发动机镀镉螺栓连接件的失效分析

对一种固体发动机安全机构上的螺栓连接失效件断口进行了扫描电子显微镜、金相组织、化学成分和Ｘ射线微区元素分析。基本朝该螺栓件失效断裂原因，由于钢制螺镀之后，低熔点金属镉从螺纹根部缺陷处渗入到基体内部引起晶界脆化，在应力的作用睛导致螺栓件失效断裂。     

Effect of nickel introduced by electroplating on pyrocarbon deposition of carbon-fiber preforms

In order to improve the deposition rate and microstructure of pyrocarbon, nickel was introduced by electroplating on carbon fibers and used as a catalyst during the deposition of pyrocarbon at 1000 C using methane as a precursor gas. The distribution of nickel catalyst and the microstructure of pyrocarbon were characterized by scanning electron microscopy（SEM）, energy dispersive spectroscopy（EDS）, X-ray diffraction（XRD）, and Raman micro-spectrometry. Results show that nano-sized nickel particles could be well distributed on carbon fibers and the pyrocarbon deposited catalytically had a smaller d002 value and a higher graphitization degree compared with that without catalyst. In addition, the deposition rate of pyrocarbon in each hour was measured.The deposition rate of pyrocarbon in the first hour was more than 10 times when carbon cloth substrates were doped with nickel catalysts as compared to the pure carbon cloths. The pyrocarbon gained by rapid deposition may include two parts, which are generation directly on the nickel catalyst and formation with the carbon nanofibers as crystal nucleus.     

大功率柴油机排气阀机器人焊接系统及工艺

为了提高船舶焊接质量,采用机器人柔性化焊接系统堆焊镍合金阀盘。设计了高效、高质量的机器人焊接系统,对SNCrW不锈钢进行了焊接工艺研究,并对样件进行了检验分析。经检验,不存在超过0.06mm的缺陷,完全符合阀盘质量检测标准,属于合格产品,完成了国内首个高质量镍基堆焊阀盘的焊接。     

SiCp增强体表面改性对铁基复合材料组织性能的影响

为了改善粉末冶金方法制得的SiCp/Fe复合材料性能，采用化学镀的方法，成功地在SiCp表面沉积镍，考察了颗粒表面改性对铁基复合材料组织性能的影响。结果表明，镀镍层的作用明显：第一，阻碍了SiCp/Fe界面的过度反应以及Si原子向基体中的扩散；第二，镀镍层的存在改善了颗粒与基体的界面状况，使得颗粒能够更好地发挥增强体的作用。     

掺氮TiO2光学薄膜的吸光特性研究

TiO2在光催化方面具有较好的应用前景,可望用于有害污染物的降解处理;但由于其禁带宽度对应的激发波长在紫外区,限制了其大规模应用。文章利用操作简便、易于控制的真空阴极电弧离子镀膜技术,制备了非掺氮和掺氮的TiO2薄膜。并分别在300℃和500℃退火后,获得了非晶态向锐钛矿结晶的转变。结果还表明,掺氮TiO2薄膜的相变温度比非掺氮的TiO2薄膜要高,其光吸收区也从紫外区扩展到了可见光区。     

Re/ Ir 高温抗氧化性能

采用电弧离子镀技术在Re 金属表面制备Ir 涂层,研究沉积态Ir 涂层的微观形貌、成分和相结构
以及在不同温度区域的高温抗氧化性能。通过分析表明,利用电弧离子镀方法,可以在Re 金属基体表面制备
出连续、致密和均匀的Ir 涂层。Re/ Ir 试样的抗氧化寿命,1 800℃可达到4 h;2 000℃可达到2 h。在1 950℃
条件下,进行120 次热震试验,试验后Ir 涂层表面光滑致密,表面没有发现任何剥离现象。     

化学镀Ni-P合金涂层及其耐磨性

 对化学镀 Ni- P的硬度和耐磨性的关系进行了研究。低温长时加热可以获得高硬度 ,继续保温后其值不变。高温加热硬度达最大硬度以后保温硬度降低。不同温度处理其最大值相同 ,但耐磨性不同 ,高温处理优于低温处理。光电子能谱分析表明镀层表面富磷     

碳纳米管表面修饰的研究进展

回顾了碳纳米管表面修饰的理论与实验方法,详细介绍了碳纳米管表面修饰的新方法和最新研究进展,并对碳纳米管表面修饰技术给出了简要评价。     

柔性热敏薄膜传感器阵列工艺研究

分析了热敏薄膜传感器测量流场温度和壁面剪应力的原理,选择聚酰亚胺为衬底材料,金属镍为热敏材料,提出了一种电镀引线的柔性热敏薄膜传感器阵列结构及其制作工艺.经热敏性能测试,该柔性热敏薄膜传感器阵列结构简单,可贴附于高曲率复杂表面,实现非破坏动态流场参数测量.     

Studies of Electromagnetic Properties of MWCNTs after Electroless Plating with Co-Fe Alloy

A method of electroless plating is utilized to deposit Co-Fe alloy on the surface of multi-walled carbon nanotubes (MWCNTs), and electromagnetic parameters of MWCNTs with and without electroless plating are discussed. The MWCNTs covered by Co-Fe is a desirable light absorbent in wide wave band by utilizing electroless plating process in experiments. Field-emission scanning electron microscope (FESEM) and field-emission transmission electron microscope (FETEM) images as well as energy dispersive spectroscopy (EDS) results are presented to show the morphology, components and electromagnetic parameters of MWCNTs. Electromagnetic properties of MWCNTs are enhanced after electroless plating observed from contrast of results between MWCNTs with and without plating. In conclusion, the covering Co-Fe on the surface of MWCNTs in 2-18 GHz frequency range has better electromagnetic properties. When the material is in the 6.5 GHz electromagnetic waves, the reflection loss is up to ?10 dB, and the bandwidth more than ?4 dB is 5 GHz. The excellent electromagnetic properties make it probable for MWCNTs to be utilized as absorbent in electromagnetic shielding materials.