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为深入了解二硝酰胺铵(ADN)的热分解,为该氧化剂在推进剂中应用提供必要的技术保障和实验依据,采用热重分析法(TG)及差示扫描量热法(DSC),实验研究了氮气流量、合成中间体烷基羰基N-硝酰胺铵(AUN)及硝酸铵(AN)对ADN热分解过程的影响,并利用model-free isoconversional方法模ADN热分解过程的活化能曲线。结果表明:氮气流量和硝酸铵(AN)对ADN的热分解过程有显著影响,而AUN可使ADN热分解曲线产生肩峰,但基本不影响ADN的热分解过程。 相似文献
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Electron concentration and Hall mobility have been investigated in pure zinc oxide single crystals, while in the dark and under ultraviolet (UV) excitation. Mode of scattering in ZnO has been determined by studying the temperature dependence of various electrical parameters in the range from -170 to 120°C. It has been observed that the degradation to the crystals by UV irradiation is limited only to the surface layer and shows up only at relatively lower temperatures, which is in contrast to the degradation behavior in thin films and powders. 相似文献
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S. M. Krimigis D. G. Mitchell D. C. Hamilton S. Livi J. Dandouras S. Jaskulek T. P. Armstrong J. D. Boldt A. F. Cheng G. Gloeckler J. R. Hayes K. C. Hsieh W.-H. Ip E. P. Keath E. Kirsch N. Krupp L. J. Lanzerotti R. Lundgren B. H. Mauk R. W. McEntire E. C. Roelof C. E. Schlemm B. E. Tossman B. Wilken D. J. Williams 《Space Science Reviews》2004,114(1-4):233-329
The magnetospheric imaging instrument (MIMI) is a neutral and charged particle detection system on the Cassini orbiter spacecraft designed to perform both global imaging and in-situ measurements to study the overall configuration and dynamics of Saturn’s magnetosphere and its interactions with the solar wind, Saturn’s atmosphere, Titan, and the icy satellites. The processes responsible for Saturn’s aurora will be investigated; a search will be performed for substorms at Saturn; and the origins of magnetospheric hot plasmas will be determined. Further, the Jovian magnetosphere and Io torus will be imaged during Jupiter flyby. The investigative approach is twofold. (1) Perform remote sensing of the magnetospheric energetic (E > 7 keV) ion plasmas by detecting and imaging charge-exchange neutrals, created when magnetospheric ions capture electrons from ambient neutral gas. Such escaping neutrals were detected by the Voyager l spacecraft outside Saturn’s magnetosphere and can be used like photons to form images of the emitting regions, as has been demonstrated at Earth. (2) Determine through in-situ measurements the 3-D particle distribution functions including ion composition and charge states (E > 3 keV/e). The combination of in-situ measurements with global images, together with analysis and interpretation techniques that include direct “forward modeling’’ and deconvolution by tomography, is expected to yield a global assessment of magnetospheric structure and dynamics, including (a) magnetospheric ring currents and hot plasma populations, (b) magnetic field distortions, (c) electric field configuration, (d) particle injection boundaries associated with magnetic storms and substorms, and (e) the connection of the magnetosphere to ionospheric altitudes. Titan and its torus will stand out in energetic neutral images throughout the Cassini orbit, and thus serve as a continuous remote probe of ion flux variations near 20R
S (e.g., magnetopause crossings and substorm plasma injections). The Titan exosphere and its cometary interaction with magnetospheric plasmas will be imaged in detail on each flyby. The three principal sensors of MIMI consists of an ion and neutral camera (INCA), a charge–energy–mass-spectrometer (CHEMS) essentially identical to our instrument flown on the ISTP/Geotail spacecraft, and the low energy magnetospheric measurements system (LEMMS), an advanced design of one of our sensors flown on the Galileo spacecraft. The INCA head is a large geometry factor (G ∼ 2.4 cm2 sr) foil time-of-flight (TOF) camera that separately registers the incident direction of either energetic neutral atoms (ENA) or ion species (≥5∘ full width half maximum) over the range 7 keV/nuc < E < 3 MeV/nuc. CHEMS uses electrostatic deflection, TOF, and energy measurement to determine ion energy, charge state, mass, and 3-D anisotropy in the range 3 ≤ E ≤ 220 keV/e with good (∼0.05 cm2 sr) sensitivity. LEMMS is a two-ended telescope that measures ions in the range 0.03 ≤ E ≤ 18 MeV and electrons 0.015 ≤ E≤ 0.884 MeV in the forward direction (G ∼ 0.02 cm2 sr), while high energy electrons (0.1–5 MeV) and ions (1.6–160 MeV) are measured from the back direction (G ∼ 0.4 cm2 sr). The latter are relevant to inner magnetosphere studies of diffusion processes and satellite microsignatures as well as cosmic ray albedo neutron decay (CRAND). Our analyses of Voyager energetic neutral particle and Lyman-α measurements show that INCA will provide statistically significant global magnetospheric images from a distance of ∼60 R
S every 2–3 h (every ∼10 min from ∼20 R
S). Moreover, during Titan flybys, INCA will provide images of the interaction of the Titan exosphere with the Saturn magnetosphere every 1.5 min. Time resolution for charged particle measurements can be < 0.1 s, which is more than adequate for microsignature studies. Data obtained during Venus-2 flyby and Earth swingby in June and August 1999, respectively, and Jupiter flyby in December 2000 to January 2001 show that the instrument is performing well, has made important and heretofore unobtainable measurements in interplanetary space at Jupiter, and will likely obtain high-quality data throughout each orbit of the Cassini mission at Saturn. Sample data from each of the three sensors during the August 18 Earth swingby are shown, including the first ENA image of part of the ring current obtained by an instrument specifically designed for this purpose. Similarily, measurements in cis-Jovian space include the first detailed charge state determination of Iogenic ions and several ENA images of that planet’s magnetosphere.This revised version was published online in July 2005 with a corrected cover date. 相似文献
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Jessica M. Sunshine Michael F. A’Hearn Olivier Groussin Lucy A. McFadden Kenneth P. Klaasen Peter H. Schultz Carey M. Lisse 《Space Science Reviews》2005,117(1-2):269-295
The science payload on the Deep Impact mission includes a 1.05–4.8 μm infrared spectrometer with a spectral resolution ranging
from R∼200–900. The Deep Impact IR spectrometer was designed to optimize, within engineering and cost constraints, observations
of the dust, gas, and nucleus of 9P/Tempel 1. The wavelength range includes absorption and emission features from ices, silicates,
organics, and many gases that are known to be, or anticipated to be, present on comets. The expected data will provide measurements
at previously unseen spatial resolution before, during, and after our cratering experiment at the comet 9P/Tempel 1. This
article explores the unique aspects of the Deep Impact IR spectrometer experiment, presents a range of expectations for spectral
data of 9P/Tempel 1, and summarizes the specific science objectives at each phase of the mission. 相似文献