藜蒿中绿原酸溶剂提取方法研究

应用醇溶剂回流法提取藜蒿中绿原酸，通过正交试验，对藜蒿中绿原酸进行溶剂提取条件的优化研究，并分剐讨论了各因素对绿原酸提取率的影响。实验表明，乙醇浓度70％、12倍的提取剂用量、温度85℃、提取时间4h、提取两次为乙醇溶剂提取藜蒿中绿原酸的最佳条件，总绿原酸提取率为1.24％。     

Optical identification of X-ray sources in the Einstein observatory medium and deep surveys

Methods are discussed for establishing the optical identification of X ray sources in the medium and deep X-ray surveys of the Einstein Observatory. Of the 63 X-ray sources with a statistical significance of 5 in the medium survey (Maccacaro et al. 1981), optical identification work is summarized for 51, of which identifications have been made with 30 active galactic nuclei. The optical properties of some of these X-ray selected objects are briefly discussed.The Einstein deep survey of Pavo (Griffiths et al. 1981) is used to illustrate the problems and methods used for securing optical identifications for X-ray sources in the deep survey fields. Identifications have been made with 4 QSOs at the bright end of the optical candidate distribution (together with 3 G stars) and it is shown that a further 7 fainter objects are also likely to be QSOs.     

The Resolution Performance of Range Estimators

The theoretical basis and methods of implementation of a moment algorithm for the range separation estimation of two closely spaced point targets are presented. Moment estimation and noise filtering techniques introduced here result in a considerable improvement over Baum's algorithm. The error bounds are established and it is shown that the spectral moment estimator exhibits optimum (zero bias, minimum variance) performance when the target separation normalized to the standard deviation of the Gaussian pulse is 2?1.5. Monte Carlo simulation is performed to verify the approximations made and to demonstrate the feasibility of the working models.     

Plasmaspheric Density Structures and Dynamics: Properties Observed by the CLUSTER and IMAGE Missions

Plasmaspheric density structures have been studied since the discovery of the plasmasphere in the late 1950s. But the advent of the Cluster and Image missions in 2000 has added substantially to our knowledge of density structures, thanks to the new capabilities of those missions: global imaging with Image and four-point in situ measurements with Cluster. The study of plasma sources and losses has given new results on refilling rates and erosion processes. Two-dimensional density images of the plasmasphere have been obtained. The spatial gradient of plasmaspheric density has been computed. The ratios between H⁺, He⁺ and O⁺ have been deduced from different ion measurements. Plasmaspheric plumes have been studied in detail with new tools, which provide information on their morphology, dynamics and occurrence. Density structures at smaller scales have been revealed with those missions, structures that could not be clearly distinguished before the global images from Image and the four-point measurements by Cluster became available. New terms have been given to these structures, like “shoulders”, “channels”, “fingers” and “crenulations”. This paper reviews the most relevant new results about the plasmaspheric plasma obtained since the start of the Cluster and Image missions.     

The Lunar Gravity Ranging System for the Gravity Recovery and Interior Laboratory (GRAIL) Mission

The Lunar Gravity Ranging System (LGRS) flying on NASA’s Gravity Recovery and Interior Laboratory (GRAIL) mission measures fluctuations in the separation between the two GRAIL orbiters with sensitivity below 0.6 microns/Hz^1/2. GRAIL adapts the mission design and instrumentation from the Gravity Recovery and Climate Experiment (GRACE) to a make a precise gravitational map of Earth’s Moon. Phase measurements of Ka-band carrier signals transmitted between spacecraft with line-of-sight separations between 50 km to 225 km provide the primary observable. Measurements of time offsets between the orbiters, frequency calibrations, and precise orbit determination provided by the Global Positioning System on GRACE are replaced by an S-band time-transfer cross link and Deep Space Network Doppler tracking of an X-band radioscience beacon and the spacecraft telecommunications link. Lack of an atmosphere at the Moon allows use of a single-frequency link and elimination of the accelerometer compared to the GRACE instrumentation. This paper describes the implementation, testing and performance of the instrument complement flown on the two GRAIL orbiters.     

