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使用微波等离子体技术(microwave plasma chemical vapor deposition,MPCVD)对膜厚100μm的(100)和(111)晶面金刚石膜进行刻蚀处理,研究其抗氧等离子体的行为。结果表明:(100)晶面刻蚀首先发生在晶棱晶界处,而(111)晶面金刚石的刻蚀首先发生在晶面处;30 min刻蚀后,(100)面金刚石有明显晶面显现,(111)面金刚石膜晶面不明显;60 min刻蚀后,(100)和(111)晶面金刚石膜的择优取向消失;(100)晶面金刚石特征峰的半高宽值(full width at the half maximum,FWHM)由刻蚀前的8.51 cm–1上升至刻蚀后的12.48 cm–1,(111)晶面金刚石FWHM值由8.74 cm–1上升至148.49 cm–1;(100)晶面金刚石膜刻蚀速率在40 min时为0.35μm/min,60 min时上升至1.34μm/min;刻蚀前期,(100)晶面金刚石膜具有更好的抗氧等离子体刻蚀能力,刻蚀后期其抗刻蚀能力与(111)晶面金刚石膜相似。 相似文献
293.
在以酒石酸钠为成膜剂的新型无氟环保电解液体系中对TC18钛合金进行阳极氧化,制备出一种钛合金阳极氧化膜。通过扫描电子显微镜和拉曼光谱仪分析了阳极氧化膜的形貌和相结构。采用电化学方法研究了阳极氧化后TC18钛合金的耐腐蚀性能。采用万能高频疲劳试验机进行高频疲劳试验。结果表明:膜层具有沟壑与鼓包的表面形貌。膜层具有非晶态、锐钛矿型及金红石型TiO2结构,可能有板钛矿TiO2结构。阳极氧化后TC18钛合金的耐蚀性有显著的提高。阳极氧化后TC18钛合金的拉伸性能与疲劳性能基本不降低,相比于传统硫酸-磷酸型阳极氧化,拉伸性能和疲劳性能得到了一定的改善。 相似文献
294.
The paper deals with state estimation problem of nonlinear non-Gaussian discrete dynamic systems for improvement of accuracy and consistency. An efficient new algorithm called the adaptive Gaussian-sum square-root cubature Kalman filter(AGSSCKF) with a split-merge scheme is proposed. It is developed based on the squared-root extension of newly introduced cubature Kalman filter(SCKF) and is built within a Gaussian-sum framework. Based on the condition that the probability density functions of process noises and initial state are denoted by a Gaussian sum using optimization method, a bank of SCKF are used as the sub-filters to estimate state of system with the corresponding weights respectively, which is adaptively updated. The new algorithm consists of an adaptive splitting and merging procedure according to a proposed split-decision model based on the nonlinearity degree of measurement. The results of two simulation scenarios(one-dimensional state estimation and bearings-only tracking) show that the proposed filter demonstrates comparable performance to the particle filter with significantly reduced computational cost. 相似文献
295.
It is urgent to carry out detailed research on storage performance of rubber sealing ring to get the criterion for its storage life. This paper acquires material ageing regularity by theoretical analysis and experimental confirmation. On this condition, failure mode and failure criterion of typical sealing structure is studied, and the failure mechanism is found. Thus by analyzing the stress distribution, the relationship between ageing state and sealing condition is established. Rationalization proposal is put forward and storage life of sealing ring is evaluated. The research mentionedabove has special reference to the design of sealing structures and can provide reference for prolonging their service life. 相似文献
296.
In this paper, a novel algorithm is presented for direction of arrival(DOA) estimation and array self-calibration in the presence of unknown mutual coupling. In order to highlight the relationship between the array output and mutual coupling coefficients, we present a novel model of the array output with the unknown mutual coupling coefficients. Based on this model, we use the space alternating generalized expectation-maximization(SAGE) algorithm to jointly estimate the DOA parameters and the mutual coupling coefficients. Unlike many existing counterparts, our method requires neither calibration sources nor initial calibration information. At the same time,our proposed method inherits the characteristics of good convergence and high estimation precision of the SAGE algorithm. By numerical experiments we demonstrate that our proposed method outperforms the existing method for DOA estimation and mutual coupling calibration. 相似文献
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