中性水基氧化铝陶瓷料浆的流变学研究

采用流变学的方法在RV 2 0型流变仪上研究了不同条件对中性氧化铝悬浮体流变性的影响。重点研究了固含量、分散剂加入量、球磨工艺对料浆流变性的影响。研究表明 :随临界固含量的降低 ,“剪切增厚”的临界剪切速率呈明显的升高趋势 ,从固含量为 5 6vol%时的 82s-1增加到固含量为 5 0vol%时的 192s-1;分散剂的加入量对料浆的临界剪切速率具有显著的影响 ,当固含量为 5 6vol%时 ,分散剂合适的量为 1 0wt% ;随着球磨时间的延长 ,料浆的“剪切增厚”临界剪切速率增大 ,而且逐渐不再有“剪切变稀”阶段。     

固相含量对Al2O3料浆及瓷体性能的影响

研究了固相浓度对用于凝胶注成型的Al2O3料浆的粘度和流动性能的影响,并分析了由不同浓度的料浆制得的瓷体结构和性能与料浆浓度的关系.结果表明,控制合适的体浓度对于获得适合浇注的高性能料浆是必要的.同时由于料浆浓度会影响球磨效率和坯体密度,因此会对最终瓷体的质量有较大影响.在本文的实验条件下,料浆中固相的最佳含量为50vol%.     

pH值对凝胶注模氧化铝陶瓷料浆性能的影响

重点研究了在低粘度,高固相体积分数氧化铝浓悬浮体制备过程中,料浆的pH值对料浆性能的影响。结果表明:当pH值达到5左右时,Al_2O_3颗粒在水中的Zeta电位等于0,此时,料浆的粘度最大,分散效果最差。当pH值达到9时,Zeta电位的绝对值达到最大,此时料浆的悬浮稳定性最佳。     

凝胶注模氧化铝陶瓷坯体的结构与表征

研究了凝胶注模氧化铝陶瓷坯体的密度、强度、空隙率分布及微观结构等特征。结果表明,影响凝胶注模陶瓷坯片密度的因素主要有:料浆的固含量、单体含量、单体和胶联剂的比值。随着料浆固含量的提高,坯片的抗弯强度呈下降趋势,坯片内部的孔隙率降低,从平均孔隙度为110nm降为90nm,而且均为单峰分布。凝胶注模成型的陶瓷坯片在干燥后,坯片强度优于注射成型、流延成型等传统成型方式。     

复合固体推进剂药浆粘度的预估

本文通过对影响固体推进剂药浆粘度的因素进行分析和相关试验,导得了药浆粘度预估的数学关系式。试验结果表明,对含过氯酸铵推进剂药浆粘度的预估值93％的数据在实验值的±15％内;对含铝粉推进剂药浆粘度的预估值92％的数据在实测值的±20％范围内。     

POE-g-MAH 对PA66 共混体系性能的影响

讨论了POE-g-MAH含量、MAH接枝率对PA66/POE/POE-g-MAH共混物性能的影响.当POE-g-MAH含量为10wt％～15wt％时,PA66/POE-g-MAH共混物发生脆-韧转变;随POE-g-MAH含量增加,共混物的缺口冲击强度、断裂伸长率显著增大,拉伸强度、弯曲强度、弯曲模量、熔体流动速率、吸水率均明显下降.当POE-g-MAH接枝率为0.05wt％～0.2wt％时,PA66/POE/POE-g-MAH共混物发生脆-韧转变;随POE-g-MAH接枝率增加,共混物的缺口冲击强度、断裂伸长率增大,拉伸强度、弯曲强度、弯曲模量、吸水率变化不大,熔体流动速率下降.SEM照片和Molau实验表明,POE-g-MAH对PA66具有显著的增容增韧效果.     

有序多孔氧化铝陶瓷微观结构研究

利用扫描电镜(SEM)对模板法制备的有序多孔氧化铝陶瓷的微观结构特征、孔隙结构和晶粒生长进行了研究.结果表明:通过模板法制备的多孔氧化铝陶瓷孔结构均匀、排列有序,孔洞内部相互连通;随着料氧化铝浆固相体积的增加,多孔陶瓷的孔隙率相应降低;孔洞边缘没有出现晶粒的异常生长,与发泡法制备的多孔陶瓷相比,烧结致密度更高.     

