太空原位制造和修复技术研究现状分析

概述了太空原位制造和修复技术（In—situ Fabrication and Repair,ISFR）的概念和特点,并结合该技术的发展背景,介绍了国内外以选择性激光烧结和电子束熔融技术为代表的太空原位制造、空间钎焊修复、太空基地建筑构建等方向发展现状及趋势。结合我国空间技术事业发展,提出充分借鉴国外相关技术成果,围绕主要应用材料,重点开展空间环境适应性和应用验证研究,并探索利用模拟月壤开展太空原位制造技术研究的设想与建议。     

亚微米晶NiAl-Al2O3复合材料的制备及其烧结-锻造短流程成形

以Ni粉和Al粉为原料,通过机械合金化和真空热压烧结制备了高致密的NiAl-5％Al2O3(体积分数,下同)复合材料,并利用烧结-锻造技术制成了该材料的前缘模拟件.机械球磨后,粉末颗粒充分细化,Ni和Al发生原位反应,并最终生成NiAl-5％Al2O3复合材料粉末.经1300℃真空热压烧结,获得致密的NiAl-Al2O...     

合金元素及第二相对钨的影响

综述了活化烧结元素,合金化元素,杂质元素及化合物对钨合金组织和性能的影响,并对新型钨基合金及其复合材料的研究、开发提出了一些看法。     

复杂陶瓷件烧结过程温度场数值模拟及仿真

随着陶瓷应用领域的不断扩展,对其品质要求也越来越高.而传统的设计工艺与制造过程是相分离的,到最终生产工艺的定型需要大量的反复修改.为解决传统陶瓷设计工艺只能依靠经验的现状,节约成本,缩短生产周期,故开发了复杂陶瓷零构件烧结过程计算机仿真软件.首先借助传热学原理来建立温度场模型,其次借助有限差分法处理温度场模型,编写出此仿真模拟软件的核心计算代码,从而实现了复杂陶瓷零件和组合构件烧结过程中温度场的模拟仿真.      

Preparation of bimodal grain size 7075 aviation aluminum alloys and their corrosion properties

The bimodal grain size metals show improved strength and ductility compared to traditional metals; however, their corrosion properties are unknown. In order to evaluate the corrosion properties of these metals, the bimodal grain size 7075 aviation aluminum alloys containing different ratios of coarse(100 μm in diameter) and fine(10 μm in diameter) grains were prepared by spark plasma sintering(SPS). The effects of grain size as well as the mixture degree of coarse and fine grains on general corrosion were estimated by immersion tests, electrochemical measurements and complementary techniques such as scanning electron microscope(SEM) and transmission electron microscope-energy disperse spectroscopy(TEM-EDS). The results show that, compared to fine grains, the coarse grains have a faster dissolution rate in acidic NaCl solution due to the bigger size,higher alloying elements content and larger area fraction of second phases in them. In coarse grains,the hydrogen ions have a faster reduction rate on cathodic second phases, therefore promoting the corrosion propagation. The mixture of coarse and fine grains also increases the electrochemical heterogeneity of alloys in micro-scale, and thus the increased mixture degree of these grains in metal matrix accelerates the corrosion rate of alloys in acidic NaCl solution.     

热压烧结型石油射孔弹药形罩的配方优化

介绍了一种制备石油射孔弹药形罩的新方法，采用粉末冶金热压烧结工艺制备石油射孔弹药形罩，并对药形罩的配方进行优化。试验结果表明采用该工艺制备的石油射孔弹药形罩品质较好。     

非金属电热膜材料及工艺分析

本文论述了制作电热膜的工艺过程.对电热膜的材料、烧结工艺及使用寿命进行了试验,获得了有价值的结论.并论述了提高电热膜产品寿命应注意的问题.     

电沉积烧结薄膜高温氧化性能研究

用电沉积烧结方法在１Ｃｒ１８Ｎｉ９Ｔｉ不锈钢表面形成铬、钇氧化物薄膜，通过研究比较不同沉积条件试样氧化层的高温氧化行为，发现１Ｃｒ１８Ｎｉ９Ｔｉ表面经铬、钇氧化物改性后抗高温氧化性能得到提高。     

烧结温度对高韧性Al2O3陶瓷断裂韧性的影响

针对一种通过球磨方法向初始原料氢氧化铝中添加晶种、采用热压方式烧结获得的高韧性Al₂O₃陶瓷材料,采用三点弯曲试件测定了不同烧结温度下的成组断裂韧度值,研究了烧结温度对该材料断裂韧性的影响规律,得出了断裂韧度随烧结温度增加有先升后降趋势,因而存在最佳烧结温度的结论.同时,通过不同烧结温度下瓷体表面显微结构的观察,分析了上述影响规律产生的机理.     

Effect of Sintering on Thermal Conductivity and Thermal Barrier Effects of Thermal Barrier Coatings

Thermal barrier coatings (TBCs) are mostly applied to hot components of advanced turbine engines to insulate the components from hot gas. The effect of sintering on thermal conductivity and thermal barrier effects of conventional plasma sprayed and nanostructured yttria stabilized zirconia (YSZ) thermal barrier coatings (TBCs) are investigated. Remarkable increase in thermal conductivity occurs to both typical coatings after heat treatment. The change of porosity is just the opposite. The grain size of the nanostructured zirconia coating increases more drastically with annealing time compared to that of the conventional plasma sprayed coating, which indicates that coating sintering makes more contributions to the thermal conductivity of the nanostructured coating than that of the conventional coating. Thermal barrier effect tests using temperature difference technique are performed on both coatings. The thermal barrier effects decrease with the increase of thermal conductivity after heat treatment and the decline seems more drastic in low thermal conductivity range. The decline in thermal barrier effects is about 80 °C for nanostructured coating after 100 h heat treatment, while the conventional coating reduces by less than 60 °C compared to the as-sprayed coating.