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541.
542.
研究了N-(5-硝基-6-氯-3-吡啶甲基)邻苯二甲酰亚胺的合成方法。该法先在室温条件下以邻苯二甲酰亚胺与氢氧化钾反应合成了邻苯二甲酰亚胺钾。然后在70°C条件下,以邻苯二甲酰亚胺钾作为亲核试剂,与2-氯-5-氯甲基吡啶发生缩合反应,制备了N-(6-氯-3-吡啶甲基)邻苯二甲酰亚胺。缩合产物再经过硝化,合成N-(5-硝基-6-氯-3-吡啶甲基)邻苯二甲酰亚胺,其熔点为143.1~143.8°C,收率为90.5%。用红外光谱(IR)、核磁共振氢谱(1HNM R)、气谱-质谱(GC-M S)解析以确定中间体和产物的结构;用高效液相色谱测定合成产物的含量。实验结果表明合成了具有较高含量和较高收率的产品。 相似文献
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544.
Ti-15V-3Cr-3Sn-3Al合金是一种在航空航天工业领域具有广泛应用前景的亚稳定β型钛合金。本文用恒应变速率法进行实验,测试Ti-15-3板材的超塑性,为超塑成形提供参考依据。 相似文献
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546.
在边坡、城市峡谷、高架等复杂的公路交通定位环境中,存在海量多样的定位需求与复杂的定位环境,北斗信号穿越建筑空间时强度被削弱,产生严重的信号反射和衍射,使得北斗卫星信号难以到达和有效使用,系统可用率下降,无法提供可靠的定位服务。结合第五代移动通信网络(5G)系统高密度部署的特点,提出了一种北斗+5G联合定位模型以及基于最小二乘残差Helmert后验加权的误差校正方法。在复杂公路交通环境中,可以改善可见卫星数少的问题,优化卫星的几何构型,提高用户终端定位精度,能够为用户终端提供高精度、全天候、连续、实时的定位服务。实验表明,北斗+5G联合定位模型能够大幅提升复杂公路交通环境下的定位性能。 相似文献
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548.
N.C. Patel S.P. Karia K.N. Pathak 《Advances in Space Research (includes Cospar's Information Bulletin, Space Research Today)》2019,63(6):1860-1881
This paper investigated the performance of the latest International Reference Ionosphere model (IRI-2016) over that of IRI-2012 in predicting total electron content (TEC) at three different stations in the Indian region. The data used were Global Positioning System (GPS) data collected during the ascending phase of solar cycle 24 over three low-latitude stations in India namely; Bangalore (13.02°N Geographic latitude, 77.57°E Geographic longitude), Hyderabad (17.25°N Geographic latitude, 78.30°E Geographic longitude) and Surat (21.16°N Geographic latitude, 72.78°E Geographic longitude). Monthly, the seasonal and annual variability of GPS-TEC have been compared with those derived from International Reference Ionosphere IRI-2016 and IRI-2012 with two different options of topside electron density: NeQuick and IRI01-corr. It is observed that both versions of IRI (i.e., IRI-2012 and IRI-2016) predict the GPS-TEC with some deviations, the latest version of IRI (IRI-2016) predicted the TEC similar to those predicted by IRI-2012 for all the seasons at all stations except for morning hours (0500 LT to 1000?LT). This shows that the effect of the updated version is seen only during morning hours and also that there is no change in TEC values by IRI-2016 from those predicted by IRI-2012 for the rest of the time of the day in the Indian low latitude region. The semiannual variations in the daytime maximum values of TEC are clearly observed from both GPS and model-derived TEC values with two peaks around March-April and September-October months of each year. Further, the Correlation of TEC derived by IRI-2016 and IRI-2012 with EUV and F10.7 shows similar results. This shows that the solar input to the IRI-2016 is similar to IRI 2012. There is no significant difference observed in TEC, bottom-side thickness (B0) and shape (B1) parameter predictions by both the versions of the IRI model. However, a clear improvement is visible in hmF2 and NmF2 predictions by IRI-2016 to that by IRI-2012. The SHU-2015 option of the IRI-2016 gives a better prediction of NmF2 for all the months at low latitude station Ahmedabad compare to AMTB 2013. 相似文献
549.
《Advances in Space Research (includes Cospar's Information Bulletin, Space Research Today)》2020,65(1):95-106
To understand global variability and triggering mechanisms of ionospheric nighttime equatorial spread F (ESF), we analyzed measurements from satellite and a ground-based GPS station for the years between 2010 and 2017. In this study we present seasonal-longitudinal as well as monthly variability of ESF occurrence for solar minimum and yearly variations of ESF occurrence for solar maximum and minimum periods. One of the long standing open questions in the study of ESF is what exactly initiates the Rayleigh-Taylor (RT) plasma instability growth. This question is the focus of the present work. Zonal background eastward electric field and E × B upward plasma drift speed patterns are found to be critically important in understanding plasma irregularity formation. In addition to particular patterns observed on these parameters, the background plasma density in the local evening hours just before the onset of ESF occurrence is very important. Stronger plasma densities just before the onset of irregularities resulted in stronger plasma irregularities, while relatively less dense plasma just before the onset of irregularities resulted in relatively lower plasma irregularities. Seasonal variations in ESF activity between March and September equinox seasons with comparable plasma densities can be defined in terms of the rate of change of solar flux F10.7 (dF10.7/day) index. Strongest ESF occurrence and strongest dF10.7/day are measured in the same month out of all other months in 2016 and 2017. Longitudinal variations of ESF activity in our measurements are related to longitudinal variations of plasma densities. We also found that ESF occurrence is better correlated with rate of change of F10.7 index for months in equinox seasons than for months in solstice seasons for the years between 2013 and 2016. 相似文献
550.
Yi Zhang Bo Xu 《Advances in Space Research (includes Cospar's Information Bulletin, Space Research Today)》2021,67(1):662-677
A kinetic impact occurs when an asteroid is moving. The impact may be caused by other small celestial body or an artificial object. Ejecta is produced from an impact. Dynamics of ejecta near a binary system which contains an ellipsoid and a sphere is analyzed. A phase diagram which comes from numerical simulation is shown in this work. The phase diagram shows a clear structure. Some special trajectories are also shown, which indicates a potential source of asteroid orbiting objects. 相似文献