高能超声辅助原位合成Al-Cr/Al复合材料

采用高能超声辅助铸造法制备Al-Cr金属间化合物/Al原位复合材料.利用扫描电镜观察复合材料中增强体颗粒的大小、形貌和分布,应用XRD、EDS对复合材料进行物相分析,并研究复合材料的硬度.结果表明:通过高能超声辅助铸造法制备的Al-Cr/Al原位复合材料中金属间化合物增强体颗粒呈多边形,尺寸较为细小,分布均匀;原位反应时Al和Cr首先生成Al0.983Cr0.017金属间化合物,随着Cr含量的增加,然后生成高Cr化合物;随着温度的升高,有利于更稳定、性能更好的化合物生成;这些金属间化合物会相互扩散,最终形成均匀的混合增强相,并保持Al,Cr的原子比例不变;复合材料的硬度随Cr含量的增加而增加,随Cr颗粒尺寸的增加而具有最大值,当Cr含量为10％,粒径为75 μm时,复合材料硬度增加了2.5倍.     

化学镀Ni-P合金涂层及其耐磨性

 对化学镀 Ni- P的硬度和耐磨性的关系进行了研究。低温长时加热可以获得高硬度 ,继续保温后其值不变。高温加热硬度达最大硬度以后保温硬度降低。不同温度处理其最大值相同 ,但耐磨性不同 ,高温处理优于低温处理。光电子能谱分析表明镀层表面富磷     

LY2铝合金的激光冲击强化区硬度和残余应力测试分析

为了研究激光冲击处理对LY2航空铝合金力学性能的影响,采用Nd:YAG激光器对航空铝合金LY2进行了激光冲击强化处理,测定其显微硬度和残余应力.结果表明,经过激光冲击处理后,试样表面没有受强脉冲激光和冲击波的破坏,而显微硬度和残余压应力明显提高,激光冲击处理后的强化区与光斑相当,深度约为1.2mm.     

ISO6507金属材料维氏硬度试验方法的测量不确定度评定实例

介绍了ISO6507金属材料维氏硬度试验方法的测量不确定度评定,并针对两种评定方法分别给出了评定实例。     

Development of microstructural inhomogeneity in multi-pass flow forming of TA15 alloy cylindrical parts

Revealing the development of microstructural inhomogeneity in the multi-pass flow forming of titanium alloy components is of great significance to the microstructure control and property tailoring. To this end, the microstructural inhomogeneity of TA15 alloy spun cylindrical parts was analyzed based on the deformation history. The results indicate that the material underwent significant compressive strain in the normal direction (ND), tension strain in the rolling and circumferential directions (RD and CD), while tension strain in the CD is slightly small due to the limited material flow in this direction. These strain characteristics make the microstructure, especially the primary α (α_p), present different morphologies in the different planes of the part. Meanwhile, the combined effects of inhomogeneous deformation and temperature distribution in the ND also cause the inhomogeneity of microstructure morphology and parameters in this direction. Quantitative analyses show that with the forming pass increasing, the aspect ratio of α_p increases most in the normal-rolling plane, then in the normal-circumferential plane and least in the circumferential-rolling plane, whereas α_p content decreases in an opposite trend. Along the ND, the aspect ratio and content of α_p is relatively high in the outer and inner surface areas but lowest in the central area, and these inhomogeneous characteristics can be gradually diminished with the forming pass increasing. Furthermore, the variation of hardness inhomogeneity factor indicates that a four-pass forming with the total reduction ratio of 63% could obtain a homogenous microstructure along the ND of the TA15 alloy spun cylindrical part.     

工件底孔直径对Q460高强度钢冷挤压内螺纹的影响

试验研究了工件底孔直径对Q 460高强度钢冷挤压内螺纹的影响,包括分析工件不同底孔直径下内螺纹牙形、表面残余应力、硬度及端面表面形貌的变化。结果表明,冷挤压加工后内螺纹端面堆积体呈两边高、中间低的凹陷形,随着工件底孔直径的减小,端面堆积的高度不断增加,堆积程度也就变得愈加严重,螺纹牙顶、牙侧与牙根处表层硬度与表面残余压应力均升高。工件底孔直径的选择,在正确保证螺纹质量和丝锥寿命的前提下应尽可能取最大值,但是,一般情况下没有必要过分要求最高的牙高率,否则将给内螺纹挤压成形带来许多困难。Q 460高强度钢冷挤压内螺纹的工件底孔直径最佳取值范围为21.20～21.30 mm,牙高率超过80%,完全符合螺纹质量要求。     

超声波硬度传感器在大口径管件内镀层硬度测量中的应用

通过分析超声波硬度传感器的特点,提出采用超声波硬度传感器技术实现对管件镀层硬度进行现场无损测量的方法.     

Radiation testing of a commercial 6-axis MEMS inertial navigation unit at ENEA Frascati proton linear accelerator

We present the first results of a novel collaboration activity between ENEA Frascati Particle Accelerator Laboratory and University La Sapienza Guidance and Navigation Laboratory in the field of Radiation Hardness Assurance (RHA) for space applications.The aim of this research is twofold: (a) demonstrating the possibility to use the TOP-IMPLART proton accelerator for radiation hardness assurance testing, developing ad hoc dosimetric and operational procedures for RHA irradiations; (b) investigating system level radiation testing strategies for Commercial Off The Shelf (COTS) components of interest for SmallSats space missions, with focus on devices and sensors of interest for guidance, navigation and control, through simultaneous exploration of Total Ionizing Dose (TID), Displacement Damage (DD) dose and Single-Event Effects (SEE) with proton beams.A commercial 6-axis integrated Micro Electro-Mechanical Systems (MEMS) inertial navigation system (accelerometer, gyroscope) was selected as first Device Under Test (DUT). The results of experimental tests aimed to define an operational procedure and the characterization of radiation effects on the component are reported, highlighting the consequence of the device performance degradation in terms of the overall navigation system accuracy. Doses up to 50 krad(Si) were probed and cross sections for Single-Event Functional Interrupt (SEFI) evaluated at a proton energy of 30 MeV.     

Al_2O_（3P）／Zn－Al复合材料的硬度与耐磨性能

研究了流变铸造法制备的Ａｌ２Ｏ３Ｐ／Ｚｎ－Ａｌ复合材料硬度和耐磨性能。结果表明Ａｌ２Ｏ３Ｐ的加入，提高了Ｚｎ－Ａｌ合金的室温和高温硬度，改善了其耐磨性能。颗粒体积含量增加，或者颗粒粒径的减小都将提高该复合材料的硬度和耐磨性，而试验温度的增加会引起其硬度的迅速降低。不过，Ａｌ２Ｏ３Ｐ的加入显著改善了Ｚｎ－Ａｌ合金耐高温性能。此外，文中还研究了淬火、回火或循环热处理对该复合材料硬度值的影响。     

钽的氮离子注入法研究

实验研究证实，通过氮离子注入的方法对钽基材进行表面强化，可大大提高钽村的表层硬度及耐蚀性能。俄歇电子能谱及Ｘ射线衍射分析表明，Ｔａ注入Ｎ＋后生成了新相ＴａＮｏ．１。