NEPE推进剂中聚乙二醇的结晶性

利用X射线衍射技术研究了NEPE推进剂中聚乙二醇的结晶特性。探讨了填料、化学交联和增逆剂对聚乙二醇结晶的影响，实验结果表明上述几种因素都会显著降低聚乙二醇的结晶性。     

水相合成CdSe量子点用于荧光标记的光谱研究

生物素-亲和素系统（BAS）已成为目前广泛用于微量抗原、抗体定性、定量检测及定位观察研究的新技术。采用水相合成的CdSe纳米粒子标记生物分子亲合素,用荧光分光光度法研究了亲合素与量子点的结合作用,结果表明标记了亲合素的量子点发光强度高于单一的CdSe量子点,光谱峰位置稍微有所红移。通过改变体系的pH值,亲合素的浓度及荧光显微成像等手段,发现光谱的变化确实是由量子点和亲合素的结合作用所引起的,证明CdSe可以很好的用于生物标记。     

Compound Ceramic Coatings Grown by Micro-plasma Oxidation on Ti-6Al-4V Alloy

Compound ceramics coatings on the Ti-6Al-4V alloy were prepared by the direct current micro-plasma oxidation (MPO) in NaAlO2 solution. The composition and morphology of the coatings were studied with the X-ray diffraction (XRD) and the scanning electron microscopy (SEM), respectively. Inductively coupled plasma atomic emission spectrometer technique was used to analyze the solution features of Ti-6Al-4V alloy in the process of preparation. The results reveal that Al2TiO5 forms in the coatings at the initial stages of MPO reaction, and its content changes rapidly with the reaction continuing: after 20 min, the ceramics coatings are composed of α-Al2O3, γ-Al2O3 and Al2TiO5, but after 40 min, its main composition is of α-Al2O3. The content of Ti in the solution will increase when the MPO time extends, and as will Al in the anode area until, after 30 min, it reaches the maximum and keeps constant from then on. Both substrata of Ti and Al in the electrolyte join the MPO reaction at the initial stage, where the formation of Al2TiO5 happens; but as the MPO reaction prolongs, more and more Al in the electrolyte will take part in the reaction, leading to the appearance of a large amount of Al2O3.     

压强场非接触测量新建议

掺有碘分子的流动流体,在激光的作用下会产生感应的荧光发射,激光感应的碘分子荧光包含有压强的信息,采用成像法,得到的是压强场在一个平面上的分布,因而这一测量是多点测量。作者测量了压强对激光感应的碘分子荧光的影响,去除喇曼散射引起的散射峰,提出了直接利用激光感应的荧光测量流动流体的压强场的非接触测量新方法,还探讨了这一方法的理论和实验方案。     

长波通滤波器的研究

用激光照射掺有碘分子的流场，感应的碘分子荧光包含着流动参数如速度、压强、温度和密度的信息，可用其来对这些参数进行测量。但荧光信号通常很弱，在没有合适滤波器的情况下，测量的信噪比是差的。为了去掉作为噪音的散射的激光和背景光，设计和制造了长波通滤波器，它们具有高质量性能，相应的测量有好的信噪比。     

CMP加工过程中加工载荷对液膜厚度的影响分析

本文采用激光诱导荧光技术(LIF)来研究抛光参数对化学机械抛光加工区液膜厚度的影响.研究表明,抛光液膜厚度随着抛光载荷的增加而减少,减小的趋势随抛光载荷的提高而减缓.同时液膜厚度随着抛光速度的增加而变大.通过抛光参数的变化对抛光液液膜厚度影响的分析,为改善CMP加工工艺提供理论性的依据.     

An icy mineralogy package (IMP) for in-situ studies of Titan’s surface

We describe the scientific case for and preliminary design of an instrument whose primary goal is to determine the chemistry (element abundance) and mineralogy (compound identity and abundance) of Titan’s surface using a combination of energy dispersive X-ray fluorescence spectroscopy (EDXRF) and X-ray diffraction (XRD). XRD is capable of identifying any crystalline substance present on Titan’s surface at relative abundances greater than ∼1 wt%, allowing unambiguous identification of, for example, structure I and II clathrates (even in the presence of ice), and various organic solids, which may include C₂H₂, C₂H₄, C₄H₂, HCN, CH₃CN, HC₃N, and C₄N₂). The XRF component of the instrument will obtain elemental abundances for 16 < Z < 60 with minimum detection limits better than 10 ppm (including detection of atmospheric noble gas isotopes), and may achieve detection limits of 0.01–1% for lighter elements down to Z = 6 (carbon). The instrument is well suited to integration with other analytical tools as part of a light-weight surface chemistry and mineralogy package. Although considerably less sensitive to elemental abundance than GC–MS (10⁻² vs. 10⁻⁸) it is likely to be significantly lighter (<0.5 kg vs. 10 kg).     

飞船舱门机构中密封件性能测试方法介绍

文章以某型号飞船的舱门组件中锁紧机构的橡胶密封件的性能试验为背景,介绍了环境模拟试验密封结构设计和密封件密封性能测试的试验过程、结果和漏率测试方法,验证了密封结构设计和密封材料选择的可靠性.     

基于实时引导修正的大口径天线对星快速校相方法

对测控站中快速校准和差通道相位的方法进行了原理分析,以18 m口径天线为例,论证了在X频段下大口径天线的空间波束相对于S频段更窄,利用X频段空间目标进行快速校相时需要天线系统提供更高的指向精度来满足校相时的角度偏置处于主瓣内.通过分析抛物面天线的指向误差源和模型,提出了基于该模型进行目标引导数据误差反向修正的工程应用方...     

光纤pH值传感器

综述了光纤ｐＨ值传感器,详细阐述和分析比较了光吸收式、荧光特性式及折射率波动式三大类ｐＨ值传感器的工作原理及其各自的优点。还介绍了光纤ｐＨ值传感器作为一种新型传感技术,在生物工程、医学、环境监测及工业过程控制中的应用前景。