主成分分析用于近红外光谱定量测定高硅氧／酚醛预浸料树脂含量及挥发份含量研究

采用傅里叶变换近红外漫反射光谱技术分析了酚醛树脂固化过程的光谱变化,发现高硅氧/酚醛预浸料的近红外光谱经一阶导数处理后,被树脂信息掩盖的挥发份(乙醇)的光谱信息显露出来,由此采用处理后的光谱定量分析挥发份能取得更精确的结果。结合主成分分析法研究了高硅氧/酚醛预浸料树脂含量、挥发份含量的定量分析。结果表明,预浸料的第一主成分在树脂含量上有极高的正载荷。用主成分回归所建立的模型对未知样品预测,树脂含量和挥发份含量平均标准偏差分别为0.6114和0.1885。     

电子束固化高模量纤维增强复合材料力学性能研究

用湿法缠绕工艺制备了M40／EB99—1预浸料，研究了电子束固化高模量石墨化碳纤维M40增强EB99-1环氧树脂复合材料的常规力学性能、耐热疲劳性能和热物理性能，并与M40／5228、M40/4211等热固化复合材料的性能进行了比较。实验研究表明，除了剪切强度稍逊于热固化M40/5228复合材料外，其它常规力学性能都优于热固化M40／5228、M40/211复合材料，表现了较好的综合力学性能。电子束固化M40／EB99—1复合材料经冷热交变循环后的性能明显优于热固化M40／5228、M40/4211复合材料，表现了较好的耐热疲劳性能。     

纳米铝粉的活性评价方法研究进展

综述了纳米铝粉活性的2类评价方法:单质铝含量法和热分析参数法.单质铝含量的测定方法主要有气体容量法、氧化还原滴定法、热重分析法和透射电镜分析法,其中氧化还原滴定法又可分为重铬酸钾滴定法、水溶剂高锰酸钾滴定法、非水溶剂高锰酸钾滴定法及硫酸高铈法.基于热分析参数的活性评价方法主要采用:氧化起始温度、最大氧化速率、一定温度范...     

基于空间矢量脉宽调制的过调制策略研究

在电机控制中,过调制算法能够显著提高逆变器输出的电压,对提高电机转速有着重要意义。为了改善空间矢量脉宽调制对直流母线电压利用率不足的缺点,研究了基于空间矢量脉宽调制的单模式过调制算法,对输出电压基波幅值与其谐波含量进行理论分析。针对过调制区实际输出电压基波幅值与参考电压不一致这一问题,对目标调制比与给定调制比的关系作出可控性分析,作出拟合曲线并求出函数关系,最后对该过调制算法进行了仿真研究和试验验证。仿真分析和试验验证结果均证明了理论分析的正确性和可行性。     

A nonlinear background removal method for seismo-ionospheric anomaly analysis under a complex solar activity scenario: A case study of the M9.0 Tohoku earthquake

A precise determination of ionospheric total electron content (TEC) anomaly variations that are likely associated with large earthquakes as observed by global positioning system (GPS) requires the elimination of the ionospheric effect from irregular solar electromagnetic radiation. In particular, revealing the seismo-ionospheric anomalies when earthquakes occurred during periods of high solar activity is of utmost importance. To overcome this constraint, a multiresolution time series processing technique based on wavelet transform applicable to global ionosphere map (GIM) TEC data was used to remove the nonlinear effect from solar radiation for the earthquake that struck Tohoku, Japan, on 11 March, 2011. As a result, it was found that the extracted TEC have a good correlation with the measured solar extreme ultraviolet flux in 26–34 nm (EUV_26–34) and the 10.7 cm solar radio flux (F_10.7). After removing the influence of solar radiation origin in GIM TEC, the analysis results show that the TEC around the forthcoming epicenter and its conjugate were significantly enhanced in the afternoon period of 8 March 2011, 3 days before the earthquake. The spatial distributions of the TEC anomalous and extreme enhancements indicate that the earthquake preparation process had brought with a TEC anomaly area of size approximately 1650 and 5700 km in the latitudinal and longitudinal directions, respectively.     

