PEEK/ZrO2固体合金的探索研究

在聚醚醚酮(PEEK)玻璃化转变温度以下,用外动式高能旋转球磨机使PEEK和二氧化锆(ZrO₂)混合物反复变形、断裂和结合,并形成新的相,即形成PEEK/ZrO₂固体合金.通过扫描电镜(SEM)、差示扫描量热仪(DSC)、红外光谱(FT-IR)和动态热力学分析装置(DMTA)对PEEK/ZrO₂=1/2和2/1固体合金的结构及性能进行研究;并与纯PEEK对比,探讨PEEK与ZrO₂形成固体合金的可能性;讨论固体合金化工艺对PEEK/ZrO₂固体合金性能的影响,分析PEEK/ZrO₂固体合金的形成机理.     

GH150氩弧焊接头组织和力学不均匀性研究

研究了ＧＨ１５０合金对接氩弧焊接头显微组织和力学性能的不均匀性，用金相分析和微型剪切试验等方法得到了该焊接接头各区域的微观组织和力学性能分布特性。结果表明，该焊接接头中存在着比较严重的微观组织和力学性能不均匀性，其不均匀程度在熔合线附近最为严重。因而认为熔合区是该焊接接头力学性能最薄弱的部位。同时，由微型剪切试验所得到的力学性能梯度曲线还表明，ＧＨ１５０合金是一种高强度材料，其韧塑性却偏低；在焊接接头各区域中的强度指标变化不大，但是焊缝和热影响区的韧塑性比母材降低较多。其中，焊缝的剪切变形率降低２１．８％，剪切功降低２５．５％。     

TiAlB合金中初生TiB2的形貌及其形成机理

用原位自生法制备了Ti-53Al-xB合金,并用X射线衍射仪、扫描电镜对合金的相组成和微观组织进行了研究.结果表明:该合金主要由TiAl和TiB2两相组成;初生TiB2呈六面棱柱状,在TiAlB合金凝固过程中,Al原子富集在初生TiB2固-液界面前沿,导致固-液界面上B原子过饱和度不均匀性增加,使固-液界面变得不稳定, 从而在TiB2(0001)面上产生凸台或柱棒状分枝;分枝的各晶面取向与母体的取向一致,在初生TiB2(0001)面的凸台状或柱棒状分枝上能观察到清晰的台阶.     

Tool Life and Surface Integrity in High-speed Milling of Titanium Alloy TA15 with PCD/PCBN Tools

Titanium alloys are widely used in aeronautics that demand a good combination of high strength, good corrosion resistance and low mass. The mechanical properties lead to challenges in machining operations such as high process temperature as well as rapidly increasing tool wear. The conventional tool materials are not able to maintain their hardness and other mechanical properties at higher cutting temperatures encountered in high speed machining. In this work, the new material tools, which are polycrystalline diamond (PCD) and polycrystalline cubic boron nitride (PCBN) tools, are used in high-speed milling of Ti-6.5Al-2Zr-1Mo-1V (TA15) alloy. The performance and wear mechanism of the tools are investigated. Compared to PCBN tool, PCD tool has a much longer tool life, especially at higher cutting speeds. Analyses based on the SEM and EDX suggest that attrition, adhesion and diffusion are the main wear mechanisms of PCD and PCBN tools in high-speed milling of TA15. Oxidation wear is also observed at PCBN tool/workpiece interface. Roughness, defects, micro-hardness and microstructure of the machined surface are investigated. The recorded surface roughness values with PCD/PCBN tools are bellow 0.3 μm at initial and steady cutting stage. Micro-hardness analysis shows that the machined surface hardening depth with PCD and PCBN tools is small. There is no evidence of sub-surface defects with PCD and PCBN tools. It is concluded that for TA15 alloy, high-speed milling can be carried out with PCD/PCBN tools.     

