溶胶-凝胶法制备纳米TiO2 及粒径控制工艺

采用溶胶-凝胶法,以钛酸丁酯为前驱体,乙二醇作为螯合剂制备纳米TiO2 粒子。考察钛的乙二

醇盐的浓度、pH 值、温度等因素对TiO2 粒径的影响,并用红外光谱和SEM 对纳米TiO2 粒子进行结构和形貌表

征。结果表明,采用溶胶凝胶法可以制备出呈椭圆形且粒径分布均匀的TiO2 纳米粒子。使用硝酸铵可以有效

阻止TiO2 纳米粒子团聚。当pH 值为2 ~3、温度为20 ~40℃,钛的乙二醇盐在丙酮中的浓度为0. 03、0. 05 及

0. 07 M 时,粒径分别为150、240 及600 nm。

     

基于变步长LMS算法的线性调频引信噪声抑制

利用自适应滤波技术,研究了线性调频引信通带内噪声的抑制问题。根据线性调频信号与噪声可预测性的差异进行噪声抑制,分析了噪声抑制原理。仿真结果表明,在SNB=-5dB时仍然可以达到很好的噪声抑制效果;在算法收敛的条件下,信噪比越小,噪声抑制对信噪比的相对改善越大。     

Numerical study on combustion efficiency of aluminum particles in solid rocket motor

The combustion of aluminum particles in solid rocket motor plays an important role in energy release of propellants. However, due to the limited residence time, aluminum particles may not be burned completely, thus hindering the improvement of specific impulse. This study aims to explore the characteristics of aluminum combustion efficiency and its influencing factors by experiments and numerical simulations, providing a guideline for engine performance improvement. As an input of simulation, the initial agglomerate size was measured by a high pressure system. Meanwhile, the size distribution of the particles in plume was measured by ground firing test to validate the numerical model. Then, a two-phase flow model coupling combustion of micro aluminum particle was developed, by which the detailed effects of particle size, detaching position and nozzle convergent section structure on aluminum combustion efficiency were explored. The results suggest that the average combustion temperature in the chamber drops with increasing initial particle size, while the maximum temperature increases slightly. In the tested motors, the aluminum particle burns completely as its diameter is smaller than 50 μm, and beyond 50 μm the combustion efficiency decreases obviously with the increase of initial size. As the diameter approaches to 75 μm, the combustion efficiency becomes more sensitive to particle size. The combustion efficiency of aluminum particle escaping from end-burning surfaces is significantly higher than that from internal burning surface, where the particle combustion efficiency decreases during approaching the convergent section. Furthermore, the combustion efficiency decreases slightly with increasing nozzle convergent section angle. And theoretically it is feasible to improve combustion efficiency of aluminum particles by designing the convergent profile of nozzle.     

电大尺寸平面数字相控阵外场通道校准测试方法

电大尺寸平面数字相控阵通道校准测试对暗室规模和质量要求极高，扫描架探针移动速度受限导致通道校准的暗室测试时间长达数小时，且长时间测试引起的温度变化会造成通道相位漂移从而导致测试结果不准确。针对存在的问题，提出了一种外场通道校准测试方法，整个阵面中所有通道单次校准测试仅需几分钟，可有效解决由于长时间测试引起的温度变化进而造成的通道相位漂移问题，并通过引入基准通道来解决外场通道校准测试中存在的收发不同源问题。测试方法可有效缩短电大尺寸平面数字相控阵的通道校准时间，提高测试准确性，降低天线测试过程中的时间成本和暗室硬件建造成本。最后，通过某Ka频段电大尺寸平面数字相控阵测控系统的外场测试，验证了方法的可行性和正确性。