基于Deform软件二次开发和BP神经网络的TA15多向锻造微观组织预报

通过热压缩实验构建了TA15合金的热变形真应力-应变曲线,以此为基础分别建立了合金双相区及单相区温度区间的热变形本构方程;基于热压缩试样动态再结晶的统计数据建立了TA15合金的动态再结晶模型。借助Deform提供的二次开发功能实现相关数学模型的程序化,制定正交实验方案,实现了TA15合金多向锻造变形的微观组织仿真。通过正交实验分析得出各项因子的影响对象及强弱差异,提出了双相区及单相区温度区间内的多向锻造最佳因子组合。建立了TA15合金多向锻造变形微观组织的BP （Back Propagation）神经网络预测模型,将预测结果与有限元仿真结果进行比较,结果表明两种方法的预测结果基本一致,但神经网络具备有限元仿真难以实现的良好细节预测能力,能更为细致地实现对微观组织分布状态的划分。     

厚度和环境对复合涂层导电性能的影响

为了给数字化刻铣曲面频率选择表面(FSS)结构的制作和加工提供参考和依据,对比研究了含片状银粉颗粒的聚氨酯基和环氧树脂基2种复合导电涂层的基本性能,并通过环境加速试验,重点研究了温度、湿度以及腐蚀气氛对2种导电涂层的界面强度、微观结构和导电性能的影响.通过电桥法测量涂层表面电阻的变化,并通过扫描电境观察环境试验前后,涂层表面和剖面的微观结构和形貌变化.试验结果表明:聚氨酯基涂层的综合性能优于环氧树脂基涂层;在实验所涉及的参数变化范围内,环境因素对2种涂层与基体的界面结合影响不大,但对其导电性能的影响比较明显.环境因素对导电性能的削弱作用,源于相应过程中导电涂层的微观结构损伤.     

Effect of Semi-solid Isothermal Heat Treatment on Microstructure of VW63Z Alloy

The effects of isothermal heat treatment on the semi-solid microstructure evolution of VW63Z (Mg-6Gd-3Y-0.4Zr, wt.%) alloy are studied. It shows that the microstructure of VW63Z alloy could transform from equiaxed crystal to semi-solid spherical crystal after isothermal heat treatment above 620 ºC. With the heating temperature elevating from 620 ºC to 635 ºC and the holding time prolonging from 10 min to 35 min, the liquid fraction increases gradually. The semi-solid microstructure evolution of VW63Z alloy can be divided into three stages, i.e., particle coarsening and spheroidization;particle necking, coalescence, and Ostwald ripening;and dynamic equilibrium. The semi-solid process window of VW63Z alloy ranges from 620 ºC to 635 ºC, where the best process parameters are holding at 635 ºC for 20 min?30 min. The solid fraction, the average particle size, and the shape factor are 41.1%?53.8%, 81.5 μm?83.2 μm, and 0.70?0.75, respectively. The maximum relative deviations of the solid fraction, the particle size, and the shape factor at different heights of the same billet are 44.6%, 17.4%, and 16.6%, respectively, which means that it should pay attention to the uniformity of edge and core of VW63Z alloy during isothermal heat treatment. The driving force of microstructure is supposed to be the reduction of solid-liquid interface free energy.     

Investigation of vertical profile of rain microstructure at Ahmedabad in Indian tropical region

The microstructure of rain has been studied with observations using a vertical looking Micro Rain Radar (MRR) at Ahmedabad (23.06°N, 72.62°E), a tropical location in the Indian region. The rain height, derived from the bright band signature of melting layer of radar reflectivity profile, is found to be variable between the heights 4600 m and 5200 m. The change in the nature of rain, classified on the basis of radar reflectivity, is also observed through the MRR. It has been found that there are three types of rain, namely, convective, mixed and stratiform rain, prevailing with different vertical rain microstructures, such as, Drop Size Distribution (DSD), mean drop size, rain rate, liquid water content and average fall speed of the drops at different heights. It is observed that the vertical DSD profile is more inhomogeneous for mixed and stratiform type rain than for convective type rain. It is also found that the large number of drops of size <0.5 mm is present in convective rain whereas in stratiform rain, drops concentration is appreciable up to 1 mm. A comparison of measurements taken by ground based Disdrometer and that from the 200 m level obtained from MRR shows good agreement for rain rate and DSD at smaller rain rate values. The results may be useful for understanding rain structures over this region.     

