化学气相反应法在C/C复合材料抗氧化处理中的应用

通过把硅蒸气渗入预制体孔隙与碳直接反应生成SiC的化学气相反应(CVR)方法,提高初始密度和预制体结构均不同的C／C复合材料的抗氧化能力,研究了C／C复合材料的密度变化与微观结构,并对其进行了氧化试验。结果表明,因CVR温度、C／C复合材料初始密度不同,抗氧化处理后的密度增加量有显著不同。针刺炭布C／C／SiC复合材料在马福炉中于1160℃经65min氧化后,其失重率仅2．6％,而密度为1．95g／cm^3的同结构C／C复合材料相在同条件下失重率高达32％。     

SiC/CVD SiC复合涂层的抗氧化及抗热震性能研究

为了提高C/SiC复合材料耐高温性能,采用泥浆浸渍裂解与真空化学气相沉积(CVD)在材料表面制备了SiC/CVD SiC复合涂层,通过XRD、SEM分析了涂层组成与结构;研究了复合涂层的高温抗氧化(700～1 500℃)和抗热震性能。结果表明,泥浆浸渍法制备的SiC涂层具有一定的封孔效果,可使材料开孔率下降,但高温抗氧化效果并不佳,1 200℃氧化10 min后材料弯曲强度保留率下降明显仅有86%。CVD SiC涂层结构致密,与SiC封孔涂层结合较好,在700～1 500℃具有较好的抗氧化效果,随着氧化温度的升高,氧化后涂层完好,表面O元素逐渐增加,材料失重率缓慢增加但不大于0.5%,且材料性能并未下降。涂层材料在1 200℃-10 min短时热震5次后材料弯曲强度保留率仍有95%以上,且未出现开裂、剥落等热震损伤。在1 200℃-30 min长时热震10次后,涂层材料基本被完全氧化,材料失去保护作用,弯曲强度下降至90%左右。     

Influence of pre-tension on ballistic impact performance of multi-layer Kevlar 49 woven fabrics for gas turbine engine containment systems

In this paper, ballistic impact tests on wrapped multi-layer Kevlar 49 woven fabric systems were carried out with a flat blade projectile to investigate the impact response during a fan blade out event. The influences of the number of Kevlar layers and pre-tension were discussed particularly. Test results were used to analyze failure modes and energy absorption characteristics of multi-ply Kevlar fabrics. Results show that there are two kinds of impact damage for fabrics: global deformation mainly involving stretching of yarns in the impact region and fabric wrinkle from both sides to the impact zone, and local damage characterized by yarn fracture, yarn pull-out, and yarn unraveling. The energy absorption capability of Kevlar 49 woven fabrics improves with the number of fabric layers. The energy absorbed by multi-layer fabrics increases slightly at the beginning and then decreases substantially with pre-tension. The work in this paper can provide guidance for designing light-weight multi-layer fabrics containment systems.     

高频噪声场中薄壁结构响应的预估

本文用统计能量分析(StatisticalEnergyAnalysis简称SEA)法研究了在高频宽带随机噪声场中板及加筋板(航空航天器用蒙皮)的加速度响应。发现,在高频段同样外场激励情况下,加筋板的响应大于光板的。本文解释了这一用质量定理无法解释的现象,并用叠加法确定了复杂结构加筋板的模态密度、辐射阻抗和输入功率。     

混杂复合材料层合板抗冲击性能研究

为了探究复合材料层合板在实际应用中因承受冲击载荷而造成的结构安全问题,本研究采用实验和仿真相结合的方法,首先探究冲头形状对复合材料层合板损伤机理的影响,然后结合不同冲击能进一步揭示层合板的承载力和能量吸收变化规律。结果表明,相同冲击能下,层合板的损伤范围和承载力随着圆锥头、半球头、平头依次增加;相应的层合板的临界穿透能量随着圆锥头、半球头、平头依次增大;冲头形状和冲击能对层合板的吸能能力有较大的影响。     

热处理温度对硬铬镀层性能的影响

研究了热处理温度对硬铬镀层性能的影响.发现经过200～300℃1*#h热处理,镀层硬度明显提高,耐磨性得到改善,但硬度和耐磨性的最优点对应不同的热处理温度.对镀层XPS分析表明,热处理过的镀层中有有机碳化物析出.对镀层的EDAX分析表明,热处理使镀层表面氧含量增高,但对镀层微裂纹数量和宽度没有明显影响.对镀层的XRD实验结果表明,热处理后镀层的晶体结构未发生改变.     

某飞机上航炮的黑色磷化液的研究

飞机上常用的航炮要求具有优良的综合力学性能和抗腐蚀性能,一般都需要进行磷化处理和发蓝处理。介绍一种黑化装饰效果及抗蚀性好的钢铁件磷化液,其由黑化液和磷化液两部分组成部分。经飞机上航炮的试验研究表明：用该黑色磷化液处理后,既起到磷化的效果又进行了发黑处理;生成的黑色磷化膜,色泽乌黑纯真,并且有良好的稳定性和极强的抗蚀性能。     

Investigation on Thermal Contact Conductance Based on Data Analysis Method of Reliability

The method of reliability is proposed for the investigation of thermal contact conductance (TCC) in this study. A new definition is introduced, namely reliability thermal contact conductance (RTCC), which is defined as the TCC value that meets the reliability design requirement of the structural materials under consideration. An experimental apparatus with the compensation heater to test the TCC is introduced here. A practical engineering example is utilized to demonstrate the applicability of the proposed approach. By using a statistical regression model along with experimental data obtained from the interfaces of the structural materials GH4169 and K417 used in aero-engine, the estimate values and the confidence level of TCC and RTCC values are studied and compared. The results show that the testing values of TCC increase with interface pressure and the proposed RTCC model matches the test results better at high interface pressure.     

双酚B型氰酸酯的制备与性能

研究了碱性催化法合成非晶态双酚B型氰酸酯的制备工艺,利用红外光谱(FTIR)、核磁共振(NMR)、热分析(DSC)、流变仪等方法分析了双酚B型氰酸酯的结构性能和工艺特性,研究和测试了树脂固化物介电性能、耐热性能和力学性能.研究结果表明,制备的双酚B型氰酸酯纯度高,200 ℃时的凝胶时间在100 min以上;该型氰酸酯具有较低的粘度(η_25℃=470 mPa·s,η_40℃=210 mPa·s),适于室温树脂传递模塑(RTM,Resin Transfer Molding)成型工艺;250 ℃固化后的介电常数为2.75,介质损耗角正切0.007(10 GHz),玻璃化转变温度299 ℃,弯曲强度174 MPa,模量3.2 GPa,综合性能优异.     

源表法检定标准电阻

介绍了源表法检定全套标准电阻的工作原理、方法及不确定度分析,并对此方法进行了验证。