Solar activity dependence of total electron content derived from GPS observations over Mbarara

Vertical total electron content (VTEC) observed at Mbarara (geographic co-ordinates: 0.60°S, 30.74°E; geomagnetic coordinates: 10.22°S, 102.36°E), Uganda, for the period 2001–2009 have been used to study the diurnal, seasonal and solar activity variations. The daily values of the 10.7 cm radio flux (F_10.7) and sunspot number (R) were used to represent Solar Extreme Ultraviolet Variability (EUV). VTEC is generally higher during high solar activity period for all the seasons and increases from 0600 h LT and reaches its maximum value within 1400 h–1500 h LT. All analysed linear and quadratic fits demonstrate positive VTEC-F_10.7 and positive VTEC-R correlation, with all fits at 0000 h and 1400 h LT being significant with a confidence level of 95% when both linear and quadratic models are used. All the fits at 0600 h LT are insignificant with a confidence level of 95%. Generally, over Mbarara, quadratic fit shows that VTEC saturates during all seasons for F_10.7 more than 200 units and R more than 150 units. The result of this study can be used to improve the International Reference Ionosphere (IRI) prediction of TEC around the equatorial region of the African sector.     

Response of the EIA ionosphere to the 7-8 May 2005 geomagnetic storm

In this paper, response of low latitude ionosphere to a moderate geomagnetic storm of 7–8 May 2005 (SSC: 1920 UT on 7 May with Sym-H minimum, ∼−112 nT around 1600 UT on 8 May) has been investigated using the GPS measurements from a near EIA crest region, Rajkot (Geog. 22.29°N, 70.74°E, Geomag.14°), India. We found a decrease in total electron content (TEC) in 12 h after the onset of the storm, an increase during and after 6 h of Sym-H deep minimum with a decrease below its usual-day level on the second day during the recovery phase of the storm. On 8 May, an increase of TEC is observed after sunset and during post-midnight hours (maximum up to 170%) with the formation of ionospheric plasma bubbles followed by a nearly simultaneous onset of scintillations at L-band frequencies following the time of rapid decrease in Sym-H index (−30 nT/h around 1300 UT).     

Seasonal dependence of TEC and SLAB thickness

Several years of hourly daily GPS measurements of the vertical total electron content (TEC) and of the equivalent slab thickness made at different European locations are analysed by using the linear regression technique to demonstrate the response of these two ionospheric parameters to seasonal variations. It is found that both TEC and slab thickness are highly correlated with season. Analytical relationships are determined expressing the seasonal dependence of the vertical TEC and of the equivalent slab thickness as a function of the seasonal parameter cos χ at noon in each location.     

库仑分析法测定岩矿石中的金

研究了氢醌库仑法测定金含量的方法、条件、考察共存离子的影响，并应用于岩矿石中金的分析。研究表明该法选择及结果都很好。     

Ionospheric TEC disturbances over China during the strong geomagnetic storm in September 2017

From September 7 to 8, 2017, a G4-level strong geomagnetic storm occurred, which seriously impacted on the Earth’s ionosphere. In this work, the global ionospheric maps released by Chinese Academy of Sciences are used to investigate the ionospheric responses over China and its adjacent regions during the strong storm. The prominent TEC enhancements, which mainly associated with the neutral wind and eastward prompt penetration electric field, are observed at equatorial ionization anomaly crests during the main phase of the storm on 8 September 2017. Compared with those on 8 September, the TEC enhancements move to lower-latitude regions during the recovery phase on 9 September. A moderate storm occurred well before the start of the strong storm causes similar middle-latitude TEC enhancements on 7 September. However, the weak TEC depletion is observed at middle and low latitude on 9–10 September, which could be associated with the prevailing westward disturbance electric field or storm-time neural composition changes. In addition, the storm-time RMS and STD values of the ionospheric TEC grids over China increase significantly due to the major geomagnetic storm. The maximum of the RMS reaches 12.0 TECU, while the maximum of the STD reaches 8.3 TECU at ~04UT on 8 September.