硅氮烷环体的催化聚合及热解制备Si3 N4 材料

采用甲基氢二氯硅烷的氨解产物硅氮烷环体(MHSZ)为原料,以四丁基氟化铵为催化剂,制备了高分子量的硅氮烷聚合物(PHSZ),结合红外、核磁、凝胶色谱仪和热重分析了反应时间对合成的PHSZ结构、组成、分子量和陶瓷产率的影响。考察了低温氨气,高温N2气氛处理工艺对热解产物结构和组成的影响。结果表明,随着反应时间的延长,PHSZ高聚物的分子量提高,热失重降低;采用该热解方式PHSZ可转化为含碳量仅为0.5wt%的Si3N4材料,热解样品在1 600℃时完全结晶,晶相主要是α-Si3N4。     

Global ionospheric scintillations revealed by GPS radio occultation data with FY3C satellite before midnight during the March 2015 storm

Global observations of S4 amplitude scintillation index by the GPS Occultation Sounder (GNOS) on FengYun-3 C (FY3C) satellite reveal global dynamic patterns of a strong pre-midnight scintillations in F-region of the ionosphere during the St. Patrick’s Day geomagnetic super storm of 17–19 March 2015. The observed strong scintillations mainly occurred in the low latitudes, caused by equatorial plasma bubbles. During the main storm phase (March 17), the scintillations were first triggered in the New Zealand sector near 160°E longitudes, extending beyond 40°S dip latitude. They were also enhanced in the Indian sector, but significantly suppressed in East Asia near 120°E longitude and in Africa around 30°E longitude. During the initial recovery phase (March 18–19), the global scintillations were seldom observed in GNOS data. During the later recovery phase (after March 19), the scintillations recovered to the pre-storm level in Indian, African, and American sectors, but not in East Asian and any of Pacific sectors. These results closely correlate with observations of the density depletion structures by the Communication/Navigation Outage Forecasting System (C/NOFS) satellite, and ground-based instruments. Such consistency indicates reliability of our scintillation sensing approach even in a case-by-case comparison study. The prompt penetration electric field and disturbance dynamo electric field are suggested as the main factors that control the enhancement and inhibition of the scintillations during the storm, respectively.     

Early analysis of precise orbit and clock offset determination for the satellites of the global BeiDou-3 system

Eight new-generation BeiDou satellites (BeiDou-3) have been launched into Medium Earth Orbit (MEO), allowing for global coverage since March 2018, and they are equipped with new hydrogen atomic clocks and updated rubidium clocks. Firstly, we analyzed the signals for the carrier-to-noise-density ratio (C/N0) and pseudorange multipath (MP) by using international GNSS (Global Navigation Satellite System) Monitoring and Assessment System (iGMAS) station data, and found that B1C has a lower C/N0, and B2a has the same level of C/N0 as the B1I and B3I signals. For pseudorange multipath, compared with the BeiDou-2 satellites, the obvious systematic variation of MP scatters related to the elevation angle is greatly improved for the BeiDou-3 and BeiDou-3e satellites signals. For the signals of the BeiDou-3 satellites, the order of the Root Mean Square (RMS) values of multipath and noise is B3I?<?B1I?<?B2a?<?B1C. Then, the comparison of the precise orbit determination and clock offset determination for the BeiDou-2, BeiDou-3, and BeiDou-3 experimental (BeiDou-3e) satellites was done by using 10 stations from iGMAS. The 3D precision of the 24?h orbit overlap is 24.55, 25.61, and 23.35?cm for the BeiDou-3, BeiDou-3e, and BeiDou-2 satellites, respectively. BeiDou-3 satellite has a comparable precision to that of the BeiDou-2 satellite. For the precision of clock offset estimation, the Standard Deviation (STD) of the BeiDou-3 MEO satellite is 0.350?ns, which is an improvement of 0.042?ns over that of the BeiDou-2 MEO satellite. The stabilities of the BeiDou-3 and BeiDou-3e onboard clocks are better than those of BeiDou-2 by factors of 2.84 and 1.61 at an averaging time of 1000 and 10,000?s, respectively.     

MSG-3在民用航空器维修大纲制定中的应用

国内民用航空器的研发起步较晚,目前投入运行的国产航空器型号种类和数量都不多,航空器制造厂家在制定维修大纲方面的经验较少.本文对国际上通行的MSG-3维修任务分析方法进行研究,首先介绍MSG-3维修任务分析方法产生和发展的历史背景,以及其在国内民机型号中的应用;然后详细叙述MSG-3维修任务分析方法(包括航空器系统、动力装置维修任务的分析方法,结构检查和区域检查任务的分析方法,以及形成维修大纲的流程和维修任务的后期优化);最后通过对航空器型号的审查经验,总结我国民用航空器制造厂家在制定航空器维修大纲时存在的问题和改进方向.     

