轧制变形对TiNiFe形状记忆合金组织结构及力学性能的影响

对不同变形量轧制和不同温度热处理的Ti₅₀Ni₄₇Fe₃合金的组织结构、力学性能进行了研究。X射线衍射结果表明,随着轧制变形量的增加,Ti₅₀Ni₄₇Fe₃合金在轧制方向上出现了择优取向;Ti₅₀Ni₄₇Fe₃合金的晶粒尺寸随着轧制变形量的增加而减小,随着热处理温度的升高而增大;Ti₅₀Ni₄₇Fe₃合金的抗拉强度和屈服强度随着轧制变形量的增加而增大,随热处理温度的升高而降低。     

High Temperature Flow Stress Prediction of Nano-Al_2O_3/Cu Composite Using an Artificial Neural Network

Alumina dispersion strengthened copper composite (nano-Al2O3/Cu composite) was recently emerged as a kind of potentially vi-able and attractive engineering material for applications requiring high strength, high thermal and electrical conductivities and resistance to softening at elevated temperatures. The nano-Al2O3/Cu composite was produced by internal oxidation. The microstructures of the composite were analyzed by the TEM and its hot deformation behavior was investigated by means of continuous compression tests per-formed on a Gleeble 1500 thermo-simulator. Making use of the modified algorithm–Levenberg-Marquardt (L-M) algorithm BP neural network, a model for predicting the flow stresses during hot deformation was set up on the base of the experimental data. Results show that the microstructures of the composite are characterized by uniform distribution of nano-Al2O3 particles in Cu-matrix. The sliding of dislocations is the main deformation mechanism. The dynamic recovery is the main softening mode with the flow stress decreasing gen-tly from 500 ℃ to 850 ℃. The recrystallization of Cu-matrix can be retarded late into as high as 850 ℃, when it happens only partially. The well-trained BP neural network model can accurately describe the influence of the temperature, strain rate, and true strain on the flow stresses, therefore, it can precisely predict the flow stresses of the composite under given deforming conditions and provide a new way to optimize hot deforming process parameters.     

Preparation and Microstructure of Highly-Oriented LaNiO_3 Thin Films by RF Sputtering Method

In an attempt of being used as buffer layers and electrodes for the textured BaTiO3 (BTO) ferroelectric thin films, highly (100)-oriented LaNiO3 (LNO) thin films of different thicknesses were deposited directly on Si (100) substrate with radio-frequency (RF) magnetron sputtering method. It is observed that the substrate temperatures and the film thicknesses bring main influences on the micro-structures and orientation of the thin film. The effects of the thicknesses and substrate temperatures on the orientation of the films were studied on the LNO films of different thicknesses. The highly (100)-oriented LNO thin films were obtained at the substrate temperature of 600 ℃. The existence of epitaxially grown BTO films indicates that the oriented LNO thin films obtained in this work could be used as a buffer layer for epitaxial growth.     

Ti3Al基合金及其与异种材料的连接研究现状

综述了耐高温轻质结构材料Ti3Al基合金及其与异种材料的连接研究现状，阐述了熔焊、钎焊、扩散焊、TLP扩散连接等主要连接方法的优缺点，指出了实用化研究方向。     

Cr3C2／Ni3Al复合材料的组织与耐磨性能

采用氩弧焊将Cr3C2-Al-Ni焊丝堆焊于碳钢表面制成Cr3C2/Ni3Al高温耐磨复合材料.利用电弧物理热与Ni,Al反应热在线生成复合材料,增强相尺寸由原料中150μm经溶解析出减小到平均10μm以下,组织均匀稳定.复合材料常温下耐磨粒磨损性能是传统高温耐磨合金Stellite12的2倍.分析认为,在硬度几乎相同情况下,增强相体积分数、增强相尺寸、Ni3Al形变硬化能力是决定复合材料在常温下耐磨粒磨损性能的主要因素.     

碳/碳复合材料与硬铝切削表面三维测量对比研究

针对各向异性复合材料切削表面粗糙度的测量与评定是国内外急待解决的问题，采用Talyscan150表面粗糙度测试仪对C／C复合材料和硬铝（LY12）切削表面粗糙度进行三维非接触测量。通过三维评定参数的对比，研究了C／C与LY12的切削表面粗糙度。结果表明：采用二维评定参数评定C／C的切削表面粗糙度将丢失表面的许多信息，三维评定参数可以更全面、更真实地表达复合材料切削表面粗糙度的特征。C／C切削表面和LY12切削表面在峰态分布以及表面纹理方面具有较大的差别。与LY12切削表面相比较，C／C切削表面有更多的深谷，而且表面没有明显的切削进给波纹。5q参数比5a参数能更好地表达复合材料切削时的纤维拔出与纤维露头的特征。     

三维编织复合材料的拉伸强度预测

采用有限微元方法分析了三维编织复合材料的模量与强度.提出了基于计算机模拟实验的三维编织复合材料的拉伸强度分析模型,利用Visual C++6.0实现了对三维编织复合材料拉伸强度的预测,预测结果与实验结果基本一致.     

定向凝固Ni3Al基高温合金IC6A的真空钎焊

用Co45CrNiWBSi,Co45NiCrWB及N300E三种钴基钎料对定向凝固Ni3Al基合金IC6A的真空钎焊进行探索研究,测定钎焊接头在900℃下的持久性能.试验结果表明,三种钴基钎料对IC6A合金钎焊工艺性能良好,均可获得致密完整的钎焊接头.但含元素Si和B的Co45CrNiWBSi钎料钎焊接头的高温持久性能较差,而仅以B作为降熔元素的N300E和Co45NiCrWB钎料钎焊的接头具有较好的持久性能,其中Co45NiCrWB钎料钎焊IC6A合金接头在900℃/160MPa下的持久寿命达100h以上.     

激光沉积制备Nb3Al基难熔金属间化合物研究

通过控制激光功率使Nb-12Ti-22Al(at%)和Nb-22Al(at%)两种成分配比的混合元素粉末在Ti-6Al-4V基体上激光沉积合成了Nb3Al基难熔金属间化合物,并达到了预期设定的成分配比,其显微组织均匀细小,在δ-Nb3Al基体上分布着不同形态的β-Nbss.在合适的激光功率下,无裂纹的沉积层厚度有一定的限制,随着沉积厚度的增加,沉积层中残余拉应力增大,沉积薄壁件容易在底部发生断裂.由于Ti的添加使Nb-12Ti-22Al的的裂纹倾向性小于Nb-22Al.     

电子束焊接线能量对Ti-24Al-15Nb-1Mo合金接头组织性能的影响

研究了电子束焊接不同线能量对合金接头组织、性能的影响机理,确定了具有比较满意的塑性和韧性的接头性能的电子束工艺参数选择窗口.结果表明,焊态下焊缝组织为残留β/B2相和包括次生α2相、O相以及ω相在内的β转变组织;焊接线能量增加,焊缝晶粒粗化, B2相的减少、初生α2的消失和ω相的产生以及β转变组织中次生的α2/O相集束增大并促进裂纹扩展是接头强度降低和脆变的主要原因.