Thermal Fatigue Behavior of Ni_3Al Based Superalloy IC6E

The thermal fatigue behavior of Ni3Al based superalloy IC6E during the cycles between 900 ℃/1 000 ℃ and the room tempera-ture was investigated. The experimental results indicate that the primary and secondary thermal fatigue cracks initiate inside or round the borides and then spread away along grain boundaries and/or in interdendritic areas. The fracture of borides and their separation from the matrix at interfaces are mainly responsible for the crack initiation and its spreading. At temperatures higher than 1 000 ℃, the grain boundary oxidation combined with cyclic stresses accelerates the crack growth.     

Electrolytic Passivation of Nitinol Shape Memory Alloy in Different Electrolytes

The corrosion behavior of the nitinol alloy was studied in various corrosion media of different Cl–ion concentrations. The results demonstrate that the Cl–ion concentration has significant influences on the corrosion behavior of the nitinol alloy. In order to enhance the corrosion resistance, protective films were generated on the surface of the nitinol alloy by means of the electrochemical passivation method, for which five different electrolytic solutions were investigated. The surface analysis indicates full growth of all samples pas-sivated in the different electrolytic solutions with layers, however, showing different morphological features. Without any defects like micro-cracks and pores, the surface of the samples passivated in the molybdate solution turns out smoother and denser than those pas-sivated in other solutions. It is shown that the electro-chemical passivation will reduce Ni content but increase Ti content in the surface, reaching the Mole ratio of Ti:Ni=9.01:1 on the outermost surface. Potentiodynamic polarization test demonstrates that the samples electrochemically passivated in the molybdate solution present a significant increase in breakdown potential due to titanium enrichment on the outermost surface.     

Deformation Behavior of Mg-8 wt%Li Alloy under High-speed Impact

Deformation behavior of the Mg-8 wt%Li alloy at high strain rate was studied by means of the Split Hopkinson Pressure Bar (with strain rate of 103 s-1). It is found that shear localization proves to be the main damage mode for the alloy during dynamic loading. Strain and strain rate are the two necessary parameters affecting the occurrence of deformation and shear bands. Deformation bands begin to form when the strain and strain rate reach 0.20 and 1 900 s-1 respectively and will develop gradually with the strain rate increasing. Be-sides, deformation bands will transform into shear bands when the strain and strain rate reach above 0.25 and 3 500 s-1 separately.     

钛/铝异质金属搅拌摩擦焊技术研究进展

钛合金和铝合金均具有质轻、比强度高和抗腐蚀性能好等优点,已广泛应用于航空航天、军事工业和公共交通等领域,钛/铝异种金属复合结构的连接逐渐成为研究热点。然而,由于物理和化学性能差异明显,钛/铝焊接难度大,存在成形困难、接头性能较差等问题。搅拌摩擦焊作为一种固相焊接方法,对克服异种材料性能差异带来的焊接困难具有极大的优势。本文综述了钛/铝异质金属搅拌摩擦焊的研究现状,主要涉及焊缝成形、焊接参数、力学特征、冶金结合和连接机制等,以及衍生的搅拌摩擦焊新技术,为钛/铝异质金属结构的轻量化设计提供新思路,并对其未来发展进行了展望。     

钛合金加强框真空电子束焊接应用研究

钛合金加强框是飞机结构的重要构件,其在框段组合时机械连接与潜弧焊焊接方式均存在不足。真空电子束焊接(EBW)是实现钛合金框段组合的新型制造方式,具有显著优势。采用"积木式方法"展开系列试验研究:首先针对不同热处理制度下的TC4-DT焊接试样进行拉伸试验,通过标的参数对比获取合理的焊后热处理制度;然后通过系列焊接标准试样拉伸试验、断裂韧度试验及裂纹扩展率试验,获取基础性试验数据,并对焊接性能进行判断;最后经过短梁试验、部件试验以及机上应用,完成TC4-DT钛合金加强框EBW工程应用。结果表明:TC4-DT钛合金加强框EBW接头力学性能良好,较机械连接质量收益明显。     

扰流环对粉末发动机燃烧流动影响的数值模拟

为了提高粉末火箭发动机的燃烧效率,通过数值模拟方法研究了扰流环的有无、通径及位置对燃烧室燃烧流动特性的影响。结果表明:扰流环会增强Al颗粒和气相的掺混和换热程度,促进Al颗粒蒸发和燃烧,从而提高粉末火箭发动机的燃烧效率。当扰流环通径比在0.538~0.846范围内时,扰流环的通径越小,燃烧效率越高;当扰流环头部距离比在0.3~0.8范围内时,扰流环位置离头部越近,燃烧效率越高。设计扰流环时,应在距离燃烧室头部30%~40%的位置布置小通径的扰流环。      

GH3044合金堵盖高温氧化机理研究

为了研究固体推进剂燃气对GH3044合金堵盖的作用机理,通过光学显微镜、扫描电镜、硬度测试仪等手段对GH3044合金堵盖的孔洞进行测试与分析。结果显示:在氧化性气氛下,GH3044合金出现了沿晶界的择优氧化,形成了楔形裂纹,在热应力及氧化物长大的膨胀应力作用下发生剥落并最终形成喇叭形的烧蚀孔洞;其中,燃气中的金属氧化物(PbO)沿晶界与基体中的Ni发生氧化还原反应,形成低熔点的Pb-Ni共晶,进一步加剧了GH3044合金的高温氧化。     

铝合金壳体阳极化膜颜色异常分析

铝合金壳体在阳极化处理后表面阳极化膜存在颜色异常(发黑)现象。本文通过对壳体阳极化膜表面及基体形貌观察、金相分析和成分分析对发黑的原因进行了分析。结果表明壳体阳极化膜发黑的原因是由于该区域存在成分偏析(合金含量高),导致该区域的晶粒尺度比正常区域小、耐蚀性比正常区域差,膜层微观结构与正常区域存在差异,膜层内部化合物较多,致使该区域膜层呈现黑色。     

Al—7%Si合金综合处理及其力学性能的研究

在有效的熔体处理基础上,对Al-Si合金进行适当的微合金化处理,可明显提高Al-Si合金的力学性能,本文通过对Al-7%Si合金精炼,细化,变质处理后,加入Mg,Zr ,V等元素,使合金力学性能大幅度提高。     

基于最小加工表面裂纹的TiAl合金铣削参数优化

TiAl合金以其优异的性能被广泛应用于航空、航天制造领域,但由于TiAl合金自身的物理、化学特性,导致其切削性能较差,加工过程中容易出现工件表面烧伤、表面微裂纹等问题。为了研究TiAl合金铣削加工过程中切削工艺参数对加工表面裂纹的影响规律,设计了TiAl合金切削参数与加工表面裂纹之间的正交试验。结果表明:切削速度对TiAl合金铣削表面裂纹的影响最大,其次是切削深度和切削宽度,每齿进给量对表面裂纹的影响最小。基于遗传算法,以表面裂纹长度为目标函数,优化得到的最优参数组合为:ae=0. 2 mm、ap=0. 2003 mm/z、fz=0. 02001 mm/z、vc=20. 0004 m/min。采用优化后的参数铣削TiAl合金,发现工件表面的实际加工裂纹长度和经过算法优化的裂纹长度相差较小,该优化方法可行性较高,误差较小。