增材制造技术的研究应用进展:由3D到4D北大核心CSCD

增材制造技术是一种逐点、逐线、逐面增加材料而形成三维复杂结构零件的近净成形工艺,3D打印技术日渐成熟,其所制备出的产品组织结构致密、性能稳定。近年来,学者们将增材制造技术应用于智能材料的打印,实现该技术由空间维度到时间维度的扩展。本文重点介绍了3D打印与4D打印的研究现状与发展前景,以期为从事该领域的工作人员提供借鉴。     

多孔氮化硅高温氧化特性分析

采用TG-DSC、XRD、SEM、ICP 等分析手段,对某一典型多孔氮化硅样品进行4 个不同温度点的

静态和微动态连续氧化试验,最高氧化温度为1 400℃。结果表明:多孔氮化硅在0. 1 MPa 静态空气气氛下,

800℃之前,氧化反应非常微弱,800℃以上可见明显的氧化反应,1 000℃以上氧化反应加剧,增重速率加快,并

优先发生在表面与外部孔壁处,之后再发生在样品的内部孔隙处,氧化反应受界面处的化学动力学控制,以被

动氧化为主,主要生成物是SiO2,属吸热反应。当生成的SiO2 将氮化硅表面和孔壁处覆盖时,在其界面处,随

着温度的进一步升高或时间的延长,会生成Si2N2O,且需要注意防范样品可能出现脆性断裂情况。此外,同等

温度下,动态氧化气氛将加速氮化硅的氧化,特别是多孔和粉末状样品。

     

Biaxial tensile behavior of Ti-6Al-4V under proportional loading

The biaxial tensile behavior of isotropic Ti-6Al-4 V is characterized in this paper. A novel cruciform specimen was designed and optimized to achieve uniform stress and strain distribution within the gauge area. Biaxial tensile tests were conducted at three different loading ratios by the biaxial testing machine. The Digital Image Correlation (DIC) technique was applied to determine strain distribution, and a high-speed camera was employed to record the fracture process. An Inverse Analysis (IA) approach with a combined experimental and numerical method was proposed to determine the true stresses at the gauge section of the specimen during biaxial tensile tests. The results indicate that the initial yield locus can be described by the Cazacu criterion accurately, whereas the Mises criterion can predict better the strengthening behavior of Ti-6Al-4 V in the first quadrant in the principal stress space.     

TC4-DT钛合金线性摩擦焊接头组织特征及其形成机制

研究TC4-DT损伤容限型钛合金线性摩擦焊(linear friction welding,LFW)接头的组织特征及形成机制。利用光镜和扫描电镜对接头各区域微观组织进行表征,利用显微硬度计测试接头的显微硬度分布。结果表明:接头焊缝区(WZ)发生动态再结晶,焊接过程中WZ温度超过β转变点,焊后快冷的条件下发生了β→α′及β→α两种相变并析出了大量α′马氏体以及二次层片α;TC4-DT钛合金母材(BM)组织具有较高的变形抗力,使得接头形成的热力影响区(TMAZ)较窄。TMAZ内组织在强烈的热力耦合作用下拉长变形并破碎,焊后快冷的条件下析出少量α′马氏体及大量二次层片α;毗邻TMAZ的热影响区(HAZ)基本保留了BM不同位向的α集束的组织特征,但受热的影响α集束内α/β相界两侧元素相互扩散,层间β消耗,初生α长大;WZ组织的细晶强化和第二相强化,TMAZ组织的应变强化和第二相强化,以及HAZ内α相的长大使得接头上述区域显微硬度均高于BM。     

CFRP/TC4叠层结构制孔技术对比实验

因CFRP、TC4材料的物理性能差异较大，导致CFRP/TC4叠层构件切削性能匹配性较差，钻削过程中存在界面损伤、CFRP孔壁损伤难以调控的问题。针对上述问题，本文采用变参数啄式钻削工艺、变参数钻削工艺和恒参数钻削工艺对CFRP/TC4叠层结构进行了制孔实验，并对不同工艺条件下的轴向力、界面质量、TC4的切屑形态、CFRP层孔壁质量进行了对比分析。结果表明：相对于其他两种钻削工艺，在变参数啄式钻削工艺条件下，TC4材料层轴向力明显较高，产生短带状和短螺旋状切屑；CFRP层出口和入口处的孔径更接近于名义孔径，孔壁缺陷较少，表面粗糙度相对较小。     