温度对飞机燃油射流泵工作特性影响

建立了射流泵数学模型,采用数值计算方法对其工作特性进行了模拟,搭建了实验台,采用RP-3燃油,通过实验数据验证了模型的正确性.在此基础上,分别选择了RP-3和JET-A两种燃油,计算了从-40℃~40℃温度下,不同操作压力对射流泵流量比的影响.结果表明:燃油温度高于0℃时,温度对射流泵工作特性影响并不明显,随着温度的降低,射流泵性能与标准温度下（20℃）偏差越来越大,且压比越高此偏差越明显.当温度高于0℃时,采用RP-3和JET-A燃油性能相差不大,RP-3燃油性能略优于JET-A燃油,但是在低温下,RP-3燃油性能远高于JET-A燃油.因此当燃油温度较低且压比较高时,必须充分考虑温度对射流泵特性的影响.      

Al/Ni含能多层膜在Al2O3陶瓷/不锈钢焊接中的应用

采用磁控溅射设备,生长AuSn合金做焊料层、Al/Ni含能多层膜做热量提供层,实现了不锈钢和Al_2O_3间的异质材料自蔓延高温扩散焊。利用SEM、XRD和DSC等测试手段表征AuSn合金和Al/Ni含能多层膜的微观形貌、相成分和放热量;用万能试验机测试焊接接头的力学性能。结果表明,AuSn合金的质量比基本达到80∶20,而多层膜的层状结构清晰,反应热达到1 239 J/g。焊接实验结果表明,仅使用AuSn焊料时,剪切强度仅为46 MPa,在增加Al/Ni含能多层膜后,其剪切强度可达90 MPa,强度提高了约一倍。焊接接头的界面显微形貌和相结构研究表明,剪切强度的增强主要是Al/Ni多层膜提供了额外能量使得界面处的反应剧烈,陶瓷金属化层与中间层的反应加剧,形成了新的反应生成物。     

基于C51单片机的MP3播放器的设计与实现

介绍一种基于C51内核的单片机MP3解码系统的设计与实现,系统采用高性能51单片机和灵活的模拟音频接口,通过对MP3的编解码算法和编程的改进与优化,实现实时解码过程。     

含多部位损伤搭接结构应力强度因子三维有限元分析

应力强度因子(Stress intensity factor,SIF)分析是含多部位损伤(Multiple site damage,MSD)结构剩余强度和裂纹扩展寿命预测的基础和关键。考虑接触与摩擦,建立了含MSD搭接结构的三维有限元模型,研究了不同裂纹长度、铆钉类型以及损伤模式下裂纹尖端SIF分布情况和变化规律。结果表明,搭接件孔边裂纹Ⅰ型SIF起主导作用,Ⅱ型和Ⅲ型SIF可忽略不计。由于次弯曲、铆钉变形和板厚度等因素,SIF在外表面最小,接触面一侧较大,最大值多位于蒙皮内部。MSD会使裂纹间的干涉作用增强,SIF增大,且裂纹间距离越近干涉作用越强。裂纹长度相同时,埋头铆钉的孔边裂纹SIF积分均值大于平头铆钉,且接触面的SIF埋头铆钉大于平头铆钉,外表面则相反。     

基于北斗三号短报文的共视数据压缩传输方法

共视时间比对通过交换两地共视数据完成远距离高精度的时间比对。针对无地面通信网地区,本文提出了一种基于北斗短报文的共视数据压缩传输方法,该方法通过将共视数据进行压缩,利用北斗的短报文功能对压缩后的共视数据进行实时传输,在无地面通信网的地区进行了共视时间比对试验。试验结果表明,本文设计的共视数据压缩方法具有较好的压缩效果,可以通过北斗短报文实现无地面通信网的情况下的实时共视时间比对。     

面向3D打印的设计制造一体化探索

紧密围绕航天结构未来发展需求,以增材制造复杂产品研发为研究对象,对实现设计制造一体化的技术路线和关键技术进行分析。把设计、仿真和制造有机统一起来,把工艺设计纳入结构设计流程,通过仿真驱动设计来提高产品质量、降低制造成本。研究成果可应用于航天领域增材制造产品研发,对传统设计制造模式向智能制造转型具有积极探索意义。