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用气体雾化制粉技术成功制备了Ti-46Al-2Cr-2Nb-0.2B-0.1W球形预合金粉末,粉末中的氧和氢的质量分数分别为0.059%和0.001%,粉末的粒度呈正态分布,粒度主要分布在50-190μm。采用热等静压技术将该预合金粉末制备成了致密的TiAl系金属间化合物,组织比较细小、均匀,热处理后材料的延伸率达到了2.5%。 相似文献
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高铌钛铝合金的制备工艺 总被引:5,自引:0,他引:5
研究了高铌TiAl金属间化合物的材料制备工艺。结果表明,感应凝壳熔炼时的合金收得率远远小于自耗熔炼时的合金收得率,因此在熔炼过程中损失主要来自于感应熔炼过程,而感应熔炼过程中合金的损失主要来自于凝壳大小及合金熔液挥发的多少;高铌TiAl合金的成分波动主要是由于凝壳大小波动造成的,感应熔炼完成后合金的Al含量取决于凝壳和合金溶液挥发对合金Al含量的共同影响效果;高铌TiAl合金在熔炼过程中,Nb的含量是在逐渐增加的。经过1200℃,24小时均匀化退火可以消除原始铸态组织的枝晶偏析。 相似文献
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基于粉末热等静压近净成形技术,在930℃/120 MPa/3 h的条件下开展了TA7 ELI(超低间隙)高承压泵壳体的成形研究,通过两批次粒度存在差异的粉末(粉末表面为胞晶形貌,D50为67μm、74μm)分析了制粉时的粒度波动对成形材料力学性能的影响,并结合有限元仿真手段开展了高承压泵壳体的粉末收缩规律研究。此外,根据高承压泵在液体火箭发动机中的实际服役情况,对近净成形的高承压泵毛坯进行解剖,分析了特征截面位置的显微组织及硬度分布情况。结果表明,粉末热等静压近净成形技术制备的TA7 ELI合金力学性能达到锻件水平,粉末粒度波动对合金力学性能无显著影响,高承压泵壳体的显微组织均匀,特征截面的硬度值波动小,壳体内部流道关键尺寸实测结果与模拟预测结果的最大偏差为5.37%。 相似文献
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采用烧结 等温锻造的方法制备Ti-17粉末合金,对粉末合金制备过程中各工序的密度、显微组织变化规律等进行了试验研究.试验结果表明:经相同条件烧结后,-140目粉末烧结棒材和-80/ 140目粉末烧结棒材分别达到理论密度的98.06%和93.55%,在-80/ 140目粉末烧结棒材显微组织中观察到有大量的残留空隙存在.采用高低温等温锻造工艺能够有效去除粉末合金烧结后残留的空隙,提高合金的密度,使合金的显微组织得到显著细化和均匀化.烧结 等温锻造是制备优质粉末钛合金的有效方法. 相似文献
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采用数值模拟的方法对TiAl合金粉末的射频(radio frequency)等离子体球化过程进行研究,分析速度场和温度场对不同粒径TiAl合金粉末的运动轨迹及质量变化的影响。结果表明:粉体颗粒在等离子体的高温作用下温度急剧升高,表面蒸发导致粒径降低,太小的颗粒很快蒸发消失掉;在冷却塔下端,不同粒径颗粒的运动轨迹存在较大差异,小颗粒倾向于随气流进入气流出口,大颗粒落到冷却塔底部被收集;增大气流量会提高球化系统中的气流速度,导致在气流出口能被气流带走的颗粒粒径变大,收粉率降低;模拟得到TiAl合金粉末球化后的粉末粒径分布、平均粒径及收粉率等参数与实验结果比较接近,模型能够较好地符合实际球化过程。 相似文献
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郎泽保%崔玉友%王亮%徐磊%张绪虎 《宇航材料工艺》2007,37(6):70-73
成功制备了Ti-46Al-2Cr-2Nb-0.2B-0.1W(原子分数)球型预合金粉末,并对粉末的特性进行了研究。在随后的粉末冶金技术研究中,运用热等静压技术得到了组织细小、均匀的粉末TiAl系金属间化合物,但材料的伸长率很低。经热处理后,材料的伸长率达到了2.5%。 相似文献
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合金元素Y对高铌TiAl高温合金长期抗氧化性的影响 总被引:1,自引:0,他引:1
研究不同含Y量对高铌TiAl合金在900℃恒温条件下,1000h的抗氧化性的影响.结果发现,从长期看,氧化速率、氧化膜结构以及氧化膜抗剥落能力均与Y含量有关.在900℃等温氧化条件下,0.4 at%Y含量能有效提高高铌TiAl合金的抗氧化性,而高Y含量对与抗氧化性的负面影响在氧化初始阶段已经十分明显.通过对氧化后样品SEM和EDS分析发现,适量Y元素的加入可以细化氧化物颗粒,促使合金表面形成连续Al2O3保护膜,提高氧化膜与合金基体的粘附性,从而提高高铌TiAl合金的高温长期抗氧化性. 相似文献
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采用粉末热挤压法制备了一种Al-Zn-Mg-Cu超高强铝合金,研究了粉末粒度和挤压比对合金组织和力学性能的影响。结果表明,400℃挤压时,粉末中位径D50=28.38μm和挤压比λ=25可使挤压合金获得最好的力学性能,挤压合金经过460℃/2.5h水淬+120℃/24h空冷(T6)处理后的抗拉强度、屈服强度和伸长率分别为731MPa,670MPa和6.2%;晶粒细化是挤压合金力学性能随粉末粒度减小而提高的原因;挤压比λ为9~25时,挤压合金力学性能随挤压比增大而提高;λ=36时,挤压合金力学性能降低的原因是MgZn2析出相粗大和发生完全动态再结晶。 相似文献
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JING Mao-xianga * SHEN Xiang-qiana ZHOU Jian-xina LI Dong-hongb LI Wang-xingb aSchool of Materials Science Engineering Jiangsu University Zhenjiang China bZhengzhou Research Institute of Chalco Henan Zhengzhou China 《中国航空学报》2006,19(Z1)
Alumina-based composites containing 0-15wt% Ni metallic phase were produced by hot press-sintering Ni-coated alumina pow-ders. The Ni-coated alumina powders were prepared by the aqueous heterogeneous precipitation of alumina micro-powders and nickel sulfate salt followed by reduction process. The microstructural features and dispersion of Ni phase in Ni-coated alumina powders and the subsequent alumina-Ni cermets were investigated using scanning electron microscope (SEM), X-ray diffractometer (XRD), and trans-mission electron microscope (TEM). The relative density of the hot press-sintered composites was measured