Hardware qualification for scientific ballooning missions

The European Stratospheric Balloon Observatory (ESBO) initiative aims at simplifying the access to stratospheric balloon missions. We plan to provide platforms and support with instrument design in order to support scientists. During the design process, the inevitable question of qualification for the harsh flight conditions arises. Unfortunately, there is no existing standard for qualification of stratospheric ballooning hardware. Thus, we developed a qualification procedure for use within ESBO and similar projects.In this paper, we present our analysis of the environmental conditions in the stratosphere. While conditions at typical balloon float altitudes are similar to the space environment, there are also some relevant differences. For example, the thermal environment is dominated by radiation and thermal conduction, but the remaining atmosphere still supports a certain amount of convection. The remaining atmospheric pressure in the stratosphere also leads to reduced arcing distances. Vibrational loads are far less than for space missions, but quasi-static or shock loads may occur. The criticality of radiation increases with mission duration.Based on the environmental conditions, we present the qualification procedures for ESBO, which are based on the European Cooperation for Space Standardization (ECSS) standards for space systems. Overtesting against too high requirements leads to overengineering, driving mission cost and mitigating the advantages of balloons over space missions. Therefore, we modified the ECSS standards to fit typical scientific ballooning missions over several days at altitudes up to 40 km. Furthermore, we analyzed design rules for space systems with regard to their relevance for scientific ballooning, including material and component selection. We present the experience from the hardware qualification process for the ESBO prototype STUDIO (Stratospheric UV Demonstrator of an Imaging Observatory). Even though boundary conditions are different for each individual mission, we aimed for a broader approach: We investigated more general requirements for scientific ballooning missions to support future flights.     

TC4钛合金激光冲击强化数值模拟

采用连续显式动态冲击策略对航空用TC4钛合金进行激光冲击强化数值模拟研究.根据冲击波能量变化曲线确定单次冲击求解时间为3000ns,并分析了应力波传播过程.在此基础上开展多点冲击模拟,分析了功率密度、冲击次数和光斑搭接率对残余应力、应变场的影响.得出增加功率密度对增大表面残余压应力的效果更好;增加冲击次数对增大残余压应...     

电动膨胀循环液氧甲烷变推力发动机动态特性研究

电动泵压式液体火箭发动机受到了广泛的关注，然而电池有限的输出功率和过于沉重的质量成为限制电动泵压式发动机发展的重要因素。为此本文提出了一种电机驱动燃料泵和涡轮驱动氧泵的电动膨胀循环液体火箭发动机方案，并着重研究了该型发动机的动态响应特性。首先给出了20 kN级电动膨胀循环发动机的技术指标和部组件参数，进一步基于AMESim平台建立了全系统动力学模型，验证了方案的可行性和部组件动力学模型的准确性，并深入研究了单点工况和调节工况的动态响应特性。结果表明，针对启动过程而言，涡轮泵调整时间较电动泵长，这降低了系统响应速度，但工况越高，系统响应速度越快；高工况启动时，甲烷在冷却通道内的剧烈相变和跨临界状态的不连续物性相互耦合易引发系统振荡；就调节过程而言，推力调节时普遍存在超调或凹坑现象，且系统在两相同工况之间调节时，正调响应速度快于负调，这也导致阶跃幅值相等条件下的系统调整时间随目标工况升高而缩短。     

共沉淀法制备花状NiCo2O4及其吸波性能的研究

通过共沉淀法制备花状NiCo₂O₄吸波材料，利用XRD、FTIR、BET、XPS和SEM等方式表征了样品成分及形貌特征，将不同煅烧温度（300、400、500、600、700 ℃）的产物利用矢量网络分析仪通过同轴测试法模拟了不同厚度下的吸波性能。结果表明：400 ℃煅烧样品在反射损耗值、吸收带宽以及样品厚度都表现出较好的性能，当厚度为1.5 mm时，在14.32 GHz处吸波材料达到最大的吸收损耗值为-43.71 dB，有效吸收带宽为4.48 GHz （12.08~16.56 GHz），可以预见镍钴基吸波材料具有很大的潜力。     

Study of aerosol anomaly associated with large earthquakes (M>6)

We present the variation of unusual atmospheric phenomena, aerosols, to understand the preseismic irregularities for two major earthquakes in Japan. We consider aerosol optical depth and Angstrom exponent data retrieved from the Moderate Resolution Imaging Spectroradiometer (MODIS) instrument onboard the Terra satellite to establish possible connections between earthquakes and the generation of aerosols. Variation of the aerosol parameters shows significant changes before the April 15, 2016, Kumamoto earthquake ($M=7.0,h=10$ km) and the November 21, 2016, Fukushima earthquake ($M=6.9$ and $h=9$ km), where M indicates the Richter magnitude and h indicates the focal depth. To identify the source of the aerosol particles, we use the Hybrid Single-Particle Lagrangian Integrated Trajectory model (HYSPLIT-4). This model uses both Lagrangian and Eulerian approaches to compute trajectories and establish a source-receptor relationship. We compute backward trajectories to check whether the aerosol generated near the epicenter is due to the preseismic processes or is transported from other areas. From our results, we conclude the fine-mode aerosols are generated in the vicinity of the epicenter, 3–7 days before the earthquakes.