Solidification and Crystal Growth on the SJ-10 Recoverable Scientific Experiment Satellite

The low-gravity environment aboard the space provides a unique platform for understanding crystal-growth-related phenomena that are masked by gravity on the Earth and for exploring new crystal growth techniques. We have characterized the wetting behavior of metal alloys and carried out melt growth of compound semiconductors under the support of materials science program in the SJ-10 recoverable satellite. We found that interfacial reaction plays a significant role in the interfacial evolution of Sn-based alloys. Detached growth of InAsSb was realized under microgravity, whereas during the terrestrial experiment the crystal and the crucible wall contact with each other. Moreover, the suppression of buoyancy-driven convection results in a more uniform composition distribution in the InGaSb and Bi₂Te₃-based semiconductor alloys.      

Microgravity Material Research in China:2016

Firstly, recent research works of high undercooling and rapid solidification of metallic alloys under ground simulation conditions in Northwestern Polytechnical University are reviewed. Secondly, under normal gravity and microgravity of binary to quinary Nickel-base single crystal alloys with different contents of W, Ta, Al and Ti elements are comparatively investigated by Institute of Metal Research using drop tube. Thirdly, solidification and crystal growth of SJ10-Recoverable Scientific Experiment Satellite by Institute of Semiconductors is introduced.      

ADVANCES IN MATERIAL RESEARCHES UNDER MICROGRAVITY 2000-2002

The Engineering of Chinese Spacecraft provides Chinese scientists of materials great opportunity in the experiments for preparing materials under microgravity. On board of Spacecraft-Shenzhou No.3 (SZ-3), alloys and semiconductors, such as Al Mg2Si, Nd60Al10Fe20Co10, Pd40Ni10Cu30P20, Al-Al3Ni, GaMnSb, Bi12SiO20:Ce, and Cd0.96Zn0.04Te:Ge, were prepared. SZ-3 successfully returned to the earth on April 1, 2002. Profiting from SZ-3, great progress has been made in the researches on ma terials under microgravity in space. The quartz ampoules containing the materials grown on board of SZ-3 were shown in CFig. 1 (see the Appendix). The properties of the materials prepared on board of SZ-3 are still under investigation.     

Influence of Fast Global Variations of Solar Magnetic Fields on Space Weather in Cycle 23

It is established that the large-scale and global magnetic fields in the Sun's atmosphere do not change smoothly, and long-lasting periods of gradual variations are superseded by fast structural changes of the global magnetic field. Periods of fast global changes on the Sun are accompanied by anomalous manifestations in the interplanetary space and in the geomagnetic field. There is a regular recurrence of these periods in each cycle of solar activity, and the periods are characterized by enhanced flaring activity that reflects fast changes in magnetic structures. Is demonstrated, that the fast changes have essential influencing on a condition of space weather, as most strong geophysical disturbances are connected to sporadic phenomena on the Sun. An explanation has been offered for the origin of anomalous geomagnetic disturbances that are unidentifiable in traditionally used solar activity indices. Is shown, main physical mechanism that leads to fast variations of the magnetic fields in the Sun's atmosphere is the reconnection process.     

Survey on the Magnetic Structure of the Neutral Sheets in Earth's Magnetotail

Based on the multipoint magnetic observations of Cluster from 2001 to 2004, the magnetic field structure in magnetotail Neutral Sheet （NS） is statistically surveyed. The results are as follows. In NS, a cubic function is selected to reveal the relation between y （GSM） and positional parameter z. The relation between y and magnetic field values indicates that the magnetic field is weak at midnight region and strengthens gradually at the duskside and dawnside. The relation between y and curvature radius is expressed by a quadratic function. And R_c of flattened CS is less than that of the normal CS. B_y determines the orientation of MFLs' configuration. The polar angle of the curvature vector is affected by the NS configuration. In addition, the correlation between the polar angle of the curvature vector and z is higher. The polar angle of the normal of the osculating plane is uncertain in the center area. The relation between the azimuthal angles of the curvature vector （the normal of the osculating plane） and y is negatively correlated. An empirical model applied to yz plane of the three-dimensional structure of the magnetic field lines in the NS are developed, and it is represented as a function of the positional parameter y. Finally, the current density is also statistically surveyed.      

A 3rd Order WENO GLM-MHD Scheme for Magnetic Reconnection

A new numerical scheme of 3rd order Weighted Essentially Non-Oscillatory (WENO)type for 2.5D mixed GLM-MHD in Cartesian coordinates is proposed. The MHD equations are modified by combining the arguments as by Dellar and Dedner et al to couple the divergence constraint with the evolution equations using a Generalized Lagrange Multiplier (GLM). Moreover, the magnetohydrodynamic part of the GLM-MHD system is still in conservation form. Meanwhile, this method is very easy to add to an existing code since the underlying MHD solver does not have to be modified. To show the validation and capacity of its application to MHD problem modelling,interaction between a magnetosonic shock and a denser cloud and magnetic reconnection problems are used to verify this new MHD code. The numerical tests for 2D Orszag and Tang's MHD vortex,interaction between a magnetosonic shock and a denser cloud and magnetic reconnection problems show that the third order WENO MHD solvers are robust and yield reliable results by the new mixed GLM or the mixed EGLM correction here even if it can not be shown that how the divergence errors are transported as well as damped as done for one dimensional ideal MHD by Dedner et al.      