关于复合固体推进剂批次间性能差异的研究(报告之二:药浆的粘度分析)

复合固体推进剂药浆是固体粒子含量很高的粘性流体。影响其粘度的除了粘结剂的度粘外,主要还有固体粒子的容积百分比和尺寸匹配。文中介绍了计算药浆粘度公式,还就粒子形状、尺寸、表面性质对有粒子悬浮的浆液粘性影响作简要回顾。文中还指出,由于药浆的固体粒子含量高,用不同测试方法测得的药浆粘度可能会差距甚大以及粒子容积含量的少量不均匀性可能会导致粘度值差很多。     

Al-Mg-Sc 和Al-Mg-Er 合金的组织与性能

采用铸造—轧制—稳定化退火技术制备了Sc含量为0.10wt％和Er含量为0.25wt％的两种Al-Mg合金薄板,研究了不同处理工艺下两种合金板材拉伸性能、剥落腐蚀性能和显微组织的变化规律.结果表明,两种合金冷轧板材稳定化退火过程中拉伸性能有相同的变化规律,即随着退火温度升高,板材强度下降而塑性升高,Sc含量为0.10wt％的合金350℃/1 h退火仍然表现出很强的抗退火软化能力,而Er含量为0.25％的合金当退火温度高于280℃后迅速软化;300℃/1 h退火条件下,含Sc合金和含Er合金的抗拉强度、屈服强度和伸长率分别为424 MPa、314 MPa、18.3％和350 MPa、177 MPa、29.1％;与此同时,随退火温度的升高,板材抗剥落腐蚀的能力也表现出相同规律性的变化,即200℃/1 h左右退火时剥落腐蚀最严重,随着退火温度升高,腐蚀抗力增加,两种合金板材经280℃以上1h稳定化退火后,合金板材可以获得较好的抗剥落腐蚀性能;其次,与Sc含量为0.25wt％的5B70合金相比,研制的Sc含量为0.10wt％合金综合性能接近5B70合金,而这种合金的Sc含量只有5B70合金的40％,能显著降低合金的制造成本,预示着低Sc含量的合金在航天领域有良好的开发应用前景.     

MWNT/PEK-C导电薄膜的制备及其性能研究

利用WD-01分散剂辅助球磨分散法和涂布技术,制备多壁碳纳米管(MWNT)/改性聚醚酮(PEK-C)复合薄膜,考察树脂浓度、球磨时间、涂布液放置时间及MWNT含量等因素对薄膜导电性能的影响,研究MWNT含量及残留溶剂对薄膜储能模量及玻璃化转变温度(Tg)的影响。结果表明,由WD-01分散剂辅助球磨分散法可以剪短并有效分散MWNT;涂布液黏度增大能有效抑制MWNT的再团聚;在MWNT含量在8%~33.3%的范围内,薄膜电导率随MWNT含量的增加呈线性升高,在MWNT含量为33.3%时,薄膜电导率达7.2S/cm;碳纳米管吸附溶剂使薄膜的玻璃化转变温度降低。     

The effect of inlet conditions on the flow and heat transfer in multiple rotating cavity with axial throughflow

This paper discusses experimental results from two different build configurations of a heated multiple rotating cavity test rig.Measurements of heat transfer from the discs and tangential velocities are presented.The test rig is a 70% full scale version of a high pressure compressor stack of an axial gas turbine engine.Of particular interest are the internal cylindrical cavities formed by adjacent discs and the interaction of these with a central axial throughflow of cooling air.Tests were carried out for a range of non-dimensional parameters representative of high pressure compressor internal air system flows(Re up to 5×106 and Rez up to 2×105).Two different builds have been tested.The most significant difference between these two build configurations is the size of the annular gap between the(non-rotating) drive shaft and the bores of the discs.The heat transfer data were obtained from thermocouple measurements of surface temperature and a conduction solution method.The velocity measurements were made using a two component,LDA system.The heat transfer results from the discs show differences between the two builds.This is attributed to the wider annular gap allowing more of the throughflow to penetrate into the cavity.There are also significant differences between the radial distributions of tangential velocity in the two builds of the test rig.For the narrow annular gap,there is an increase of non-dimensional tangential velocity V/Ωr with radial location to solid body rotation V/Ωr=1.For the wider annular gap,the non-dimensional velocities show a decrease with radial location to solid body rotation.      

Research on Auto-detection for Remainder Particles of Aerospace Relay Based on Wavelet Analysis

Aerospace relay is one kind of electronic components which is used widely in national defense system and aerospace system. The existence of remainder particles induces the reliability declining, which has become a severe problem in the development of aerospace relay. Traditional particle impact noise detection (PIND) method for remainder detection is ineffective for small particles, due to its low precision and involvement of subjective factors. An auto-detection method for PIND output signals is proposed in this paper, which is based on direct wavelet de-noising (DWD), cross-correlation analysis (CCA) and homo-filtering (HF), the method enhances the affectiv-ity of PIND test about the small particles. In the end, some practical PIND output signals are analysed, and the validity of this new method is proved.     

Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl4 and SbCl3 and Azeotropic Drying

Antimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl4 and SbCl3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration.     

Effects of Mo on the Microstructure and Hydrogen Sorption Properties of Ti-Mo Getters

The effects of Mo on the microstructure evolution, porosity and hydrogen sorption properties of Ti-Mo getters are investigated in this work. The results show that the addition of Mo prolongs the densification process of Ti-Mo getters and results in a significant amount of sintered pores. With the Mo content increasing, the porosity of getters firstly increases reaching the maximum value as it at- tains about 7.5wt.%, and then drops. At the room temperature, the hydrogen sorption property of getters increases progressively with the Mo content increasing, but the tendency is not very clear before its content lies below 2.5wt.%. When the Mo content achieves about 7.5wt.%, the hydrogen sorption property proves to be the best. The discussion is made about the above mentioned phenomena inclusive of hydrogen sorption properties of getters under different activation conditions (from 500-750 ℃).     