纳米TiC粉末改性钎料钎焊CBN磨粒的结合界面和磨损特性

采用了Ag-Cu-Ti 合金和纳米 TiC 粉末组成的新型复合钎料钎焊立方氮化硼(CBN)磨粒和工具基体,运用了三维体式显微镜和扫描电镜,研究了CBN磨粒与改性钎料之间的结合体系,包括界面微结构和反应产物,并进行了钎焊磨粒耐磨性试验.试验结果表明:加入的纳米TiC粉末均匀分布在钎料层内,细化了Ag-Cu-Ti合金钎料层的显微组织,有效控制了CBN磨粒与钎料的剧烈反应;磨粒表面化合物均匀致密,确保了CBN磨粒、纳米改性钎料和基体之间的结合强度;钎焊CBN磨粒的磨损形式以磨耗磨损为主,后期出现微小破碎,无磨粒脱落.     

Ti-6Al-4V钛合金激光弯曲成形微观组织研究

以1mm厚Ti-6Al-4V合金薄板为对象,运用光学金相显微镜、电子探针、扫描电子显微镜、氮氢氧联合分析仪、显微维氏硬度计,研究了特定累积线能量下90°弯曲角弯折区显微组织。结果表明,弯折区组织与累积线能量输入有关,当累积线能量在适当范围时,材料堆积增厚,极表层出现轻微复熔铸态组织,上层为板条马氏体α′,中层为针状马氏体α′,底层为长大粗化的(α+β)组织;距表层约0.2mm范围吸收间隙元素强烈致使硬度急剧提高并呈明显梯度;累积线能量输入过大,弯折区出现大面积复熔铸态组织并伴有裂纹产生。     

新型Co基合金Co-9Al-(9-x) W-xMo-2Ta-0.02B的显微组织与高低温力学性能

以新型Co基合金Co-9Al-9W-2Ta-0.02B成分为基础,分别添加了原子分数为2％、4％、6％、9％的Mo元素替代W（分别称2Mo、4Mo、6Mo、9Mo合金,W+Mo的原子分数为9％,无Mo添加的称为0Mo合金）,研究了Mo元素对合金相组成、显微组织形貌、维氏硬度和高低温压缩强度的影响.结果表明铸态合金由Co...     

Ag和稀土Y复合添加对金属间化合物NiAl显微组织的影响

研究了Ag和Y的复合添加对金属间化合物NiAI显微组织的影响。利用非自耗电弧炉制备了三种不同Y和Ag含量（1．0,5．0,10．0质量分数％）的NiAJ合金,其中一组试样进行了高温固溶和时效处理。实验结果表明,随着Y和Ag含量的增加,铸态下的NiAI合金晶粒呈逐渐细化的趋势,并且柱状晶生长方式逐渐演变为典型的糊状凝固方式。EDS和XRD分析表明,晶界处有富Ag、Y相形成;固溶时效后的NiAl合金组织则演变为粗大的等轴晶粒,Y和Ag元素仍然在晶界处偏聚。     

IC10高温合金的微观组织

研究了IC10高温合金的微观组织。研究表明:铸态组织包括γ′和γ,′以及γ γ′共晶相和MC碳化物,其中γ′体积百分数为64%,碳化物相主要是TaC和H fC,碳化物呈骨架状和点状、块状分布,共晶相多为葵花状。热处理后有残留的γ γ′共晶相,碳化物分解并有γ′包覆,γ′相发生球化,晶界上MC分解,并有H fC析出。IC10合金经950℃,3000h长期时效后组织保持稳定,未析出有害的TCP相;长期时效的组织变化表现为γ′的长大和条状化;枝晶间二次析出细小的富H f的MC相;晶界上析出少量的M6C和M23C6。     

Phase Transformation and Microstructure of Ti50Ni48-xFe2Ndx Shape Memory Alloys

The influences of rare earth element Nd on the phase transformation and the microstructure of Ti₅₀Ni_48−xFe₂Nd_x shape memory alloys are investigated by means of electrical resistivity, optical microscopy, electron probe microanalyzer, and X-ray diffraction. The results show that TiNiFe alloys with different Nd contents exhibit two-step martensitic transformation. The start temperature of martensitic transformation increases sharply from 212 K to 267 K when 0.1 at.% Nd is added in, and then decreases gradually if Nd content further increases. The microstructure of TiNiFeNd quaternary alloys consists of TiNi matrix, Ti₂Ni second phase, and Nd₃Ni intermetallic compound. The spherical Nd₃Ni precipitate-particles evenly disperse in the matrix.