新型低密度Nb-Ti合金抗氧化涂层制备及组织性能分析

针对新型低密度Nb-Ti合金抗氧化性能需求,开展了Si-Cr-Ti系抗氧化涂层研究,重点分析了所制备涂层抗氧化性能和微观组织在氧化前后的变化。结果表明,1 200℃下涂层寿命大于10 h,涂层抗热震性能良好;涂层与基体之间形成一层扩散层,保证了涂层的结合强度;在高温大气环境下,涂层表面生成一种隔绝氧气填补涂层表面空隙的玻璃质SiO_2层,因而具有良好的抗氧化性能。     

Statistical characterisation of spread F over South Africa

The occurrence of mid-latitude spread F (SF) over South Africa has not been extensively studied since the installation of the DPS-4 digisondes in 1996 and 2000 at Grahamstown (33.32 °S, 26.50 °E) and Madimbo (22.38 °S, 30.88 °E) respectively. This study is intended to quantify the probability of occurrence of F region disturbances associated with SF over South Africa. A study was conducted using data for 8 years (2001–2008) over Madimbo (with a time resolution of 30 min) and Grahamstown (with a variable time resolution of 15 and 30 min). In this study, SF has been classified into frequency SF (FSF), range SF (RSF) and mixed SF (MSF). The SF events were identified by manually identifying ionograms showing SF and tabulating them according to type for further statistical analysis. The results show that the diurnal pattern of SF peaks strongly between 01:00 and 02:00 local time, LT (LT = UT + 2 h), where UT is the universal time. This pattern is true for all seasons and types of SF at Madimbo and Grahamstown in 2001 and 2005, except for RSF which had peaks during autumn and spring in 2001 at Madimbo. The probability of both MSF and FSF tends to increase with decreasing solar activity, with a peak in 2005 (a moderate solar activity period). The seasonal peaks of MSF and FSF are more frequent during winter months at both Madimbo and Grahamstown. In this study, SF was evident in ∼0.03% and ∼0.06% of the available ionograms at Madimbo and Grahamstown respectively during the 8 years.     

基于IRI-2012模型广州地区f_0F_2实测与预测的对比分析

利用广州台站(23.2°N,113.3°E)的实测数据和IRI-2012模型提供的预测数据,对比分析了2013年广州地区f_0F2的变化特征.结果表明,IRI-2012模型能够较好预测该地区f_0F_2的变化趋势,并且CCIR参数得到的预测值比URSI参数更接近实测值;预测值与实测值存在系统偏差,在11:00 LT-06:00 LT时段,观测值均比预测值大,其他时段则相反.在日落后至午夜前时段,预测值与实测值有较大差距.绝对偏差的极值点通常出现在20:00 LT左右,最大超过4 MHz.相对偏差变化比较明显的时段是午夜后至凌晨;在02:00 LT或04:00 LT及06:00 LT附近,可能会出现双误差峰值点,最大超过0.4;但在σ变化很大的20:00 LT附近,相对偏差却变化不大.夜间增强现象会使得偏差增大,导致预测值不能很好反映实测f_0F2的变化.     

F-12 纤维/RE14复合材料压力容器成型工艺研究

研究讨论了缠绕过程中几种主要工艺参数对F— 12纤维 /RE14配方Φ15 0mm压力容器复合材料性能的影响。结果表明 :采用“交替”铺层方式缠绕成型 ,含胶量控制在 30 %～ 4 0 % (质量分数 ) ,缠绕张力控制在 15 0N～ 2 0 0N ,采用GPC谱图控制固化时机 ,得到的复合材料综合性能较好 ;用优化出的工艺参数进行了Φ4 80mm压力容器试验 ,结果表明其容器特性系数PV/W值为 37.0 2km ,纤维强度转化率高达73.2 6 %。     

