A New Scheme and Microstructural Model for 3D Full 5-directional Braided Composites

Three-dimensional(3D) braided composites are a kind of advanced ones and are used in the aeronautical and astronautical fields more widely. The advantages, usages, shortages and disadvantages of 3D braided composites are analyzed, and the possible approach of improving the properties of the materials is presented, that is, a new type of 3D full 5-directional braided composites is developed. The methods of making this type of preform are proposed. It is pointed out that the four-step braiding which is the most possible to realize industrialized production almost has no effect on the composites'properties. By analyzing the simulation model, the advantages of the material compared with the 3D 4-di- rectional and 5-directional materials are presented. Finally, a microstructural model is analyzed to lay the foundation for the future theoretical analysis of these composites.     

铼(Re)对定向高温合金组织与性能的影响

以第二代定向柱晶DZ9合金成分为基础,调整Re含量,通过对三种不同Re含量的定向合金的研究,探讨了Re含量的变化对定向高温合金组织和性能的影响。结果表明:加入Re可提高合金的初熔温度和γ'相的回溶温度;Re的含量显著影响合金的γ+γ'共晶相形态和γ'相的尺寸和形态;增加Re含量,可提高合金的室温拉伸强度和合金的高温持久寿命。     

热处理对BT25 Y钛合金组织和性能的影响

本文研究了不同的固溶温度、固溶后冷却速度以及热暴露对BT25Y钛合金组织和性能的影响。结果表明,BT25Y钛合金于950℃固溶属于α β两相区固溶,其组织由初生等轴α相和片状α β相组成,硬度随冷速的增大而增大,但随着热暴露时间的延长,在40小时时硬度达到最大值,而后降低;而990℃固溶属于β区固溶,由β相降温分解的α β两相组成,硬度较950℃固溶高,也随冷速的增大而增大,但随着热暴露时间的的延长,硬度在30小时时达到最低值,而后持续增大。     

BT-14钛合金舱口外盖白斑问题

BT-14钛板为某产品舱口盖结构用材料,焊前检查时,发现钛板表面有数量不等的白色圆状斑点。文章从白斑的外观形貌、微观组织以及力学性能等方面进行分析,重点研究了白斑组织对钛板使用性能的影响,并提出后续生产中的预防措施。     

Improving tensile-shear properties of friction stir lap welded dissimilar Al/Mg joints by eliminating hook defect and controlling interfacial reaction

To improve tensile-shear properties of fiction stir lap welded(FSLW) dissimilar Al/Mg joints, pin-tip profiles were innovatively designed and welding speed was optimized, and effects of them on formation, interface microstructure and mechanical properties of different FSLW joints were investigated. With increasing the welding speed, the tensile-shear load of FSLW joints produced by three pins presents an increasing firstly and then decreasing trend. Compared with Rpin, the hook and hole defect i...     

A hybrid chemical modification strategy for monocrystalline silicon micro-grinding: Experimental investigation and synergistic mechanism

For high performance manufacturing of micro parts and features, a hybrid chemical modification strategy is proposed to decrease critical energy barrier of mechanical removal of hard and brittle crystal material by refining localized machining condition. The strategy, namely UV-light and IR-laser hybrid chemical modification (UVIR-CM) strategy, includes two steps, an ultraviolet light (UV-light) catalytic advanced oxidation and an infrared laser (IR-laser) assisted selective modification based on Fenton liquid–solid reaction for monocrystalline silicon. The modification effects of UVIR-CM strategy were investigated by surface morphology micro-observation, cross-section transmission electron microscopy (TEM) observation, Raman spectroscopy analysis and nanoindentation test. Experimental results demonstrated that varied degrees of laser texturing appeared on different strategy samples’ IR-laser scanned area. And the IR-laser thermal damage has been successfully inhibited due to the refraction and reflection of energy by bubbles in liquid medium. But for the UVIR-CM strategy, a uniform and amorphous silicate layer is detected in a certain boundary. The UV-light promotes oxidation cycle ability of the chemical solution and ensures sufficient oxide modified layer for subsequent step. Attributing to synergism of photochemical, photothermal and kinetic effects induced by IR-laser, the modified layer displays layered structure with about 600 nm thickness, (2.7 ± 0.60) GPa nanohardness, and (93.7 ± 22.9) GPa indentation modulus. And the layered structure is amorphous layer, nanocrystal and micro-twins layer from the surface to the interior of sample. Consequently, it reveals that the subsequent mechanical removal will become easy due to decreasing energy barrier of monocrystalline silicon in selective area. Meanwhile, its original excellent mechanical properties also are maintained under a certain depth. The results contribute to develop a novel combined micro-machining technology to achieve collaborative manufacturing of structure shape and surface integrity for micro parts and feature.     