The Galileo Dust Detector

The Galileo Dust Detector is intended to provide direct observations of dust grains with masses between 10^-19 and 10^-9 kg in interplanetary space and in the Jovian system, to investigate their physical and dynamical properties as functions of the distances to the Sun, to Jupiter and to its satellites, to study its interaction with the Galilean satellites and the Jovian magnetosphere. Surface phenomena of the satellites (like albedo variations), which might be effects of meteoroid impacts will be compared with the dust environment. Electric charges of particulate matter in the magnetosphere and its consequences will be studied; e.g., the effects of the magnetic field on the trajectories of dust particles and fragmentation of particles due to electrostatic disruption. The investigation is performed with an instrument that measures the mass, speed, flight direction and electric charge of individual dust particles. It is a multicoincidence detector with a mass sensitivity 10⁶ times higher than that of previous in-situ experiments which measured dust in the outer solar system. The instrument weighs 4.2 kg, consumes 2.4 W, and has a normal data transmission rate of 24 bits s^-1 in nominal spacecraft tracking mode. On December 29, 1989 the instrument was switched-on. After the instrument had been configured to flight conditions cruise science data collection started immediately. In the period to May 18, 1990 at least 168 dust impacts have been recorded. For 81 of these dust grains masses and impact speeds have been determined. First flux values are given.     

Galileo Photopolarimeter/Radiometer experiment

The Photopolarimeter/Radiometer (PPR) is a remote sensing instrument on the Galileo Orbiter designed to measure the degree of linear polarization and the intensity of reflected sunlight in ten spectral channels between 410 and 945 nm to determine the physical properties of Jovian clouds and aerosols, and to characterize the texture and microstructure of satellite surfaces. The PPR also measures thermal radiation in five spectral bands between 15 and 100 m to sense the upper tropospheric temperature structure. Two additional channels which measure spectrally integrated solar and solar plus thermal radiation are used to determine the planetary radiation budget components. The PPR photopolarimetric measurements utilize previously flown technology for high-precision polarimetry using a calcite Wollaston prism and two silicon photodiodes to enable simultaneous detection of the two orthogonal polarization components. The PPR radiometry measurements are made with a lithium tantalate pyroelectric detector utilizing a unique arrangement of radiometric stops and a scene/space chopper blade to enable a warm instrument to sense accurately the much colder scene temperatures.     

俄罗斯铝锂合金的研制和应用概况

本文介绍了俄国1420,1430,1450等铝锂合金的研制过程和性能,并与西方类似合金进行了对比,同时还列举了铝锂合金在战斗机、运输机、民航机和直升机上作为结构元件和应用情况。     

Radial and meridional trends in solar wind thermal electron temperature and anisotropy: Ulysses

Ulysses plasma measurement from 1.15 to 5.31 AU and from S6.4° to S48.3° solar latitude are used to assess the trends in the solar wind thermal electron temperature and anisotropy. Improved spacecraft potential corrections and data products have been incorporated. The radial temperature gradient is steeper than in previous determinations, but flatter than adiabatic. When normalized to 1 AU, temperature decrease with increasing latitude. Little change in the average thermal anisotropy has been seen during the mission.     

SWE,a comprehensive plasma instrument for the WIND spacecraft

The Solar Wind Experiment (SWE) on the WIND spacecraft is a comprehensive, integrated set of sensors which is designed to investigate outstanding problems in solar wind physics. It consists of two Faraday cup (FC) sensors; a vector electron and ion spectrometer (VEIS); a strahl sensor, which is especially configured to study the electron strahl close to the magnetic field direction; and an on-board calibration system. The energy/charge range of the Faraday cups is 150 V to 8 kV, and that of the VEIS is 7 V to 24.8 kV. The time resolution depends on the operational mode used, but can be of the order of a few seconds for 3-D measurements. Key parameters which broadly characterize the solar wind positive ion velocity distribution function will be made available rapidly from the GGS Central Data Handling Facility.