不同频率及相转移催化剂条件下的安息香缩合反应

本文介绍了在不同频率超声波及不同相转移催化剂条件下对安息香缩合反应的影响,实验发现,超声波的频率对安息香的收率有一定程度的影响,收率随着超声波频率的增加而增加。在选择的三种相转移催化剂中,采用苄基三乙基溴化铵效果最好,安息香的收率最高。     

A closed-form solution for moving source localization using LBI changing rate of phase difference only

Due to the deficiencies in the conventional multiple-receiver localization systems based on direction of arrival(DOA) such as system complexity of interferometer or array and amplitude/phase unbalance between multiple receiving channels and constraint on antenna configuration,a new radiated source localization method using the changing rate of phase difference(CRPD)measured by a long baseline interferometer(LBI) only is studied. To solve the strictly nonlinear problem, a two-stage closed-form solution is proposed. In the first stage, the DOA and its changing rate are estimated from the CRPD of each observer by the pseudolinear least square(PLS) method,and then in the second stage, the source position and velocity are found by another PLS minimization. The bias of the algorithm caused by the correlation between the measurement matrix and the noise in the second stage is analyzed. To reduce this bias, an instrumental variable(IV) method is derived. A weighted IV estimator is given in order to reduce the estimation variance. The proposed method does not need any initial guess and the computation is small. The Cramer–Rao lower bound(CRLB) and mean square error(MSE) are also analyzed. Simulation results show that the proposed method can be close to the CRLB with moderate Gaussian measurement noise.     

含噪信号经验模式分解虚假分量识别方法

针对含噪信号Hilbert-Huang变换存在虚假分量,提出改进的奇异值分解(SVD)方法进行降噪,改进包含两个部分:一是利用重构相空间代替传统矩阵如Hankel矩阵,以去掉信号冗余,再者提出奇异值能量熵分量差分法,更易于定出重构奇异值阶次;二是提出了频谱比值法对虚假分量进行辨识,更有效辨识出虚假分量.首先利用经验模式分解(EMD)得到本征模式分量(IMF),识别并剔除趋势项,重构信号,然后进行SVD,重构降噪后的信号,消除虚假分量,最后进行时频分析.联合方法应用于含噪仿真信号,信噪比(signal noise ratio,SNR)提高了5.5%,虚假分量辨识率提高至100%,用于双跨转子故障振动信号,得到正确的时频结果,表明了所提方法识别含噪信号虚假分量的有效性.     

交会对接寻的段水平双脉冲交会轨道精确求解

基于考虑摄动影响的精确轨道动力学模型,对交会对接寻的段水平双脉冲交会轨道的精确求解方法进行了研究。提出了将控制脉冲的俯仰角近似转化为控制时刻的轨道幅角,从而调整脉冲控制时刻以消除径向速度增量的方法,精确求解首末水平双脉冲的启控时刻;引入导引终点位置偏差的比例控制方法,精确求解水平双脉冲的精确控制量。仿真结果表明,2轮整体迭代可获得首末水平脉冲控制时刻和控制量的精确值,脉冲水平特性达到俯仰角小于1°,导引终点相对位置精度达到10m,验证了该方法的正确性。     

Assessing the feasibility of involving gaseous products resulting from physicochemical oxidation of human liquid and solid wastes in the cycling of a bio-technical life support system

The study addresses the possible ways of involving gaseous products produced by “wet” incineration of human wastes mixed with H₂O₂ in an alternating electric field in the cycling of the physical model of a bio-technical life support system (BTLSS). The resulting gas mixture contains CO₂ and O₂, which are easily involved in the cycling in the closed ecosystem, and NH₃, which is unacceptable in the atmosphere of the BTLSS. NH₃ fixation has been proposed, which is followed by nitrification and involvement of the resulting products in the mass exchange of the closed system. Experiments have been performed to show that plants can be grown in the atmosphere resulting from the closing of the gas loop that includes a physicochemical installation and a growth chamber with plants representing the phototrophic compartment of the BTLSS. The results of the study suggest the conclusion that the proposed method of organic waste oxidation can be a useful tool in creating a physical model of a closed-loop integrated BTLSS.     

α、β相分布形态对TC11钛合金高温循环蠕变速率的影响

对TC1 1钛合金施行了不同的热处理制度 ,得到 3种组织形态 ,研究了不同的组织形态的高温循环蠕变。结果表明 ,晶间 β组织具有低的循环蠕变速率 ,而随最大应力的增加 ,蠕变速率增加快 ;而等轴组织和片状组织循环蠕变速率较高 ,但随应力的增加 ,蠕变速率增加较慢。分析认为 ,晶界滑移行为对高温循环蠕变有重要影响     

进场着陆飞行品质的地面试验研究

针对电传控制增稳飞机进行了进场着陆的飞行品质地面模拟试验研究，验证了适合于进场着陆的控制律，并得出一些重要的有关进场着陆的驾驶员评定意见。此外，还计算了轨迹角超调值，验证了该参数数可以作为一个重要的飞行品质准则。     

现代飞机驾驶员诱发振荡机理和预测研究

在说明驾驶员诱发振荡的定义，简单介绍了现代飞机的ＰＩＯ类型之后，详细分析了影响ＰＩＯ的各种因素（如飞机的动态特性、操纵面伺服器，座舱操纵感觉系统，驾驶员及诱发因素等）；为了探讨驾驶员操纵行为对ＰＩＯ的影响，采用优化控制理论，建立等效驾驶员操纵动态模型；研究飞行品质与ＰＩＯ的关系，建立相应的预测ＰＩＯ的准则。     

用低纯原料制备电冰箱起动器PTCR的重要途经——热敏钛酸钡陶瓷第二相结晶

根据Al_2O_3-SiO_2系统相图,调整Al_2O_3,SiO_2添加剂比例,可在热敏钛酸钡陶瓷显微结构中形成莫来石结晶相,莫来石的形成改善了用国产低纯原料制备电冰箱起动器PTCR的性能。本文就莫来石第二相与PTCR性能关系进行了讨论。     

模拟JJ—7飞机纵向摆动试飞研究

本文论述了BW-1变稳机空中飞行模拟H-7飞机发生两次纵向摆动时飞行状态特性,通过试飞研究其飞行品质,校核驾驶员诱发振荡(PIO)发生的可能性;并对解决PIO的方案进行了验证试飞研究,提出了排除PIO较适宜的参数值.试飞证明,空中飞行模拟试验是研究PIO的有效方法之一.