Preparation and Mechanical Properties of Glass Coats with High Temperature Radar Absorber

BaO-La2O3-B2O3 （BLB） glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the absorbing coat because it is considered to be a good high temperature absorber. The effect of the coating temperature and coating time on the tensile strength of the glass coat was investigated and the proper coating parameters to get good mechanical properties were determined. In addition, the effects of the SiCN content on the tensile strength of the absorbing coat were also discussed. Results show that it is possible to prepare the glass coat using the BLB glass as a binder. That the coat formed at 730℃ for 30 min has the best tensile strength witnesses 730 ℃, 30 min to be the proper parameter to prepare the glass coat. The BLB glass coat without SiCN powder possesses good tensile strength and the introduction of the SiCN absorber into the glass coat will lower the tensile strength. As the SiCN content increases, the tensile strength of the absorbing coat decreases, which could be attributed to the aggregation of SiCN in the coats.     

稠密气固两相流颗粒质量流量测量方法研究

为解决粉末火箭发动机和粉末冲压发动机供粉系统冷流标定过程中颗粒质量流量的测量问题,提出了一种稠密气固两相流中颗粒质量流量的测量方法,并基于旋风分离器和电子天平运用该方法设计了一套气固两相流中固体质量流量的测量装置,同时运用粉末火箭发动机的供粉系统对该测量方法和装置的测试性能进行了实验验证研究。结果表明:测量装置的粉末收集效率可高达98.5%以上,为固体颗粒的质量流量测量提供了保障;测量方法具有较好的可靠性和测量精度,其测量结果相对误差低于3%;测量方法具有较好的测量稳定性,重复性实验中测量结果相对误差低于2%;通过改变旋风分离器结构设计等参数,可拓宽测量方法的适用范围。     

真空聚苯乙烯泡沫绝热材料用于制冷保温节能效果的实验研究

通过对真空聚苯乙烯泡沫和聚胺脂进行对比实验和理论分析，证明了作为制冷保温绝热材料，真空聚苯乙烯泡沫的保温绝热效果明显优于聚胺脂。     

变形参数对挤压成型镍基粉末高温合金固溶热处理晶粒组织的影响

进行双锥体试样热模拟压缩实验,研究变形温度、应变速率及应变状态对一种挤压成型镍基粉末高温合金固溶热处理晶粒组织的影响,获得在变形温度 1060~1120 ℃,应变速率 0.003~0.3 s^-1 范围内,变形温度、应变速率与热处理晶粒组织的对应关系。结果表明:在相同应变量下,温度一定,应变速率越大,流变应力越大;应变速率一定,温度越高,流变应力越小;在相同应变速率下,较低变形温度的试样晶粒组织出现不均匀的现象;在相同的变形温度下,三种应变速率下的试样平均晶粒尺寸为 18~20 μm,但较大应变速率的试样明显出现不均匀晶粒组织。为获得均匀的晶粒组织,更适合的热变形参数为:变形温度 1120 ℃,应变速率 0.003 s^-1。在相同的变形温度和应变速率下,随局部应变的减小,平均晶粒尺寸呈逐渐增大的趋势。     

一种广义Bodner-Partom黏塑性本构模型

针对Bodner-Partom黏塑性本构模型描述合金材料的率相关塑性和循环硬化行为时精度不足的问题,在无屈服面统一黏塑性本构理论框架内对其进行了改进：利用塑性势函数重塑了流动法则,摆脱了Mises材料的限制;在内变量演化方程中引入塑性应变率修正项并由非线性因子控制,拓展了不同的硬化/恢复演变方向。利用FGH96合金在550℃下的单轴拉伸及低周疲劳试验数据将广义B-P模型与原始B-P模型进行了对比验证,结果表明本文模型的模拟效果与材料非弹性特征吻合良好,具有克服应力应变滞回曲线“过方”问题和表达平均应力循环松弛的能力。模型对不同硬化机制的考虑对于高温合金材料更具优越性。     

气相氛围中悬浮粉末燃料爆震燃烧研究进展

针对在氧化性气相氛围以及在燃料/氧化剂混合气相氛围中粉末燃料爆震燃烧波的传播特性,总结了气相氛围中悬浮粉末燃料爆震燃烧的实验和数值模拟研究进展,归纳了影响爆震波速度、稳定性、传播模式、细观结构和胞格尺寸的主要因素。同时,还介绍了粉末燃料应用于爆震发动机或燃烧室的案例;结合粉末爆震自身特点对实验装置和燃烧诊断测试手段和数值模拟方法进行总结分析;最后针对下一步需要开展的研究工作进行展望 。     

Effect of Processing and Composition on the Structure and Properties of P/M EP741NP Type Alloys

A study was carried out on the effects of processing and composition on the structure and properties of P/M EP741NP type alloys. The objectives of this study were to understand the role of Hf in a P/M superalloy containing high niobium used in aircraft engines and to determine the effects of extrusion and forging the powders as contrasted to HIPing (hot isostatic pressing) only. Two alloys of the P/M EP741NP composition were atomized: one alloy contained 0.26%Hf and the other was Hf free. After the as-atomized powders from both alloys were characterized, the powders were extruded into billets, forged and heat treated. After each process, the microstructures were characterized by SEM and the phases were extracted and identified by X-ray diffraction. The presence of Hf in the residues was probed by EDS (energy dispersive spectroscopy). The alloys were given the published Russian heat treatment as well as a more conventional heat treatment more typical of western powder alloys. Tensile, creep and stress rupture mechanical property tests were run. Results of the structural behavior of the alloys after each processing step will be presented and discussed. The role of the Hf on the mechanical proper- ties will be discussed.     

双性能粉末高温合金涡轮盘的研究进展

粉末高温合金由于在高温条件下表现出一系列优越的性能而成为制造高推重比航空发动机涡轮盘等热端部件的首选材料,特别是近年来对具有双晶粒组织的双性能涡轮盘不断深入的研究,使粉末高温合金应用前景更加乐观.本文论述国内外双性能粉末高温合金涡轮盘的研究进展,重点分析在制备中面临的问题,并对国内研制双性能涡轮盘提出建议.     

激光烧结快速成形试样强度的研究

研究了激光烧结快速成形试样密度与其静态强度的关系，烧结粉末中粘结剂含量、激光功率、激光束的扫描速度、扫描间隔以及扫描路径对试样弯曲强度的影响，分析了烧结过程中产生翘曲变形的原因，并通过三点弯曲实验测试了烧结试样的抗弯强度。     

置氢TC4钛合金粉末模压成形烧结机构及其动力学

通过建立正四面体的烧结模型,数学推导了置氢钛合金粉末烧结颈与烧结体相对密度的表达式,结合动力学实验研究了置氢TC4钛合金粉末模压成形固结加工过程中的动力学问题。结果表明:置氢TC4钛合金粉末烧结过程中的物质迁移机构由体积扩散为主的迁移机制向体积扩散和晶界扩散共同作用的物质迁移机制过渡,并由此得到了置氢TC4钛合金粉末材料模压成形固结过程的动力学方程,置氢量是影响置氢TC4钛合金粉末烧结体相对密度的最重要因素之一。