裂纹从半圆形缺口根部自然萌生。研究结果显示,TC4钛合金在恒幅载荷下,未显示出小裂纹效应。该现象与小裂纹扩展初期出现明显的裂纹偏析和分叉有关。小裂纹起始寿命较长,裂纹起始寿命约占疲劳寿命的20%~55%。7475-T7351铝合金在低应力比(R≤0)下的低应力强度因子范围内,存在经典的小裂纹效应,小裂纹起始于孔壁表面的第二相质点团或空洞处,夹杂质点团较之单个杂质点对裂纹的萌生更有害,裂纹起始寿命约占疲劳寿命的15%~29%。     

粉末合金(FGH95)蠕变/疲劳交互作用下寿命预测的损伤力学有限元分析

采用基于损伤力学的蠕变—疲劳交互作用下的寿命预测模型,应用损伤等效应力进行三维应力状态下的损伤计算,并考虑了压缩时闭合效应,利用ANSYS的二次开发工具APDL和UPFs开发程序,把基于损伤力学的寿命预测方法与ANSYS的结构分析结合起来,实现了对构件的损伤计算和寿命预测。针对粉末合金材料易含夹杂等初始缺陷的特点,提出了在寿命计算中通过单元初始损伤模拟初始缺陷对寿命影响的处理方法,探讨了考虑初始缺陷条件下的寿命预测,并利用试验对计算结果进行了对比验证。      

时效和调压浇注对ZL101A-T6合金性能的影响

实验比较了重力铸造和调压铸造对ZL101A-T6铝合金的力学性能的影响。结果表明,在相同的熔铸工艺和热处理条件下,调压铸造试样的强度,特别是延伸率得到大幅度提高。