Al2O3/hBN自润滑复合材料的制备及显微结构分析

以Al2O3为陶瓷基体,hBN为固润滑组元添加剂,在N2保护下烧成,制得了Al2O3/hBN自润滑复合陶瓷,通过SEM、EDS、XRD等分析探讨了固润滑组元的引入量、添加助熔剂及常压和热压两种烧成条件下材料显微结构的变化。结果表明,hBN引入量为10%时已有足够的量均匀分散在基体中;相同烧成温度下,热压过程中施加的压力可以破坏hBN的卡片房式结构,伴随液相的出现有利于hBN的定向排列,获得了结构致密的自润滑复合陶瓷材料。     

高强Al-Cu-Li-X铝锂合金2A97三级时效工艺及性能研究

以新型高强Al-Gu-Li-X铝锂合金2A97为研究对象,通过拉伸试验研究两种三级时效工艺及其改型工艺对合金性能的影响.结果表明,含有δ′相二次析出过程的三级时效和含有δ′相回溶过程的三级时效处理合金的强度和塑性达到T6峰值时效水平,三级时效改型工艺由于增加变形使前者合金的强度升高,塑性降低,使后者的强度显著提高.三级时效和单级时效合金的主要显微组织有δ′相、θ″/θ′相和T1相.三级时效改型工艺由于增加变形促进δ′相析出和δ′相回溶,同时变形促进T1相析出,从而改变了主要强化相δ′相和T1相的数量.     

无加力涡扇发动机二元喷管的红外辐射特性实验

对轴对称喷管和一组长宽比分别为1,4,8,12和16的二元喷管进行了红外辐射特性测试实验研究。喷管中的气流由主流燃气和次流空气组成,用以模拟涡扇发动机的喷管。得出了二元喷管的红外辐射强度的空间分布,并且将二元喷管和轴对称喷管的红外辐射强度进行了比较。      

Electrolytic Passivation of Nitinol Shape Memory Alloy in Different Electrolytes

The corrosion behavior of the nitinol alloy was studied in various corrosion media of different Cl–ion concentrations. The results demonstrate that the Cl–ion concentration has significant influences on the corrosion behavior of the nitinol alloy. In order to enhance the corrosion resistance, protective films were generated on the surface of the nitinol alloy by means of the electrochemical passivation method, for which five different electrolytic solutions were investigated. The surface analysis indicates full growth of all samples pas-sivated in the different electrolytic solutions with layers, however, showing different morphological features. Without any defects like micro-cracks and pores, the surface of the samples passivated in the molybdate solution turns out smoother and denser than those pas-sivated in other solutions. It is shown that the electro-chemical passivation will reduce Ni content but increase Ti content in the surface, reaching the Mole ratio of Ti:Ni=9.01:1 on the outermost surface. Potentiodynamic polarization test demonstrates that the samples electrochemically passivated in the molybdate solution present a significant increase in breakdown potential due to titanium enrichment on the outermost surface.     

联合应用现代优化方法与S2流面计算进行多级涡轮的气动设计

本文联合应用S2流面正问题计算和多级局部优化设计对某三级涡轮进行多级气动优化设计。优化联合采用人工神经网络和遗传算法,流场计算采用全三维粘性流N-S方程求解,计算网格采用H-O-H型网格,即入口段、出口段采用H型网格,叶片区域采用O型网格。通过优化,总效率提高1.1%,总体性能提高,达到设计要求。     

红外反射材料In（Sn）2O3（ITO）的微波吸收性能

测试7.7vol%和15.8vol%In(Sn)2O3(ITO)/石蜡在2~18GHz的介电谱。测定10vol%和20vol%In(Sn)2O3(ITO)/环氧树脂在2~8GHz的反射率。结果显示,ITO材料具有很好的介电损耗。当涂层厚度d=3mm时,两种涂层分别在4.51GHz和6.27GHz有-10.5dB和-14dB的反射率。理论值显示,15.8vol%ITO/石蜡复合材料在4.56~11GHz的反射率低于-10dB,有好的吸波性能。同时分析ITO的介电损耗机理。