树脂基防隔热复合材料高温响应分析方法研究进展

针对树脂基防隔热复合材料高温条件下复杂的热/力/化学的多场耦合问题，从高温性能预报模型、高温响应求解方法和高温试验测试三方面进行了论述。详细介绍了研究树脂基防隔热复合材料高温响应相关的热解动力学模型、材料高温热物性及力学性能演化表征方法、材料高温响应模型的求解方法以及表征材料高温响应的多种高温试验测试手段。对上述研究方法的发展进行了评述，并对未来发展趋势进行了展望。本文有助于相关研究人员认识和发展树脂基复合材料在高温下的热力响应分析方法，也可供工程技术人员对这类材料的防隔热性能和高温承载性能进行研究。     

Service life prediction of AP/Al/HTPB solid rocket propellant with consideration of softening aging behavior

The aging behavior of softening composite solid propellant was investigated by measuring its mechanical and ballistic prosperities during prolonged storage at elevated and room temperatures. Accelerated aging was conducted at 65 °C for 231 days while the normal aging was performed at 25 ± 3 °C and relative humidity less than 50% for 8 years. The mechanical properties were obtained from uniaxial tensile tests for the aged propellant specimens while the ballistic properties were determined from static firing tests of subscale motors aged for 112 days at 65 °C. The mechanical results show that the maximum tensile strength and Young's modulus initially increase and subsequently decrease with increasing aging time, while the maximum tensile strain generally increases with increasing aging time. The ballistic properties like burning rate show a small change which cannot affect the ballistic performance. The experimental results show that the changes in the mechanical properties are significant during the aging period, but the burning rate does not undergo significant changes. From this study, it is observed that the propellant ages through a combination of reactions like post-cure, oxidative cross-linking, chain scission, and hydrolysis. The chain scission and the hydrolysis effect are the most significant process, which makes the propellant soft and extendible. The observed aging mechanism has been modeled using an exponential function with two terms which can describe the complex behavior of the aging. By applying Arrhenius equation,the activation energy values were obtained based on the propellant mechanical properties. The shelf life of this propellant formulation at 25 °C is predicted to be 13 years using the modulus as failure criteria and control parameter.     

Reflected Wavefront Modulation with Phase Array by Using Acoustic Metasurface

Acoustic metasurface has attracted increasing attention due to the ability of manipulating the transmitted and reflected phase of waves to generate various acoustic functionalities with planar layer of sub?wavelength structure.We design an acoustic metasurface with a semi?closed and nested slotted tube array,and it possesses the capacity of modulating the reflected phase with sub ? wavelength thickness(about λ/23). The reflected phase shifts can be obtained from 0 to 2π by different rotation angles of internal slotted tubes. The theoretical results agree well with the numerical results by a finite element method. The results show that some excellent wavefront manipulations are demonstrated with the phase array by using acoustic metasurface such as anomalous reflection and sub?wavelength flat focusing. The design may offer a path for acoustic manipulation and promote the potential applications of acoustic metasurface in low frequency noise control,acoustic imaging and cloaking.     

空心角隅棱镜在激光干涉测角中的应用

阐述了激光小角度测量装置中使用的实心角隅棱镜由于制造和安装误差对测量结果所造成的影响,同时提出利用空心角隅棱镜可以解决问题的理论依据,通过应用实验效果对理论给予验证.     

飞机横截面积分布的跨声速面积律验证

利用跨声速面积律对超声速飞机进行外形修形是飞机外形设计中的一项重要工作。本文基于对CATIA和EXCEL进行二次开发,利用Visual Basic语言编制出自动测量飞机横截面积分布的程序。通过在多个型号飞机外形设计中的应用,说明该方法对指导超声速飞机外形设计具有重要的指导意义。     

运载器式潜射导弹水面分离运动特性

基于分数容积障碍法(FAVOUR)、不可压缩Navier Stokes方程、RNG  k ε 湍流模型和VOF函数,建立了自由液面模型并与六自由度运动方程联合求解了运载器式潜射导弹的水面分离运动。通过数值计算结果与实验值对比，验证了计算模型的精度和有效性，进而对不同海况条件以及出水角度下潜射导弹的水面分离运动特性进行了对比研究。结果表明，各工况下运载器与导弹的质心位置、姿态角和轴向速度均处于稳定和发射安全允许范围内。但随着浪高的增加，导弹姿态角散布范围也明显增大。在5级海况下，运载器与导弹俯仰角的峰值达到22°。此外，相同海况下，若控制运载器以10°倾角出水，导弹分离后最终可以获得接近垂直的姿态。本文的数值分析方法能有效地用于预测运载器式潜射导弹水面分离过程。     

Distributed cooperative guidance for multiple missiles with fixed and switching communication topologies

This study investigates cooperative guidance problems for multiple missiles with fixed and switching directed communication topologies.A two-step guidance strategy is proposed to realize the simultaneous attack.In the first step,a distributed cooperative guidance law is designed using local neighboring information for multiple missiles to achieve consensus on range-to-go and leading angle.The second step begins when the consensus of multiple missiles is realized.During the second step,multiple missiles disconnect from each other and hit the target using the proportional navigation guidance law.First,based on the local neighboring communications,a sufficient condition for multiple missiles to realize simultaneous attack with a fixed communication topology is presented,where the topology is only required to have a directed spanning tree.Then,the results are extended to the case of switching communication topologies.Finally,numerical simulations are provided to validate the theoretical results.     

离子色谱法测定标准物质DIANP中的无机阴离子

采用离子色谱法对DIANP中无机阴离子NO2-,N3-,NO3-,CO32-,SO42-进行测定。乙腈溶解DI-ANP后,加水萃取无机离子,通过On GuardⅡRP柱,去除DIANP或其分解的有机产物,用氢氧化钾溶液为淋洗液梯度洗脱,流速为1.0mL/min,采用IonPac AS11-HC阴离子色谱柱进行分析。测定结果,5种阴离子相关系数达到0.999以上,相对标准偏差为1.57%～4.30%,NO2-,N3-,NO3-,SO24-加标平均回收率为89.3%～98.6%。该方法简便、快速,且结果满意。