2-氯-4,6-二硝基-1,3-苯二酚萃取热力学研究

采用萃取平衡实验法,研究了用有机溶剂萃取水相中2-氯-4,6-二硝基-1,3-苯二酚的萃取热力学性质。考察了选用乙酸乙酯作萃取剂,苯、甲苯、环己烷和正庚烷作稀释剂时对萃取水相中2-氯-4,6-二硝基-1,3-苯二酚的影响。结果表明,萃合物的结构与稀释剂的种类有关,并且2-氯-4,6-二硝基-1,3-苯二酚在有机相中的分配系数随稀释剂介电常数的增大而增大。通过研究温度对萃取过程的影响,证实了乙酸乙酯从水相中萃取2-氯-4,6-二硝基-1,3-苯二酚的过程是一个放热过程,表观热效应ΔH=-10.088 kJ/mol。     

并联六自由度对接平台运动学标定方法研究

对并联六自由度对接平台的结构参数标走问题进行了研究。通过实测运动平台的位姿变化以及对应六根丝杆的增量，提出了直接确定结构参数的标定方法，与传统标定方法相比，避免了迭代计算与收敛判断。仿真验证表明了所提方法的有效性和实用性。     

SiB6陶瓷的制备、性能及应用

文摘介绍了富硼化合物陶瓷的性能,SiB_6的晶体结构、热力学性质及几种主要合成和烧结方法,综述了SiB_6的抗高温氧化、力学、摩擦学、电学性能及其应用,提出了今后的发展方向。     

Comparison of peak characteristics of F2 ionospheric layer over Tehran region at a low solar activity period with IRI-2001 and IRI-2007 models predictions

In the present work values of peak electron density (NmF2) and height of F2 ionospheric layer (hmF2) over Tehran region at a low solar activity period are compared with the predictions of the International Reference Ionosphere models (IRI-2001 and IRI-2007). Data measured by a digital ionosonde at the ionospheric station of the Institute of Geophysics, University of Tehran from July 2006 to June 2007 are used to perform the calculations. Formulations proposed by  and  are utilized to calculate the hmF2. The International Union of Radio Science (URSI) and International Radio Consultative Committee (CCIR) options are employed to run the IRI-2001 and IRI-2007 models. Results show that both IRI-2007 and IRI-2001 can successfully predict the NmF2 and hmF2 over Tehran region. In addition, the study shows that predictions of IRI-2007 model with CCIR coefficient has closer values to the observations. Furthermore, it is found that the monthly average of the percentage deviation between the IRI models predictions and the values of hmF2 and NmF2 parameters are less than 10% and 21%, respectively.     

生物质催化热解油的GC-MS分析

通过酸洗脱灰及脱灰后添加催化剂DHC-32等不同预处理方式处理的玉米秸秆为原料,在小型固定床反应器上制取生物油,用GC-MS分析技术对生物油的成分进行分析。研究结果表明：矿物质的存在降低了热解油的产率,矿物质和催化剂对生物油中化学组分具有显著影响。     

Variation in the ionospheric propagating factor M(3000)F2 at Ouagadougou,Burkina Faso

We use hourly monthly median values of propagation factor M(3000)F2 data observed at Ouagadougou Ionospheric Observatory (geographic12.4°N, 1.5°W; 5.9^o dip), Burkina Faso (West Africa) during the years Januar1987–December1988 (average F10.7 < 130 × 10⁻²² W/m²/Hz, representative of low solar flux conditions) and for January 1989–December1990 (average F10.7 ? 130 × 10⁻²² W/m²/Hz, representative of high solar epoch) for magnetically quiet conditions to describe local time, seasonal and solar cycle variations of equatorial ionospheric propagation factor M(3000)F2 in the African region. We show that that seasonal trend between solar maximum and solar minimum curves display simple patterns for all seasons and exhibits reasonable disparity with root mean square error (RMSE) of about 0.31, 0.29 and 0.26 for December solstice, June solstice and equinox, respectively. Variability Σ defined by the percentage ratio of the absolute standard deviation to the mean indicates significant dissimilarity for the two solar flux levels. Solar maximum day (10–14 LT) and night (22–02 LT) values show considerable variations than the solar minimum day and night values. We compare our observations with those of the IRI 2007 to validate the prediction capacity of the empirical model. We find that the IRI model tends to underestimate and overestimate the observed values of M(3000)F2, in particular, during June solstice season. There are large discrepancies, mainly during high solar flux equinox and December solstice between dawn and local midnight. On the other hand, IRI provides a slightly better predictions for M(3000)F2 between 0900 and 1500 LT during equinox low and high solar activity and equinox high sunspot number. Our data are of great importance in the area of short-wave telecommunication and ionospheric modeling.     

重量的一种遥测式监测系统

本文提出一种重量信号的无线传输和测量方法。重量信号经传感顺转换成电信号，再经Ｖ／Ｆ变换后调频发射，接收信号解调后单片机处理。单片机的信号处理采用电子计数器测频方法，经过计算送显示单元，实现重量信号的遥测。     

Effects of TADs on the F region of the mid-latitude ionosphere during an intense geomagnetic storm

Based on observations of two ionosondes at Wuhan and Kokubunji, this paper presents effects of TADs on the daytime mid-latitude ionosphere during the intense geomagnetic storm on March 31, 2001. During a positive ionospheric storm, the start of the enhancement of the foF2 (F2 peak plasma frequency) at Wuhan lags that at Kokubunji by 15 min, which corresponds to the time interval of traveling atmospheric disturbances (TADs’) propagation from Kokubunji to Wuhan. Associated with the uplifting of the hmF2 (height of F2 peak) caused by TADs, it is observed by the two ionosondes that the F1 cusp becomes better developed. Therefore, during a geomagnetic storm, TADs originating from the auroral oval may have a strong influence on the shape of the electron density profile in the F1 region ionosphere at middle latitudes. It is highly likely that TADs are responsible for the evolution of the F1 cusp.     

一类空间对称6R机构的运动学研究及组合应用

可展开平板机构已广泛应用于平板天线、太阳翼等航天机构产品。为提高可展开平板机构的刚度和展收比,将空间对称6R机构应用于可展开平板机构设计。首先,根据约束条件,计算后给出了一种空间3R运动链的几何参数关系;然后,结合螺旋理论,分析了该3R运动链的约束螺旋系;进而根据对称性,研究了空间对称6R机构的自由度、奇异性等运动特征;在此基础上,提出了一种特殊的空间对称6R转动机构;最后,研究了空间对称6R机构的组合方法,设计出一种新型单自由度可展开平板组合机构,并对其进行了运动学仿真验证。该可展机构具有二维方向的展开收拢能力,为可展开平板机构的创新设计提供了有益参考。     

S形蒙皮零件成形工艺

通过运用S3F软件对S形蒙皮拉形过程进行模拟仿真分析,评估S蒙皮拉形工艺性;预测拉形过程中将产生的缺陷;制定合理工艺方案;优化零件设计和模具结构;实现了该蒙皮零件在数控蒙皮拉伸机上的拉形。