Comparative Study on Super Fine Mesophase Powder and MCMB Used to Manufacture High-Density Isotropic Carbon Bulks

Mesocarbon microbeads (MCMB) and super fine mesophase powder (SFMP) were prepared firstly from a coal tar pitch and then hot-condensed into high-density isotropic carbon (HDIC) bulks under 160 MPa and finally sintered at 1 000 ℃ . By analyzing the ther-mogravimetric behavior of the MCMB and SFMP powders, their volume shrinkage and weight loss during sintering and the bulk density and flexural strengths of their sintered bulks, it was found that the smaller sizes and the richer β-resin contents of SFMP have facilitated formation of sintered bulks with more compact isotropic structure and higher flexural strengths than MCMB. Because of the filling and bonding effects of SFMP on MCMB bulks, addition of SFMP, albeit a little, can greatly increase the flexural strengths of sintered bulks of MCMB. However, adding MCMB, even a slight amount, into SFMP can severely impair the flexural strength of sintered bulks. This might be attributed to both the crack initiation along the boundaries between MCMB and SFMP and the formation of layered texture of MCMB sphere.     

Preparation and Mechanical Properties of Glass Coats with High Temperature Radar Absorber

BaO-La2O3-B2O3 （BLB） glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the absorbing coat because it is considered to be a good high temperature absorber. The effect of the coating temperature and coating time on the tensile strength of the glass coat was investigated and the proper coating parameters to get good mechanical properties were determined. In addition, the effects of the SiCN content on the tensile strength of the absorbing coat were also discussed. Results show that it is possible to prepare the glass coat using the BLB glass as a binder. That the coat formed at 730℃ for 30 min has the best tensile strength witnesses 730 ℃, 30 min to be the proper parameter to prepare the glass coat. The BLB glass coat without SiCN powder possesses good tensile strength and the introduction of the SiCN absorber into the glass coat will lower the tensile strength. As the SiCN content increases, the tensile strength of the absorbing coat decreases, which could be attributed to the aggregation of SiCN in the coats.     

粉末粒度对快速凝固／粉末冶金Al-Fe-Mo-Si／Zn-Al复合材料组织与性能的影响

研究不同粉末粒度Al-9.0?-1.8%Mo-1.7%Si/5%(Zn-30%Al)金属/金属复合材料的组织、拉伸性能和阻尼性能.快速凝固粉末由气体雾化制备,选取平均粒度d50分别为27.3,36.2,41.6μm粉末装入包套,经除气,再热挤压制成棒材.结果表明,粉末粒径越粗,强化相越粗大,呈团聚体存在,且有偏聚现象,材料的强度明显下降,室温下粉末较细材料的阻尼性能较好,高于100℃时粉末粒度较粗材料的阻尼性能好.     

单晶硅超精密车削加工脆塑转变机理及临界切削厚度的研究

通过分析单晶硅的纳米印压试验结果以及显微压痕透射电镜观察结果,并结合尺度效应理论,提出了一种新的单晶硅超精密切削脆塑转变机理,建立了宏微结合的单晶硅超精密切削模型。首次基于理论分析的方法给出了较为精确的单晶硅脆塑转变的临界切削厚度,并通过试验对研究结果给予验证。     

粉末合金(FGH95)蠕变/疲劳交互作用下寿命预测的损伤力学有限元分析

采用基于损伤力学的蠕变—疲劳交互作用下的寿命预测模型,应用损伤等效应力进行三维应力状态下的损伤计算,并考虑了压缩时闭合效应,利用ANSYS的二次开发工具APDL和UPFs开发程序,把基于损伤力学的寿命预测方法与ANSYS的结构分析结合起来,实现了对构件的损伤计算和寿命预测。针对粉末合金材料易含夹杂等初始缺陷的特点,提出了在寿命计算中通过单元初始损伤模拟初始缺陷对寿命影响的处理方法,探讨了考虑初始缺陷条件下的寿命预测,并利用试验对计算结果进行了对比验证。      

Ni基金属粉末激光快速制造的研究

 采用激光选区烧结的方法,对 Ni基合金混合铜粉末进行了一系列激光烧结试验。从烧结模型入手,分析了烧结过程中出现的现象,讨论了工艺参数对金属粉末烧结成形的影响,初步探索了金属粉末直接烧结成形的基本机理,为金属粉末的激光快速成形制造提供了依据。     

激光烧结快速成形试样强度的研究

研究了激光烧结快速成形试样密度与其静态强度的关系，烧结粉末中粘结剂含量、激光功率、激光束的扫描速度、扫描间隔以及扫描路径对试样弯曲强度的影响，分析了烧结过程中产生翘曲变形的原因，并通过三点弯曲实验测试了烧结试样的抗弯强度。     

超细 CaCO3 对丁羟复合固体推进剂燃烧及工艺性能的影响

通过超级及市售ＣａＣＯ３在低含量下（≤１％）对丁羟推进剂燃烧及工艺性能影响的研究,发现两种ＣａＣＯ３均可提高推进剂的燃速,且随超细ＣａＣＯ３含量增加,推进剂压强指数降低,与市售ＣａＣＯ３相比,超细ＣａＣＯ３的催化效率较高,但同时也使推进剂的工艺性能变差。     

NOPD颗粒减振机理的理论及实验研究

NOPD(Non-Obstructive Particle Damping)又称粉体阻尼技术,它是 90年代发展起来的一种新的被动减振技术。以两端自由的等截面梁为研究对象,从微小颗粒的摩擦和冲击两个方面建立其减振理论模型,实现对振动响应的数值仿真并进行了实验验证,对 NOPD的减振特性进行了较深入的研究。     

铁氧体吸收剂粉体的煅烧工艺研究

研究了铁氧体吸收剂粉体的煅烧工艺对粉体的性能、形貌和相组成的影响.研究表明,粉体的形貌和相组成对其复数磁导率有较大影响.经过对煅烧工艺进行优化,制备出了较高性能的吸收剂粉体.