超声速燃烧数值模拟中的湍流与化学反应相互作用模型

高精度数值模拟有助于理解超声速湍流燃烧中湍流与化学反应的相互作用,可为发动机燃烧室等工程应用设计提供可靠的预测模型。除直接数值模拟外,目前在湍流燃烧应用中使用的大涡模拟和雷诺平均Navier-Stokes模拟均需要借助模型模化发生在湍流小尺度上的流动与化学反应过程对湍流大尺度运动的影响。现有的湍流与化学反应相互作用模型大致可分为:火焰面类模型和概率密度函数类模型,2类模型在不同的应用中各自具有优势和局限性。此外,现有模型大都基于低马赫数燃烧,而超声速燃烧中通常会伴随快速混合、局部熄火和再着火以及激波等复杂过程,这为发展其中的湍流与化学反应相互作用模型提出了更多的挑战。     

适于低轨卫星IP网络的单核共享树组播算法(英文)

为了解决低轨卫星IP网络中现有典型源组播算法的信道资源浪费问题,本文提出了一套单核共享树组播算法,即核心群合并共享树(CCST)和加权核心群合并共享树(w-CCST)算法。CCST 算法包括动态近似中心(DAC)选核方法和核心群合并组播路径构建方法。DAC方法专为周期、规律运动的低轨卫星网络提出,不需要复杂的星上计算。在核心群合并方法中,以核节点作为初始核心群,通过核心群和剩余组成员的最短路径方法逐步扩展直至整棵组播树构建完成,从而使得组播树的树代价最小,大大提高了网络的带宽利用率和组播传输效率。w-CCST 算法中所提出的加权因子可以调整树代价和端到端传播时延之间的折衷程度,因此,可以通过调整加权因子来适度增大树代价、降低端到端传播时延以支持某些端到端时延要求苛刻的实时组播业务。最后,与低轨卫星 IP 网络中典型算法进行了性能比较,仿真结果说明,CCST 算法的平均树代价比其它算法显著降低,w-CCST 算法的平均端到端传播时延小于 CCST 算法。     

Jet Vectoring Control Using a Novel Synthetic Jet Actuator

A primary air jet vectoring control system with a novel synthetic jet actuator (SJA) is presented and simulated numerically. The results show that, in comparison with an existing traditional synthetic jet actuator, which is able to perform the duty of either “push” or “pull”, one novel synthetic jet actuator can fulfill both “push” and “pull” functions to vector the primary jet by shifting a slide block inside it. Therefore, because the new actuator possesses greater efficiency, it has potentiality to replace the existing one in various appli- cations, such as thrust vectoring and the reduction of thermal signature. Moreover, as the novel actuator can fulfill those functions that the existing one can not, it may well be expected to popularize it into more flow control systems.     

Nonlinear Adaptive Slewing Motion Control of Spacecraft Truss Driven by Synchronous V-gimbaled CMG Precession

The slewing motion control of a truss arm driven by a V-gimbaled control-moment-gyro (CMG) is a nonlinear control problem. The V-gimbaled CMG consists of a pair of gyros that must precess synchronously. The moment of inertia of the system, the angular momentum of the gyros and the external disturbances are not exactly known. With the help of feedback linearization and recursive Lyapunov design method, an adaptive nonlinear controller is designed to deal with the unknown items. Performance of the proposed controller is verified by simulation.     

An SOR Implicit Time-accurate Scheme in Calculating Unsteady Flows

A new time-accurate marching scheme for unsteady flow calculations is proposed in the present work. This method is the combination of classical Successive Over-Relaxation (SOR) iteration method and Jacobian matrix diagonally dominant splitting method of LUSGS. One advantage of this algorithm is the second-order accuracy because of no factorization error. Another advantage is the low computational cost because the Jacobian matrices and fluxes are only calculated once in each physical time step. And, the SOR algorithm has better convergence property than Gauss-Seidel. To investigate its accuracy and convergency, several unsteady flow computa- tional tests are carried out by using the proposed SOR algorithm. Roe’s FDS scheme is used to discritize the inviscid flux terms. Un- steady computational results of SOR are compared with the experiment results and those of Gauss-Seidel. Results reveal that the numerical results agree well with the experimental data and the second-order accuracy can be obtained as the Gauss-Seidel for unsteady flow computations. The impact of SOR factor is investigated for unsteady computations by using different SOR factors in this algorithm to simulate each computational test. Different numbers of inner iterations are needed to converge to the same criterion for different SOR factors and optimal choice of SOR factor can improve the computational efficiency greatly.