Effect of gravity on coupled convective and interfacial instabilities during directional solidification

We investigate the role of gravity in a linear stability analysis of the onset of coupled convective and morphological instabilities during directional solidification at constant velocity of a dilute alloy of tin in lead. For solidification vertically upwards, the temperature gradient alone would cause a negative density gradient and the solute gradient alone would cause a positive density gradient. Two types of instability are found, a convective type that occurs for long wavelengths and a morphological type that occurs for short wavelengths. In general, these are coupled but the morphological instabilities are practically independent of gravity and thus correspond to the predictions of previous morphological stability theory in which density changes and convection are neglected. The convective instabilities depend strongly on gravity; for a growth velocity of V = 1 μm/s and a temperature gradient in the liquid of G_L = 200 K/cm, the critical concentrations for convective instabilities are 3.1 × 10^?4, 3.1 × 10^?2 and 2.39 wt. % for g_e = 980 cm/s², 10^?4 g_e and 10^?6 g_e, respectively. For low velocities, the convective instabilities occur at much lower solute concentrations than the morphological instabilities whereas at high velocities, the reverse is true. At intermediate velocities where the changeover takes place, there are oscillitory instabilities of mixed character whose periods range from 60 s at g_e to 6 × 10⁴ s at 10^?6 g_e.     

2-D differential interferometer

A new type of differential interferometer based on holographic optical elements is developed, which allows the exact determination of a refractive index gradient field in two orthogonal directions. This interferometer will be used in TEXUS experiments to determine the temperature field in a convective liquid cell in which the temperature may be known at only one point.     

A review of long drop tubes as a supplement/alternative to space experiments

The 100 meter high drop tube at the Marshall Space Flight Center has proven to be a viable facility for studies of containerless solidification. Advantages are that experiments are inexpensive and large numbers of specimens can be processed rapidly. It would not be unusual to run ten specimens in a day. Another significant advantage is that the undercooling behavior can be followed with sufficient sensitivity to easily detect the onset of recalescence and subsequent events.Disadvantages are the restrictions on specimen sizes and types of alloys that can be run in a microgravity environment. Practical specimen sizes range between 50 mg and 500 mg depending on the type of furnace being used. Refractory alloys can be processed in a vacuum (about 10^?5 torr) and therefore at microgravity. Non-refractory alloys demand an atmosphere (about 200 torr) to obtain appreciable undercooling before impact at the bottom of the tube. Under these conditions significant g forces result.Because of the present limitations of the 100 meter drop tube, the most definitive work has been done on niobium based alloys. Large amounts of undercooling have been observed routinely and the effects of undercooling on microstructure have been characterized in detail. X-ray diffraction, scanning electron microscopy, and transmission electron microscopy have been used to determine types of phases, amounts of phases, and compositions of phases. It is clear, as would be expected, that the results bear some resemblance to rapid solidification processing by quenching. However, there are dissimilarities due to the uniqueness of solidification by deep undercooling without quenching in long drop tubes and accompanying recalescence effects.     

Direct observation of processes in a solidifying dispersion

The evolution of a dispersion under the action of temperature gradients and solidification was followed optically in a transparent molten salt (CsCl) with inclusions of Pb-droplets and gas bubbles. This system is believed to model a solidifying metallic alloy. Rejection of Pb-particles by the solidification front was observed, while large gas bubbles were incorporated. Thermocapillary convection at the gas bubbles considerably distorted the temperature field and even caused local remelting. Marangoni migration of bubbles was not observed, contrary to expectations.     

A ground-based study for a shuttle BRIC experiment on gravity effects on gene expression.

A BRIC (Biological Research In a Canister) experiment to investigate the effects of reduced gravity at the molecular level using Arabidopsis has been initiated. In preparation for a space flight experiment, a series of ground-based studies were conducted. Results from these studies indicate that: 1) up to 20,000 seeds can be germinated on a 100 mm diameter Petri plate, 2) nylon membrane is the best surface for recovery of plant material after freezing, 3) depending on the age of the seedlings at the time of freezing, 20 to 40 g of tissue can be obtained from Petri plates that fit in a single canister; 4) tissue from one canister yields adequate amounts of RNA to perform differential display to isolate gravity-regulated genes. Our results indicate that the proposed BRIC experiment is feasible and can provide valuable information on the possible effects of microgravity on gene regulation.     

