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Investigation on Thermal and Dimensional Stability of Epoxy Resin In-Situ Modified by Cyanate Ester Resin and Polydimethylsiloxane
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The thermal and dimensional stability of epoxy resin (EP) in-situ modified by cyanate ester (CE) and polydimethylsiloxane (PDMS) are investigated by means of experiments and numerical simulation. Thermal gravimetric analysis (TGA) and differential scanning calorimeter (DSC) are used to analyze the heat resistance of the modified EP. The dimensional stability is characterized by the volume shrinkage of the series PDMS/CE/EP obtained by the density method. The chemical structure of the PDMS/CE/EP is analyzed by Fourier transform infrared spectroscopy (FTIR). The results of TGA and DSC indicate that the thermal stability of PDMS/CE/EP decreases firstly and then increases with the increase in the amount of CE. The addition of PDMS shows a slight effect on the thermal stability. The 40% CE makes the blending system exhibit the lowest initial decomposition temperature, which reduces by 15.5% and 40.8% compared with pure EP and CE, respectively. The FTIR results suggested that the influence of CE on the thermal stability of the modified EP is mainly ascribed to the generation of oxazolidinone ring with low thermal stability and the increase in the triazine ring with high thermal stability. The volume shrinkage measurement results show that the introduction of CE and PDMS are both beneficial to the improvement of the dimensional stability of the blending systems. The in-situ addition of 80% CE shows the lowest volume shrinkage of 6.11%. The thermal stress distribution of PDMS/CE/EP generated during the solidification process is simulated by the finite element analysis. The results suggested that the introduction of 80% CE into EP results in the lowest thermal stress in the blending system, which indicates that the system has the lowest volume shrinkage, which agrees well with the experimental results. 相似文献
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分析了利用工业CT对固体火箭发动机缺陷进行检测的局限性,提出低温冷冻扩大脱粘间隙的方法,利用Ansys软件仿真了同一温度载荷作用下脱粘间隙和初始脱粘长度的关系.得出可以利用低温检测方法部分检测到冷冻前检测不到的脱粘。 相似文献
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跨声速风洞全模颤振试验悬浮支撑系统 总被引:2,自引:0,他引:2
介绍了用于CARDC的2.4m跨声速风洞全模颤振试验的悬浮支撑系统的组成、试验装置的结构及其特点、控制算法等。给出了风洞调试试验结果,并进行了简要讨论。试验结果表明,研制的悬浮支撑系统具有强度高,对模型的浮沉和滚转控制能力强等特点。 相似文献
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