Ti3Al基合金微弧氧化膜的制备和性质

利用微弧氧化方法在Ti3Al基合金上制备了厚度达120 μm的陶瓷膜.研究了陶瓷膜的生长曲线,发现膜层厚度随着氧化时间的增加而增加,在不同氧化阶段生长速度不同,膜层以向外生长为主;显微结构和硬度分析都发现,陶瓷膜分为两层结构,即内层和外层,陶瓷膜内外层的主要物相是(Ti0.6Al0.2Nb0.2)O2相,外层中还有一定数量的无定形SiO2相;陶瓷膜的最大显微硬度可以达到基体硬度的3倍左右.显微划痕实验表明:膜与基体间结合力大于40N,膜与基体结合良好.电化学极化曲线测试显示陶瓷膜在3.5%盐水溶液中的耐蚀性与Ti3Al基体相比有较大的提高.     

一种新型三维仿生扑翼机构设计与分析

以昆虫翅膀运动机理为基础,提出了一种复合3种运动的仿生扑翼新机构。由于能使翼尖按8字形或香蕉形运动及机翼扭转,同时可保证两翼的运动对称,使扑翼运动更符合昆虫运动形态。为了实现生物运动轨迹,建立了机构参数的优化模型,并据此设计了扑翼微型飞行器样机,其扑动规律能更逼真地模拟昆虫翼的扑动形态,为新型微型飞行器的设计提供样机。     

铣削加工透波性Si3N4陶瓷表面质量研究

为了探索透波性Si3N4陶瓷铣削中加工表面创成机理及加工工艺参数对其影响规律,对加工表面形貌和边缘破损特征,以及加工参数与切削力、表面粗糙度、边缘破损的映射关系等开展了试验研究。首先对加工表面形貌进行了分析,由于存在陶瓷粉末去除和破碎性颗粒去除两种形式,造成加工表面形貌结构一种体现为变化平缓,而另一种包含微裂纹、层状结构体等,且存在凹坑、沟槽等缺陷。其次研究了边缘破损形式及产生机理,当刀具运动到出口棱边处,刀尖应力集中处将产生微裂纹,并向工件侧面扩展,从而在加工表面和加工侧面诱导形成边缘破损。最后基于均匀设计试验,分析了工艺条件对加工性能的影响。结果表明:随着切削深度从0. 2增加到0. 5 mm和切削宽度从1增加到4 mm时,x轴切削力呈耦合增长,y轴切削力呈二次方增长;当切削深度和切削宽度分别为0. 2 mm和1 mm、进给速度为500 mm/min时,加工表面粗糙度值最小;转速为2 000 r/min、切削深度和切削宽度最小时,边缘破损幅值最小。此结果可为提高透波性Si3N4陶瓷铣削加工质量提供技术支撑。     

模拟月壤激光熔融成型工艺参数试验初探

月壤3D打印可以实现月球的原位资源利用,有望成为月球基地建设和持久运营维护的关键技术手段。文章综述了模拟月壤激光3D打印方法的研究现状,搭建了以CUG-1A模拟月壤为原料的激光熔融成型原理试验系统,并开展了常规环境工艺参数的初步试验。结果显示：激光功率和扫描速度影响激光熔融深度和直径,是模拟月壤激光熔融成型的关键工艺参数;模拟月壤熔融成型过程易出现孔洞、球化等典型缺陷,需要进一步对月壤激光相变机理和上述成型工艺参数进行解析优化。     

Initial virtual flight test for a dynamically similar aircraft model with control augmentation system

To satisfy the validation requirements of flight control law for advanced aircraft,a wind tunnel based virtual flight testing has been implemented in a low speed wind tunnel.A 3-degree-offreedom gimbal,ventrally installed in the model,was used in conjunction with an actively controlled dynamically similar model of aircraft,which was equipped with the inertial measurement unit,attitude and heading reference system,embedded computer and servo-actuators.The model,which could be rotated around its center of gravity freely by the aerodynamic moments,together with the flow field,operator and real time control system made up the closed-loop testing circuit.The model is statically unstable in longitudinal direction,and it can fly stably in wind tunnel with the function of control augmentation of the flight control laws.The experimental results indicate that the model responds well to the operator's instructions.The response of the model in the tests shows reasonable agreement with the simulation results.The difference of response of angle of attack is less than 0.5°.The effect of stability augmentation and attitude control law was validated in the test,meanwhile the feasibility of virtual flight test technique treated as preliminary evaluation tool for advanced flight vehicle configuration research was also verified.     

