一种用于电子薄膜导热系数和发射率测量的实验方案

薄膜传热性能对微电子设备的传热能力及其性能和可靠性有重大影响,测量薄膜的热物性参数并进一步研究其影响因素,可为微电子电路的设计和发展提供科学依据。评述了薄膜导热系数测量和研究的现状,在此基础上提出了一种新的能同时测量衬底薄膜导热系数和发射率的实验方案,并通过建立衬底薄膜试样传热的数学模型和分析推导,论证了该实验方案的可行性。本实验方案可推广应用于确定淀积在衬底薄膜上各种极小厚度薄膜的导热系数和发射率。     

3D-C/SiC复合材料拉-拉疲劳模量和电阻的变化

在室温最大应力为250MPa，应力比R＝0．1和频率为60Hz条件下，对3D－C／SiC复合材料进行了拉－拉疲劳试验。用共振法和电阻增量仪分别测试了杨氏模量及电阻的变化。结果表明：随循环次数增加，杨氏模量呈显著下降，缓慢下降和突然下降的变化规律。杨氏模量的下降大部分发生在疲劳循环的前600次。缓慢降低阶段约占疲劳寿命的94％以上，此阶段杨氏模量变化率与循环次数的对数近似呈线性关系，电阻变化率除首次循环降低外，随着循环次数增加一直在增加。增加规律大致可分为缓慢增加，台阶式增加和急剧增加三个阶段。材料的电阻变化率基本反映了纤维的损伤程度和破坏形式，可作为表征复合材料纤维损伤的有效参量。     

三维四向编织复合材料等效热特性数值分析和试验研究

 采用“米”字型枝状胞体有限元模型和试验方法对三维四向编织复合材料的整体等效热膨胀系数和等效热传导系数进行了分析并将计算结果和试验值进行了比较。研究表明枝状胞体模型能较为真实的反映三维四向编织复合材料的结构构形;有限元方法在分析热膨胀、热传导方面具有较好的精度;三维四向编织复合材料编织方向的热膨胀系数随着纤维体积比的增加而减小,随着编织角的增加而减小;热传导系数随着纤维体积比的增加而增大,随着编织角的增大而增大。     

梯度热障涂层的设计

 采用电子束物理气相沉积方法 (EB PVD)制备了梯度热障涂层,其结构设计为NiCoCrAlY粘结层 /Al₂O₃ YSZ过渡层 /YSZ陶瓷层。YSZ陶瓷层的结构为柱状晶结构,Al₂O₃ YSZ梯度过渡层为梯度微孔结构。采用有限元方法对梯度热障涂层进行热应力分析,优化了Al₂O₃ YSZ梯度过渡层的组成。计算结果表明,梯度涂层的内应力显著降低,而且界面及其附近应力和应变变化较平缓。过渡层厚度的增加有利于降低涂层内应力和缓和涂层界面处的应力集中。     

瞬态平面热源法热物理性能测量精度和适用范围的标定——常温下标准材料奥氏体不锈钢的热物理性能对比测试

瞬态平面热源法作为一种非稳态热物理性能测试技术，其测量范围、测量精度和试验参数的确定是正确评价和应用这种测试技术的前提条件。本文详细描述了采用瞬态平面热源法测量装置对热物理性能标准材料奥氏体不锈钢所进行的比对测试，并由此考察这种测试方法和测试装置的测量精度和适用范围。     

超细晶硬质合金加工机理及加工性能

围绕超细晶硬质合金精密磨削加工、在线电解修整磨削加工、电火花加工、超声复合加工、激光复合加工等加工方法,系统综述了超细晶硬质合金的加工机理和加工性能,并展望了超细晶硬质合金高效精密加工未来的研究重点。     

三元共掺杂对YSZ热障涂层热物理性能的影响

采用NiO、Er_2O_3、Yb_2O_3、Y-2O_3、ZrO_2粉末为原料,用高温固相合成法制备复合陶瓷材料,研究该复合陶瓷材料的比热、热扩散系数、热导率等热物理性能,并与传统8YSZ热障涂层材料进行对比。利用XRD测定所制备的陶瓷样块的晶体结构和物相组成,分析该陶瓷试样的物相组成及高温相稳定性。结果表明:NiO、Er_2O_3、Yb_2O_3共掺YSZ后,室温至1500℃范围内的热扩散系数为0.36～0.56 mm^2/s,与8YSZ相比,降低了约20%;室温至1500℃的热导率为1.45～1.55 W/(m·K),比8YSZ降低了18%;2EYNYSZ陶瓷材料具有单一的相结构,经1500℃热处理100 h之内不发生相变。     

微孔纳米板与陶瓷纤维板热导率对比研究

文摘采用非稳态热线法测试了微孔纳米板与陶瓷纤维板在RT~1 000℃区间热导率,利用SEM微观形貌与荧光光谱成分分析,结合微观导热机理对测试结果进行了分析。结果表明:纳米板热导率分布在0.03~0.1 W/(m·K)区间,纤维板为0.055~0.25 W/(m·K);两种材料热导率均随着温度升高而增大,且规律均为先缓后急,不同的是,纤维板热导率在300℃以后开始急剧增大,而纳米板在550℃之后才开始较快增长;纳米板整体上升趋势缓于纤维板,温度越高,两者热导率差异越大。分析认为纳米尺寸的固体颗粒及内部气孔是纳米板拥有低热导率的关键因素。     

Development of thermal sensors and drilling systems for lunar and planetary regoliths

We consider some novel concepts for thermal properties experiments aboard lunar landers or rovers, that may lead to an improved understanding of both the structure of the lunar near surface layers and the lunar thermal history. The new instruments could be developed using the experience and heritage from recently developed systems, like the Rosetta Lander thermal conductivity experiment MUPUS and existing designs used for terrestrial measurements of thermal conductivity. We describe shortly the working principle of such sensors and the main challenges faced when using them in the airless regolith layers of the Moon or other airless bodies. In addition new concepts to create appropriate drill holes for thermal and other measurements in the lunar regolith are discussed.     

Precipitation behavior and properties of extruded 7136 aluminum alloy under different aging treatments

In this work, the mechanical properties and electrical conductivity of the extruded 7136 aluminum alloy treated by single-stage aging treatment (T6), retrogression and re-aging treatment (RRA), and multiple retrogression and re-aging treatment have been investigated by means of hardness measurements, electrical conductivity tests and tensile tests. The results have shown that the properties of the 7136 alloy such as hardness, tensile strength and electrical conductivity were sensitive to retrogression time (within 90 min). With prolonging the retrogression time, the tensile strength was enhanced first and then decreased, yet the electrical conductivity was continuously increased. The 60 min-treated alloy performed the highest tensile strength (716 MPa), whereas the 90 min-treated alloy possessed the highest electrical conductivity (33.95%IACS). Compared with the T6-treated alloy, the tensile strength and electrical conductivity were improved by 3.3% and 18.9%, respectively. The electrical conductivity showed an obvious increase with repetitious times of the RRA treatment. After 3RRA60 treatment, a good combination of tensile strength (705 MPa) and electrical conductivity (33.20%IACS) can be obtained. Compared with the T6 condition, the tensile strength and electrical conductivity were improved by 1.7% and 16.3%, respectively. The mechanism of microstructure evolution under different aging treatments has been discussed in detail.