Analytic estimation and numerical modeling of actively cooled thermal protection systems with nickel alloys

Actively cooled thermal protection system has great influence on the engine of a hypersonic vehicle, and it is significant to obtain the thermal and stress distribution in the system. So an analytic estimation and numerical modeling are performed in this paper to investigate the behavior of an actively cooled thermal protection system. The analytic estimation is based on the electric analogy method and finite element analysis（FEA） is applied to the numerical simulation. Temperature and stress distributions are obtained for the actively cooled channel walls with three kinds of nickel alloys with or with no thermal barrier coating（TBC）. The temperature of the channel wall with coating has no obvious difference from the one with no coating, but the stress with coating on the channel wall is much smaller than that with no coating. Inconel X-750 has the best characteristics among the three Ni-based materials due to its higher thermal conductivity, lower elasticity module and greater allowable stress. Analytic estimation and numerical modeling results are compared with each other and a reasonable agreement is obtained.     

航天用铝合金/ 焊丝焊接性研究

针对2A14、2219、2195、2A97、1460铝合金,通过焊接热模拟试验、焊接裂纹敏感性试验和拉伸试验,建立了材料脆性温度区间大小和焊接性的关系及焊丝主成分和焊接性的关系。结果表明,试验合金焊接性从好到差的排列顺序为2219、2A14、1460、2195、2A97。其中2A14、2219铝合金现用焊丝可以满足推进剂贮箱用铝合金焊接性要求。脆性温度区间较小时,焊接性良好,随脆性温度区间增加,焊接性变差;采用满足主成分含量之和为6%的焊丝焊接时,若抗裂性满足要求,则接头延伸率满足要求。     

Electromagnetic riveting technique and its applications

With the increasing applications of novel materials and structures in new-generation aircraft, conventional joining techniques in aircraft component assembly are greatly challenged. To meet those challenges, the electromagnetic riveting (EMR) technique was developed as an advanced joining tool, which exhibits obvious advantages in the assembly of new-generation aircraft. In this paper, the riveting principle of EMR was analyzed, and its development history and status were presented in detail. Then, equipment features of three typical EMR systems were given. Moreover, three important applications of EMR were covered, i.e., composite structure riveting, titanium rivet and large-size aluminum rivet riveting, and interference fit bolt installation. Specially, a novel strengthening method for mechanical linking holes based on EMR was also presented, which can significantly improve the fatigue behaviors of mechanical joints. Finally, open questions in the EMR field were discussed, and some recommendations for future work were also made. This paper can be useful for optimizing the joint designs of aircraft components and improving the level of aircraft maintenance.     

Cr对Nb-16Si-22Ti-2Al-2Hf合金显微组织与高低温力学性能的影响

 以Nb-16Si-22Ti-2Al-2Hf成分为基础,分别添加了2%和17%(原子分数,后同)的Cr元素替代Nb(分别称2Cr和17Cr合金),研究了Cr含量对Nb-16Si-22Ti-2Al-2Hf合金相组成、显微组织形貌、室温断裂韧性和高温强度的影响,分析了高低温失效机制。结果表明,铸态和1 375 ℃×100 h热处理后2Cr合金由Nbss和Nb₅Si₃两相组成;当Cr含量为17%时,出现了具有C15结构的Laves Cr₂Nb相,合金由Nbss、Nb₅Si₃和Cr₂Nb三相组成,热处理后在Nb₅Si₃中还析出了球状Cr₂Nb相。随着Cr含量由2%提高到17%,热处理合金的室温断裂韧性K_Q由14.32 MPa·m^1/2下降到10.30 MPa·m^1/2。合金强度与Cr含量的关系受温度影响,随Cr含量提高,室温和1 150 ℃时合金的硬度或强度增高,而1 250 ℃和1 350 ℃时合金强度降低。如1 150 ℃时2Cr和17Cr合金的屈服强度σ_0.2分别为349 MPa和387 MPa;1 350 ℃时分别为306 MPa和74 MPa。