Improvement and application of Y2O3 directional solidification crucible

In order to satisfy the drastic temperature change and high chemical activity in directional solidification of Nb–Si based alloys, Y_2O_3 crucible is demanded to possess high thermal shock resistance and erosion resistance. This paper improved the sintering degree and density of Y_2O_3 crucible by optimizing the sintering temperature and time, and its practical application performance was investigated. Y_2O_3 grains gathered with the increase of sintering temperature and time, and the contact area enlarged, resulting in the open pores being changed into closed pores.The higher density caused the improvement of erosion resistance of Y_2O_3 crucibles. However, excessive density weakened the thermal shock resistance. Considering high-temperature strength, erosion resistance, thermal shock resistance and costs, optimum sintering temperature and time of Y_2O_3 directional solidification crucible were 1800 °C and 120 min, respectively, and the porosity was20%. Improved Y_2O_3 crucible has been successfully applied to directional solidification of Nb–Si based alloys, and significantly reduced the oxygen contamination. Slight interaction occurred between Hf and Y_2O_3, but no obvious dissolution, penetration or erosion was found, showing good erosion resistance and thermal shock resistance.     

多用酸洗缓蚀剂DSCH-1的研究

由含氮的脂肪胺、芳香胺等多种常用的有机缓蚀剂复配制成的ＤＳＣＨ－１ 缓蚀剂,在硝酸中对２０＃ 锅炉钢和紫铜的缓蚀效率达９９．７％ ,在盐酸中对２０＃ 锅炉的钢的缓蚀效率达９８．５％ ,对紫铜的缓蚀效率也较高。Ｆｅ３＋ 离子浓度对ＤＳＣＨ－１ 缓蚀性能有较大的影响     

苄氯法合成α-AlH3及其表征

在乙醚-甲苯混合溶剂中,苄基氯和LiAlH4反应生成AlH3乙醚络合物。此络合物在甲苯介质中脱醚得到α-AlH3。通过X射线衍射、元素分析、扫描电镜及热分析,对样品进行表征。测试结果表明,此方法得到的α-AlH3晶体纯度高,Cl含量低,形貌完整,颗粒均匀,产物的热力学性能优良。     

三维流场的光学C.T技术

本文介绍了三维流场光学Ｃ．Ｔ技术的原理，实验方法和重建算法，给出了计算机模拟研究的方法和应用实例。     

Energy absorption features of 3-D braided rectangular composite under different strain rates compressive loading

There are huge potential applications of 3-D braided composite in aerospace engineering because of the non-delamination feature of the composite under impact loading. This paper presents the analysis of energy absorption features of 3-D braided composite under compression with different strain rates. The 3-D 4-step rectangular braided composite coupons were tested on a material tester MTS 810.23 and a split Hopkinson pressure bar (SHPB) apparatus to obtain out-of-plane and in-plane compression stress vs. strain curves at quasi-static and high strain rate state. The failure modes and energy absorption features of the 3-D braided composite under different strain rates were analyzed both in time domain and frequency domain. The energy absorbed by the 3-D braided composite increases with the strain rate. From fast Fourier transform (FFT) analysis of compression stress vs. time histories, the power of energy absorption of the 3-D braided composite increases with strain rate and mostly concentrate on the high frequency region. While for quasi-static compression, the power distributes in very narrow frequency region and also is less than that in high strain rates. This feature corresponds to the different damage and energy absorption mechanisms of the 3-D braided composite under quasi-static and high strain rate compression.