Strong magnetic field effect on the dissolution process of tetragonal lysozyme crystals.

Either a homogeneous or inhomogeneous magnetic field has been known to dampen the protein crystal growth. To date the mechanism is not clear. However, it was generally proposed that the magnetic field may dampen the convection in the solution, resulting in a reduced crystal growth rate and possibly a good crystal quality, similar to the case of protein crystal growth in space. To understand the mechanism of the magnetic field effect on protein crystal growth, further explorations on the magnetic field effect on protein solution, on the processes of crystal growth and dissolution, and on different crystallization (solution) systems, should be valuable. In this paper we present our recent efforts to study magnetic field effects on the dissolution processes of tetragonal lysozyme crystals under a strong magnetic field. A layer of oriented tetragonal lysozyme crystals was prepared under a temperature gradient and magnetic field, after that the crystals were dissolved by increasing the temperature of the solution. The lysozyme molecules will diffuse upwards due to the steep concentration gradient at the lower side of the cell caused by the dissolution. The evolution of the concentration in the solution was measured in-situ using a Mach-Zehnder interferometer. The results confirmed that the dissolution process of the crystals was slowed by the magnetic field. Judging from the concentration evolution versus time at different positions in the solution, we concluded that the apparent diffusion coefficient of lysozyme molecules was decreased by the magnetic field. The results were discussed using a suspended crystal model in the initial dissolution stage.     

Ionization and recombination processes determining plasma density at the initial stage of artificial cloud injection

The initial reduction of the electron density after the injection explosion is shown to be associated with recombination at the adiabatic cooling under the cloud expansion. Primordial thermal ions can disappear in triple collisions almost entirely. Nevertheless, a minor amount of ions is conserved due to the freezing effect. The further rapid increase in the electron concentration may be attributed to the secondary ionization process. It is shown that the cumulative electronic ionization can account for the observed electron density elevation. The modified two-stream instability can provide a longitudinal (anomalous) resistance for the longitudinal electric field required for an avalanche. The electric field and longitudinal currents arise owing to the polarization with ions entrained by the neutral gas across the magnetic field and magnetized electrons moving along the field.     

泡沫铜/低熔点合金复合相变材料凝固放热分析

为研究泡沫铜/低熔点合金(LMPA)复合相变材料在间歇放热工作环境下恢复至初始状态的能力及不同孔隙率泡沫铜的添加对其凝固放热过程的影响，通过数值模拟对比分析了47合金、正二十三烷与泡沫铜复合前后的凝固放热过程，并调节泡沫铜/47合金复合材料孔隙率计算模拟芯片温度在凝固放热过程中温度随时间变化曲线。结果表明:泡沫铜的添加对2类材料凝固过程均有促进作用，模拟芯片恢复至目标温度所需时间分别被缩短6.6%和47.7%。因体积潜热值的差距，泡沫铜/47合金凝固时需放出更多热量，恢复至目标温度的时间较长，是正二十三烷复合相变材料的1.52倍。随着孔隙率的增大，复合相变材料恢复至室温状态所用时长变化不大，考虑到孔隙率对相变热控过程中的影响，实际使用时应综合考虑。      

Agravitropic mutant for the study of hydrotropism in seedling roots

Roots have been shown to respond to a moisture gradient by positive hydrotropism. Agravitropic mutant plants are useful for the study of the hydrotropism in roots because on Earth hydrotropism is obviously altered by the gravity response in the roots of normally gravitropic plants. The roots are able to sense water potential gradient as small as 0.5 MPa mm⁻¹. The root cap includes the sensing apparatus that causes a differential growth at the elongation region of roots. A gradient in apoplastic calcium and calcium influx through plasmamembrane in the root cap is somehow involved in the signal transduction mechanism in hydrotropism, which may cause a differential change in cell wall extensibility at the elongation region. We have isolated an endoxy loglucan transferase (EXGT) gene that is strongly expressed in pea roots and appears to be involved in the differential growth in hydrotropically responding roots. Thus, it is now possible to study hydrotropism in roots by comparing with or separate from gravitropism. These results also imply that microgravity conditions in space are useful for the study of hydrotropism and its interaction with gravitropism.     

