非晶态镍磷合金电沉积的研究

研究了亚磷酸—镍盐型电解液中主要工艺因素对电沉积非晶态镍磷合金的影响。结果表明,亚磷酸与氯化镍浓度比的影响最明显,该比值小于1:3时,难于形成非晶态镀层。随该比值增加,电沉积速度降低而镀层含磷量增大。镀液pH值和阴极电流密度增大时,镀层含磷量降低,不利于非晶结构的形成。从磷的阴极析出机理及其与析氢反应的相关性讨论了上述实验结果。     

NCu30-4-2-1合金在航空燃油附件上的应用分析

介绍了NC心0-4-2-1合金的成分和性能特点,以及该合金在某型发动机燃油泵-调节器中的应用;通过与3Cr13的对比,分析了该合金能有效地消除"划伤"和"点瘤"故障的原因;最后指出,该合金在航空油泵及其它附件中有很好的应用前景.     

Effect of nickel introduced by electroplating on pyrocarbon deposition of carbon-fiber preforms

In order to improve the deposition rate and microstructure of pyrocarbon, nickel was introduced by electroplating on carbon fibers and used as a catalyst during the deposition of pyrocarbon at 1000 C using methane as a precursor gas. The distribution of nickel catalyst and the microstructure of pyrocarbon were characterized by scanning electron microscopy（SEM）, energy dispersive spectroscopy（EDS）, X-ray diffraction（XRD）, and Raman micro-spectrometry. Results show that nano-sized nickel particles could be well distributed on carbon fibers and the pyrocarbon deposited catalytically had a smaller d002 value and a higher graphitization degree compared with that without catalyst. In addition, the deposition rate of pyrocarbon in each hour was measured.The deposition rate of pyrocarbon in the first hour was more than 10 times when carbon cloth substrates were doped with nickel catalysts as compared to the pure carbon cloths. The pyrocarbon gained by rapid deposition may include two parts, which are generation directly on the nickel catalyst and formation with the carbon nanofibers as crystal nucleus.     

陶瓷圆刀片车削GH4169机理研究及工艺优化

由于具有良好的切削稳定性,晶须增韧陶瓷刀片在高温合金的切削中得到越来越广泛的应用。但是作为切削高温合金的一种新型刀具,其切削机理还未得到充分阐述。为此,本文通过切削机理的研究,得出了陶瓷刀具切削高温合金的最佳工艺条件。     

SiCp增强体表面改性对铁基复合材料组织性能的影响

为了改善粉末冶金方法制得的SiCp/Fe复合材料性能，采用化学镀的方法，成功地在SiCp表面沉积镍，考察了颗粒表面改性对铁基复合材料组织性能的影响。结果表明，镀镍层的作用明显：第一，阻碍了SiCp/Fe界面的过度反应以及Si原子向基体中的扩散；第二，镀镍层的存在改善了颗粒与基体的界面状况，使得颗粒能够更好地发挥增强体的作用。     

GH33A镍基高温合金蠕变裂纹扩展行为

 <正> 蠕变裂纹扩展的研究,首要的是确定表征蠕变裂纹扩展性能的合理判据,本文报导了对燃气涡轮盘常用材料GH33A合金蠕变裂纹扩展4种判据的研究结朱,求得最佳关联该合金蠕变裂纹扩展的参量,为进一步估算寿命打下基础     

俄罗斯对两种镍基单晶合金的对比研究

在第二代和第三代单晶镍基合金中，如ＣＭＳＸ－１０及Ｎ６中都合有比较多的铼，而铼是一种很贵重的合金化元素。俄罗斯学者对含铼的Ｃ３６及不含铼的Ｃ４０单晶合金进行了一些对比性研究，本文介绍了研究的情况及结果。     

镍基合金激光超高温度梯度定向凝固

 采用高能激光束作为定向凝固的热源,研究了镍基合金在超高温度梯度（1.0×104K/cm）定向凝固下的组织结构特征。在定向凝固组织中得到了平均一次枝晶间距仅为10.6μm的细枝晶和完全无侧向分枝的“超细胞晶”.对合金元素在不同组织中偏析行为的分析表明：传统的定向凝固组织中存在严重的微观偏析,而激光超高温度梯度定向凝固组织中,元素的微观偏析大大改善甚至完全消除。     

Effect of Counterface Material on Friction and Wear Behavior of Ni-Cr-W-Al-Ti-MoS2 Composites

Ni-Cr-W-Al-Ti-MoS2 self-lubricating composites were prepared through the powder metallurgy （P/M） method. Their friction properties were investigated by a pin-on-disk tribometer in the range from the room temperature to 600 ℃. Alumina, silicon nitride and nickel-iron-sulfide alloys were selected as the counterface materials. Results indicate that the lowest friction coefficients under 0.22 can be obtained at 600℃ when rubbed against alumina. When rubbed against nickel-iron-sulfide alloys, are presented the lowest wear rates in the magnitude of 10^-6 mm^3/N-m, one order of magnitude lower than those when rubbed against ceramics. In the case of three rubbing pairs, the wear rates of the composite containing MoS2 present themselves inversely proportional to friction coefficients. With alumina ceramics used as a counterface, transfer films and glaze layers will form on the contact surface playing a main role in lubrication at high temperatures. However, when silicon nitride and nickel-iron-sulfide alloy are used, the lubricating transfer films appear not to be prominent.     

脉冲电流对镍电铸层内应力的影响

通过试验，讨论了脉冲电流参数对镍铸层内应力的影响，简要分析了铸层内应力的成因。试验结果表明，平均电流密度，频率及占空比都显著地影响着铸层内应力，合适的电参数组合可以使得铸层内应力为最小。