Magnetospheric Boundary Layer Structure and Dynamics as Seen From Cluster and Double Star Measurements

In this review, we discuss the structure and dynamics of the magnetospheric Low-Latitude Boundary Layer (LLBL) based on recent results from multi-satellite missions Cluster and Double Star. This boundary layer, adjacent to the magnetopause on the magnetospheric side, usually consists of a mixture of plasma of magnetospheric and magnetosheath origins, and plays an important role in the transfer of mass and energy from the solar wind into the magnetosphere and subsequent magnetospheric dynamics. During southward Interplanetary Magnetic Field (IMF) conditions, this boundary layer is generally considered to be formed as a result of the reconnection process between the IMF and magnetospheric magnetic field lines at the dayside magnetopause, and the structure and plasma properties inside the LLBL can be understood in terms of the time history since the reconnection process. During northward IMF conditions, the LLBL is usually thicker, and has more complex structure and topology. Recent observations confirm that the LLBL observed at the dayside can be formed by single lobe reconnection, dual lobe reconnection, or by sequential dual lobe reconnection, as well as partially by localized cross-field diffusion. The LLBL magnetic topology and plasma signatures inside the different sub-layers formed by these processes are discussed in this review. The role of the Kelvin-Helmholtz instability in the formation of the LLBL at the flank magnetopause is also discussed. Overall, we conclude that the LLBL observed at the flanks can be formed by the combination of processes, (dual) lobe reconnection and plasma mixing due to non-linear Kelvin-Helmholtz waves.      

Materials Experiment on Tiangong-2 Space Laboratory

During the China's Tiangong-2 (TG-2) flight mission, the experiments of 18 kinds of material samples were conducted in space by using a Multiple Materials Processing Furnace (MMPF) mounted in the orbital module of the TG-2 space laboratory. After the experiments of 12 kinds of samples of the first and second batches were completed successfully, astronauts packed and brought them back to the ground by ShenzhouⅡ spacecraft. By studying processing and formation on semiconductor and optoelectronics materials, metal alloys and metastable materials, functional single-crystal, micro-and nano-composite materials encapsulated in sample ampoules both in space and on Earth, we expect to explore some physical and chemical processes and mechanism of the materials formation that are normally obscured and therefore are difficult to study quantitatively on the ground due to the gravity-induced convection, to obtain the processing and synthesis technology for preparing high quality materials, and lead to the improvement and development of materials processing techniques on Earth, and also develop the experiment device and comprehensive ability for materials experiment in microgravity environment. This report briefly introduces the main points of each research work and preliminary comparative analysis results of 12 samples carried out by scientists undertaking research task.      

Mid-Latitude Pc1, 2 Pulsations Induced by Magnetospheric Compression in the Maximum and Early Recovery Phase of Geomagnetic Storms

We investigate the properties of interplanetary inhomogeneities generating long-lasting mid-latitude Pc1, 2 geomagnetic pulsations. The data from the Wind and IMP 8 spacecrafts, and from the Mondy and Borok midlatitude magnetic observatories are used in this study. The pulsations under investigation develop in the maximum and early recovery phase of magnetic storms. The pulsations have amplitudes from a few tens to several hundred pT andlast more than seven hours. A close association of the increase (decrease) in solar wind dynamic pressure (Psw) with the onset or enhancement (attenuation or decay) of these pulsations has been established. Contrary to high-latitude phenomena, there is a distinctive feature of the interplanetary inhomogeneities that are responsible for generation of long-lasting mid-latitude Pc1, 2. It is essential that the effect of the quasi-stationary negative Bz-component of the interplanetary magnetic field on the magnetosphere extends over 4 hours. Only then are the Psw pulses able to excite the above-mentioned type of mid-latitude geomagnetic pulsations. Model calculations show that in the cases under study the plasmapause can form in the vicinity of the magnetic observatory. This implies that the existence of an intense ring current resulting from the enhanced magnetospheric convection is necessary for the Pc1, 2 excitation. Further, the existence of the plasmapause above the observation point (as a waveguide) is necessary for long-lasting Pc1 waves to arrive at the ground.      