Assessment study of ionosphere correction model using single- and multi-shell algorithms approach over sub-Saharan African region

It is a known fact that ionosphere is the largest and the least predictable among the sources of error limiting the reliability and accuracy of Global Navigation Satellite Systems (GNSS) and its regional augmentation systems like Satellite Based Augmentation System (SBAS) in a safety-of-life application. The situation becomes worse in the Equatorial Ionization Anomaly (EIA) region, where the daytime ionization distribution is modified by the fountain effect that develops a crest of electron density at around ±15° to ±20° of the magnetic equator and a trough at the magnetic equator during the local noon hours. Related to this phenomenon is the appearance of ionosphere irregularities and plasma bubbles after local sunset. These may degrade further the quality of service obtained from the GNSS/SBAS system of the said periods. Considering the present operational augmentation systems, the accuracy and integrity of the ionosphere corrections estimate decreases as the level of disturbances increases. In order to provide a correct ionosphere correction to the user of GNSS operating in African EIA region and meet the integrity requirements, a certified ionosphere correction model that accurately characterizes EIA gradient with the full capacity to over-bound the residual error will be needed. An irregularities detector and a decorrelation adaptor are essential in an algorithm usable for African sub-Saharan SBAS operation. The algorithm should be able to cater to the equatorial plasma vertical drifts, diurnal and seasonal variability of the ionosphere electron density and also should take into account the large spatial and temporal gradients in the region. This study presents the assessment of the ionosphere threat model with single and multi-layer algorithm, using modified planar fit and Kriging approaches.     

Experimental study of morphological and convective instabilities: The MEPHISTO space program

It is now well established that the morphological instability, i.e. the transition during solidification from a planar L/S interface to a cellular one, is strongly influenced by convection. The most recent theories on this topic, which are very advanced, suffer from the lack of experimental tests because uncontrolled convective effects cannot be avoid on the ground. Moreover the check of all the pertinent solidification parameters are not controlled in the same time or measured in real time. After a review of the main 1g experiments and their own limitations, we describe a new apparatus (MEPHISTO) which allows :

• •in-situ measurements of the main solidification parameters and in particular the undercooling at the solidification front in real time by a non perturbative method.
• •real time supervision of convective motions influence on crystal growth. First results obtained under 1g condition are presented :
  • ◦hydrodynamic scaling laws testing,
  • ◦instabilities detection,
  • ◦transient phenomena.

Main space results are then anticipated including the role of g-jitters.     

Electromagnetic containerless undercooling facility and experiments for the shuttle

An electromagnetic furnace is being prepared for flights aboard the space shuttle. This apparatus is capable of melting metals and alloys up to 1400°C melting point by induction heating with subsequent solidification of the freely levitated melt without contact with any container. The solidification can be carried out with greatly reduced fields resulting in minimal heating and stirring of the free melt. Sequential specimens can be processed during flight. Several experiments are planned for a series of flights, beginning in 1985 with an undercooling experiment on NiSn alloys. These will be interspersed with detailed studies of fluid flow caused by low and high field levels in order to quantify the corresponding effect upon the solidification process.     

Eutectic solidification of Al-Cu alloys influenced by convection

Directional solidification of eutectic Al-Cu alloys has been studied to demonstrate the influence of both impurity concentration and convective conditions. The λ/R relations show that higher iron concentration and intensive stirring coarsen the microstructure. The formation and growth of new iron-containing phases at the solidification front restrict impurity influence. Kinetic data follow a dependence λ.Rⁿ=const with n-value close to 0,5.     

Evaluation and modification of commercial infra-red transducers for leaf temperature measurement.

Accurate measurement of the leaf to air temperature gradient is crucial for the determination of stomatal conductance and other plant responses in both single leaves and in plant canopies. This gradient is often less than 1 degree C, which means that leaf temperature must be known to within about +/- 0.1 degree C. This is a challenging task, but new, miniature infra-red transducers from Exergen Corporation (Newton, MA) and Everest Interscience (Tucson, AZ) can be modified and calibrated to achieve this accuracy. The sensors must be modified to add thermal mass and the Exergen sensor requires a measurement of sensor body temperature. Significant error is caused by the discharge of a capacitor in the standard Exergen sensor, but we tested it without the capacitor. The sensors respond rapidly to changes in target temperature, but require 2 to 10 minutes to respond to changes in sensor body temperature, which is often the largest source of error. A new, sensitive method for measuring field of view indicates substantial peripheral vision for both sensors and a wider field of view than specified by the manufacturers. Here we describe sensor output as a function of target and sensor body temperatures, and provide a generic (sensor independent) equation that can be used to achieve +/- 0.2 C accuracy with Exergen sensors. The equation was developed and verified using two black body calibrators.     

