凝固过程对颗粒增强Al—4%Mg复合材料中颗粒分布的影响

研究了凝固过程ＳｉＣ、Ａｌ＿２Ｏ＿３、ＳｉＯ＿２颗粒增强Ａｌ－４％Ｍｇ复合材料中颗粒分布的影响。通过分析，建立了描述等轴晶凝固条件下，颗粒推移强烈程度的晶粒与颗粒质量比模型，模型预测与试验结果吻合良好。     

定向凝固铝铜合金一次枝晶间距的研究

本文实验研究了凝固参数对铝铜合金一次枝晶间距的影响。结果表明,一次枝晶间距Z_1,并不随生长速度V或温度梯度G的增加而连续减小,而是在V=(1-3)V_(CS)/k时达到极大值,在G=kG_(CS)时急剧改变,其中V_(CS)和G_(CS)是平面生长成分过冷极限下的生长速度及温度梯度。仅在高速生长条件下,关系式Z_1=KG~-(1/2)V-(1/4)才成立,K——与合金性质有关的常数。一次间距的极大值或突变对应于胞晶——枝晶转变。一次枝晶是在“生长——淹没——竞争再生长”的过程中生长的,竞争再生长的方式是“扰动再生长”及“新晶再生长”。     

Microstructure evolution of a hypereutectic Nb–Ti–Si–Cr–Al–Hf alloy processed by directional solidification

In this work, the Nb–14Si–24Ti–10Cr–2Al–2Hf–0.1Y alloy(at.%) was processed by the liquid–metal-cooled directional solidification(DS) at 1750 C with withdrawal rates of 1.2, 6,18 mm/min and post heat treatment(HT) at 1450 C for 10 h. The microstructures of the directionally solidified and heat treated samples were investigated. The results show that the microstructure of directionally solidified alloy mainly consists of petaloid Nbss+ Nb5Si3eutectics and Ti-rich Nbss+ Nb5Si3+ Cr2Nb eutectics. With the increase of withdrawal rate, the primary Nb5Si3is eliminated, Nbss+ Nb5Si3eutectic cells turn round and connected with the microstructure refinement and Nbss+ Nb5Si3+ Cr2Nb eutectics turn to a river-like morphology. After heat treatment,Nbss+ Nb5Si3+ Cr2Nb eutectics disappeared and petaloid Nbss+ Nb5Si3eutectics turn to a specific fiber-mesh structure gradually, which is promoted by higher withdrawal rates. Furthermore,both the volume fraction of Cr2Nb and the content of Cr in Nbssof Nbss+ Nb5Si3eutectics change regularly with the increase of withdrawal rate and heat treatment at 1450 C for 10 h.