A review of long drop tubes as a supplement/alternative to space experiments

The 100 meter high drop tube at the Marshall Space Flight Center has proven to be a viable facility for studies of containerless solidification. Advantages are that experiments are inexpensive and large numbers of specimens can be processed rapidly. It would not be unusual to run ten specimens in a day. Another significant advantage is that the undercooling behavior can be followed with sufficient sensitivity to easily detect the onset of recalescence and subsequent events.Disadvantages are the restrictions on specimen sizes and types of alloys that can be run in a microgravity environment. Practical specimen sizes range between 50 mg and 500 mg depending on the type of furnace being used. Refractory alloys can be processed in a vacuum (about 10^?5 torr) and therefore at microgravity. Non-refractory alloys demand an atmosphere (about 200 torr) to obtain appreciable undercooling before impact at the bottom of the tube. Under these conditions significant g forces result.Because of the present limitations of the 100 meter drop tube, the most definitive work has been done on niobium based alloys. Large amounts of undercooling have been observed routinely and the effects of undercooling on microstructure have been characterized in detail. X-ray diffraction, scanning electron microscopy, and transmission electron microscopy have been used to determine types of phases, amounts of phases, and compositions of phases. It is clear, as would be expected, that the results bear some resemblance to rapid solidification processing by quenching. However, there are dissimilarities due to the uniqueness of solidification by deep undercooling without quenching in long drop tubes and accompanying recalescence effects.     

Progress in Research on Materials Under Microgravity in China

Research on materials under microgravity in China began in the 1980s, sparked by Prof. Lanying Lin (academician of CAS), Prof. Xiji Wang (academician of CAS), Prof. Guirong Min (academician of CAS), and Prof. Huabao Lin (academician of CAS), and others. The first semiconductor crystal, first optical crystal, and first alloys were grown in space on board a recoverable satellite in 1987. Since then, microgravity materials science became a new scientific branch in China.Scientific and technical activities on space crystal growth and solidification are carried out through two major programs: ground-based studies and orbital experiments. The main results obtained during 2001-2003 are reported below.     

空间微重力条件下偏晶合金的研究

利用我国首次卫星搭载,进行了偏晶合金Zn—Pb、Al—Pb 的空间微重力下的重熔试验,研究了低于临界温度下Al—Pb 合金重熔过程中的物理规律;在临界温度之上重熔了Zn—Pb 合金,发现了Marangoni 对流对合金凝固过程的影响;在液态烧结条件下制备了均匀的粉末Zn—Pb 合金。在微重力下的研究表明:空间微重力条件对消除由于重力引起的宏观偏折和自然对流十分重要,但在重力消失后,非重力的其它因素的影响又显得格外重要。     

Liquid phase sintering of tungsten composites in space: Results of tests performed in Texus

Tungsten-nickel-iron composites are commersially fabricated from powders by liquid phase sintering. They consist of almost spherical tungsten particles in a matrix of nickel-iron-tungsten. A way to contribute to the understanding of the sintering mechanism and the mechanical properties is to study composites with a low amount of tungsten particles. Depending on the great difference in density between the particles and the matrix, this can only be done under microgravity. A primary sintering test of the tungsten composite was done in space using the Texus 10 modul. Prealloys were fabricated from metal powder mixtures, which were hot isostatic pressed. Liquid phase sintering of the two tungsten composites under microgravity has shown that the particles are evenly distributed and that no segregation occured due to convection. Despite an uneven distribution of the particles in the preformed specimens and the short melting period the patricle distribution has become even. Compared to short time sintering tests made on four alloys in the laboratory, the growth and separation of the particles was fast.     

一种空间相变换热器热设计与仿真分析及其改进

基于相变计算方法即焓法处理相变材料凝固/融化模型,对一个以水为主动冷却介质,内填充石蜡类相变蓄热材料的板式相变换热器的换热进行数值模拟.得到了不同重力条件下冷却面的温度分布,相变材料在融化过程中的动态温度场分布、相变界面分布、融化时间等结果,验证了该相变换热器的可行性.对比该相变换热器在重力与微重力不同条件下的性能差异,利用添加强化传热肋片与泡沫复合相变材料方法,提高了微重力条件下该类相变换热器的效率,可为空间相变蓄热装置的设计及实验研究提供重要参考.      

Contactless positioning,manipulation and shaping of liquids by gas bearing for microgravity applications

Contactless positioning, manipulation and shaping of liquids using the gas bearing principle is demonstrated by ground experiments. Extensions to microgravity applications are presented also associated with solidification of molten materials.     

液态金属镓微重力下的融化传热特性

相变蓄热适用于周期性热流作用下航天器内部工作单元的温度控制,但是需解决微重力环境下相变材料融化速率低的问题.鉴于液态金属高导热系数和高单位体积潜热的特点,在微重力下将液态金属作为相变材料有望提高融化速率.通过对微重力下液态金属镓融化过程的相界面演化、流线和温度分布特征进行数值研究,分析了腔体尺寸和过热度对融化过程的影响.结果表明:微重力下镓的融化过程中,热传导起主导作用;镓的融化时间比冰和正十八烷分别减少了88.3%和96.4%,储热量分别为冰和正十八烷的1.2倍和2.2倍;融化时间随过热度增加而减小,随腔体半径增大而增大.此外推导出了液相分数随无量纲时间变化的关系.