Chandra imaging spectroscopy of the central region of AWM7

We report on the results of Chandra observations of the galaxy cluster AWM7. The ACIS image reveals new substructures with a spatial extent of more than 8″ (4 kpc at AWM7) near the cD galaxy center, represented by a hard sub-peak and a soft peak. These substructures suggest that a dynamical process related to the formation of the cD galaxy is now taking place. Inside the cluster core within a radius of 2′, annular spectra with every 10″ step are fitted well by single temperature models. The temperature gradually drops from 4.2 keV at a radius of 60 kpc (2′) to 1.8 keV at the cluster center. The radial abundance profile shows a gradient with a peak metallicity of 1.5 solar at a radius of about 15″ (7 kpc). A two-dimensional map shows two high metallicity blob-like regions, which may be the gas expelled from the cD galaxy.     

The importance of conductivity gradients in ground-based field-aligned current studies

Magnetosphere-ionosphere coupling is achieved primarily through magnetic field-aligned currents. Such currents are difficult to measure directly and are usually inferred from satellite magnetometer recordings or from ground-based measurements of the divergence of ionospheric electric fields. The latter technique requires a knowledge of the ionospheric conductance distribution. Although it is possible to obtain the ionospheric electric field distribution over large spatial areas with good temporal resolution from coherent backscatter radars, these instruments cannot measure conductivity. Since the equation for computing field-aligned currents explicitly requires the gradient in conductance to be known, the use of statistically averaged models is excluded for case studies. If a dense enough array of magnetometers is available, these data may be used in combination with radar data to produce a measured conductance distribution within the overlapping fields of view. This has been done for data obtained in northern Scandinavia. Comparing field-aligned currents, computed with and without knowing the ionospheric conductance distribution, shows that gradients in conductance can not be ignored, even for quiet geomagnetic conditions.     

Role of cell differentiation in high tolerance by prokaryotes of long-term preservation in permafrost

The effect of low temperature on the cell structure of bacteria isolated from permafrost results in structural changes leading to cell differentiation into types of resting cells rangign from spores showing a high endogenous dormancy to typical “dormant” cells of non-spore-forming bacteria showing exogenous dormancy, which is considered to be less highly resistant to extreme conditions in laboratory experiments. In permafrost, dormant cells of non-spore-forming bacteria may demonstrate considerable resistance to long-term freezing and as a result a higher survival level than spore-forming bacteria.     

复杂涂覆目标的角闪烁特性分析

适当的涂覆材料可以使空中目标的后向雷达散射截面缩小,但同时,涂覆材料也会影响角闪烁偏差.为了充分利用涂覆材料的特性,利用图形电磁学和相位梯度法,在高频区对涂覆目标进行了角闪烁特性的建模与计算.鉴于图形电磁学的特色,涂覆目标的角闪烁计算不仅具有可视化特点,而且计算速度快、效率高.利用该方法对两球目标和复杂目标进行了仿真计算,计算结果表明涂覆材料在减小后向雷达散射截面的同时,对角闪烁具有一定的增强作用.      

等离子体片边界层中静电不稳定性产生的波-粒动量交换率

本文介绍了非均匀等离子体片外边缘离子束流-密度梯度漂移不稳定性的二级理论。二级动量交换率的计算表明, 模型等离子体中冷、暖束流离子的场向动量以及暖束流离子的横向动量可以被静电波来减小。这些波是由离子束流-密度梯度漂移不稳定性产生的。这些结果对于理解等离子体片外边缘等离子体的各向同性化和热化是很有用的。      

Influence of freezing rate changes on MnBiBi eutectic microstructure

In an attempt to explain the influence of space processing on the microstructure of MnBiBi, eutectic mixtures were directionally solidified with a sudden change of translation rate. The MnBi fiber spacing was able to adapt to the changing freezing rate as predicted by heat transfer computations. Thus the microstructure adapts more rapidly than the freezing rate could be changed in the present experiments.