Effect of Isothermal Forging on the Microstructure and Mechanical Properties of Mg-8Gd-3Y-0.5Zr Alloy

Aiming at the problems of poor plastic forming ability， narrow forging temperature range， and strain rate sensitivity of rare earth magnesium alloys， a study on the microstructure and mechanical properties of Mg-8Gd-3Y-0.5Zr alloy with different isothermal forging processes is carried out. The microstructure and properties of the alloy in the as-cast， isothermal forged， and post-aging states after forging are studied with optical microscope (OM)， scanning electron microscope (SEM)， and tensile testing. The results show that significant dynamic recrystallization occurs during the isothermal forging process， a fine equiaxed grain structure is formed， and the mechanical properties of the alloy are greatly improved. When the isothermal forging temperature is 460 ºC and the strain rate is 0.02 s－1， the alloy structure performance is the best， the room temperature tensile yield strength (TYS) is 218 MPa， the ultimate tensile strength (UTS) is 299 MPa， and the fracture elongation (FE) is 19.2%. When the alloy is post-forging artificial aged， the α-Mg matrix is dispersed， the Mg5(Gd，Y) phase is precipitated， the UTS of the alloy is increased to 392 MPa， and the FE is reduced to 12.0%.     

激光熔化沉积15-5PH沉淀硬化不锈钢组织及拉伸性能

利用激光熔化沉积技术制备15-5PH沉淀硬化不锈钢板,利用金相显微镜(OM)、扫描电镜(SEM)、透射电镜(TEM)、电子探针(EPMA)技术,对沉积态组织进行分析,测试沉积态组织的室温拉伸性能。结果表明:激光熔化沉积15-5PH不锈钢沉积态组织由沿沉积增高方向贯穿多层外延生长的柱状晶组成,柱状晶内包含多个细长整齐排列的胞状树枝晶,枝晶内为马氏体组织,枝晶间为铁素体;沉积态组织中弥散分布大量细小的NbC析出相,尺寸12～20 nm;15-5PH不锈钢沉积态组织具有良好的力学性能,纵向抗拉强度和延伸率分别为1 128.5 MPa和14.0%,横向抗拉强度和延伸率分别为1 101 MPa和12.25%。     

干式铣削Al-50wt%Si高硅铝合金刀具磨损与表面粗糙度评价

本文以Al-50wt%Si高硅铝合金为研究对象，采用单因素试验方法进行无涂层硬质合金刀具干式铣削试验，分析切削参数对刀具磨损和表面粗糙度的影响。结果表明：表面粗糙度受每齿进给量的影响最显著，随每齿进给量的增加而增加，当每齿进给量从0.07 mm/z增加到0.16 mm/z时，表面粗糙度增加2倍；刀具磨损受切削速度的影响最显著，随切削速度的增加而增加，当切削速度从140 m/min增加到260 m/min时，切削总长度降低3倍，而刀具后刀面磨损量仅是260 m/min速度下的0.8倍；表面粗糙度随刀具磨损的增加呈现先增加后降低的变化趋势，切削长度从350 mm增加到1 750 mm，刀具磨损量平均增加4.5倍，而表面粗糙度却下降2倍；硬质合金刀具主要的磨损形式为磨粒磨损、崩刃。     

Microstructure and Hot Deformation Behavior of Mg-9Al-3Si-0.375Sr-0.78Y Alloy

Using Gleeble-3500 thermal simulator， the high temperature plastic deformation behavior and microstructure evolution of Mg-9Al-3Si-0.375Sr-0.78Y alloy are investigated at the temperature of 523 K?673 K and the strain rate of 10-3 s-1?10 s-1. True strain-true stress curves show the characteristics of the typical dynamically recrystallization process. The Arrhenius constitutive equation of the hyperbolic model is established. The average activation energy and the strain rate sensitivity index are， respectively， 221.578 kJ.mol-1 and 0.137. The result shows that the α-Mg phase exhibits dynamic recrystallization (DRX) characteristics obviously. But no DRX occurs in theβ-Mg17Al12 phase. Hot deformation does not affect the primary Mg2Si phase. Under the conditions of low temperature (523 K?673 K) and high strain rate (1 s-1?10 s-1)， the flow instability and macro-defects such as crack appear in the specimens. However， there are finer recrystallization grains. Under the conditions of high temperature (≥673 K) or low strain rate， the microstructure of the alloy shows good homogeneity. The size of the primary Mg2Si phase is uniform， the size of the β-Mg17Al12 phase is small， and the distribution of the β-Mg17Al12 phase is uniform.