with the Archimedes’ method while the fracture strength and the fracture toughness were defined with the three-point bending method and the mi-cro-indentation fracture method. In the formation of alumina-Ni cermets from sintered Ni-coated alumina powders, Ni phase to some extent limits the densification rate and stifles the coarsening and growing process of alumina grains. The Ni phase is found to be located at the interfaces and the triple-joint junctions of alumina grains which results into alteration of the fracture mode of alumina and its in-creased fracture strength and fracture toughness if compared with monolithic alumina. 相似文献
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电子回旋共振离子推力器栅极光学系统的PIC/MCC模拟 总被引:2,自引:1,他引:1
为了寻求日益昂贵的电推力器工质氙气的替代品,探讨氩气作为电子回旋共振离子推力器工质的适用性,采用混合PIC方法模拟了氩等离子体在栅极光学系统中输运过程,分析了氩离子束流的聚焦效果、氩等离子体的空间分布和流动特性。结果表明:氩离子束流在已有栅极系统中具有良好的聚焦效果;束流中CEX离子仅占离子总数的万分之一,影响较小;氩气作为工质时,离子喷射速度为75km/s,加速栅极后回流速度为38km/s,与电动力学理论预估值一致。 相似文献
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Alan Burgess G 《航空制造技术》2004,(Z1):5-11
The use of fine powders in thermal spray can lead to many advantages. These advantages include denser coatings, coatings with increased wear resistance, coatings with smoother surface finish, coatings that can be applied to internal surfaces, less expensive coatings. The use of fine powders also has an disadvantage that th ey can have poor flow characteristics. The paper will discuss a feeder that is able to feed fine powders to overcome this difficulty and the coating equipment, both axial plasma and HVOF systems, used to deposit these materials to produce smooth dense coatings. 相似文献
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Effect of Processing and Composition on the Structure and Properties of P/M EP741NP Type Alloys 总被引:1,自引:0,他引:1
A study was carried out on the effects of processing and composition on the structure and properties of P/M EP741NP type alloys. The objectives of this study were to understand the role of Hf in a P/M superalloy containing high niobium used in aircraft engines and to determine the effects of extrusion and forging the powders as contrasted to HIPing (hot isostatic pressing) only. Two alloys of the P/M EP741NP composition were atomized: one alloy contained 0.26%Hf and the other was Hf free. After the as-atomized powders from both alloys were characterized, the powders were extruded into billets, forged and heat treated. After each process, the microstructures were characterized by SEM and the phases were extracted and identified by X-ray diffraction. The presence of Hf in the residues was probed by EDS (energy dispersive spectroscopy). The alloys were given the published Russian heat treatment as well as a more conventional heat treatment more typical of western powder alloys. Tensile, creep and stress rupture mechanical property tests were run. Results of the structural behavior of the alloys after each processing step will be presented and discussed. The role of the Hf on the mechanical proper- ties will be discussed. 相似文献
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氧气体扩散电极是电化学CO2浓缩器的关键因素之一,氧电极催化能力的研究有利于提高CO2的转移指数和转移速率。通过活性炭的预处理及Pt/C粉制备方法的选择,改进了氧电极的制备工艺。此外,以正交试验的结果分析为基础,得到了氧电极Pt/C粉的最佳制作条件。 相似文献
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本文用ESCA及电子显微分析方法研究了预处理Rene’95粉末表面的成分及析出相情况。预处理后粉末表面出现大量ZrO_2析出。雾化粉末表面的M’C碳化物在原位转变成MC。在粉末表面上还有大量二次碳化物,这些碳化物依附表面氧化物生核长大。预处理不能减少表面析出相数量,也未改变表面析出相的类型。 相似文献