2,6—二（5—叔丁基邻羟基苄基）—4—叔丁基苯酚合成方法的改进

本文以改进的方法通过二步合成了２,６－二（５－叔丁基邻羟基苄基）－４－叔丁基苯酚,在第一步,由对叔丁基苯酚和甲醛在碱性条件下合成２,６－二羟甲基－对叔丁基苯酚,产物未作完全纯化直接用于第二步反应;第二步反应以对甲苯磺酸作催化剂,与文献相比,总产率由１８％提高至４３％,处理更容易。     

带振荡上仰翼型分离流研究

对带振荡的快速上仰翼型的非定常分离流问题进行了计算研究。采用微分形式的动力学方程和积分形式的运动学方程相结合的有效方法,以及可用于有分离流动的Baldwin-Lom ax 湍流模型,精确地模拟大雷诺数大攻角下的复杂流场。依据流场的不同特点,使用分区方法进行计算,保证了计算精度,大大节省了计算时间。文中分析研究了非定常前缘强旋涡的演化过程和气动力的变化,探讨了不同上仰率和振荡频率对分离流动的影响     

固体超强酸TiO2／SO4^2—催化合成苹果酯—B

使用ＴｉＯ２／ＳＯ４＾－２为催化剂,催化乙酰乙酸乙酯和１,２－丙醇反应合成苹果酯－Ｂ。结果表明：使用该催化剂１．０ｇ,乙酰乙酸乙酯（０．０７７ｍｏｌ）与１,２－丙二醇摩尔比为１：１．２,环已烷１５ｍｌ,反应２．５ｈ,苹果酯－Ｂ产率达７３％。产品经理化检验确认。     

美国跨域作战体系研究

介绍了美国海军协同作战系统、空军先进作战管理系统等跨域作战理念,深入剖析了美军跨域作战体系的历史背景、武器构成、异构信息火力一体的体系,得出互操作平台在跨域作战的重要性.最后,总结了跨域协同体系发展理念和对我军相关系统建设的启示.     

Liquid-Solid Phase Equilibria of Nb-Si-Ti Ternary Alloys

To determine the liquid-solid phase equilibria of the Nb-Si-Ti ternary system, Nb-Si-Ti alloys of different compositions are prepared. By means of scanning electron microscopy （SEM）, X-ray diffraction （XRD） and electron probe microanalysis （EPMA）, the phases in the alloys, such as Si-based solutions, Ti（Nb）Si, Ti（Nb）Si2, Nb（Ti）Si2, Ti（Nb）5Si4, Nb（Ti）5Si3, Ti（Nb）5Si3, Nb（Ti）3Si and Nb-based solutions are identified, and the phase evolution is analyzed. As a result, the microstmctural and microchemical evidence provides a clear definition of the Nb-Si-Ti liquidus surface projection and indicates that the ternary phase diagram has seven transition reactions.     

自适应捷变频雷达干扰方法分析及其效果度量

对自适应捷变频雷达的抗干扰性能进行分析,探讨了干扰自适应捷变频雷达的主要技术,如宽带阻塞干扰、回答式干扰、扫频式干扰等,并在功率准则基础上提出了一种更为全面、实用的干扰效果度量方法,为自适应捷变频雷达的干扰评估提供了一种新途径.     

不合格测量设备的处置

不合格测量设备的处置是测量设备确认体系要素之一，在贯标中应建立相应的不合格测量设备处置管理程序，以实现对不合格测量设备进行有效的控制。     

A fiber-optic current sensor for aerospace applications

A robust, accurate, broadband, AC sensor using fiber optics that is being developed for space applications at power frequencies as high as 20 kHz is described. It can also be used in low- and high-voltage 60-Hz terrestrial power systems and in 400-Hz aircraft systems. It is intrinsically immune to electromagnetic interference (EMI) and has the added benefit of excellent isolation. The sensor uses the Faraday effect in optical fiber and standard polarimetric measurements to sense electrical current. The primary component of the sensor is a specially treated coil of single-mode optical fiber, through which the current-carrying conductor passes. Improved precision is accomplished by temperature compensation by means of signals from a novel fiber-optic temperature sensor embedded in the sensing head. The technology used in the sensor is discussed, and the results of precision tests conducted at various temperatures within the wide operating range as well as the results of early EMI tests are reported     

Au基六元合金中的Ni固溶体研究

本文运用TEM.EDS等微观分析手段对Au基六元合金中的Ni固溶体进行了研究。结果表明,Ni固溶体为f,c,c结构(a_(Ni)=0.355nm).经调幅分解形成的置换式固溶体,成分为65at％Ni,10at％Au,18at％Fe,7at％cr,与基体有如下取向关系:(11-1)_(Ni)∥(11-1)_(Au),[011]_(Ni)∥[011]_(Au)。Ni固溶体在合金中起界面强化和弥散强化作用。     

多光谱扫描仪的杂光计算

本文采用蒙特卡洛法计算太阳光进入星载光学系统的杂光数量级。并对一具体结构的多光谱扫描仪进行了计算，以确定其消杂光能力。对某些参数的变动也进行了计算，为设计和修改提供了依据