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1.
Nb-22Ti-14Si-2Hf-2Al-xCr (x=2, 6, 10, 14, 17 at%) alloys are prepared by arc-melting under argon atmosphere. Microstructural characteristics, mechanical properties and oxidation resistance of the arc-melted alloys are investigated. At 2 at% Cr content, the microstructure is composed of Nbss, Nb3Si and a small quantity of Nb5Si3, when the Cr contents increase, Nb3Si disappears. For the high Cr content (x ≥ 10 at%) alloys, besides the Nbss and Nb5Si3, Cr2Nb is also detected. With the increase of Cr content, the volume fractions of Cr2Nb and Nb5Si3 increase, while that of Nbss increases firstly and then begins to degrade when the Cr content is higher than 6 at%. For the alloy with 2 at% Cr, the room temperature fracture toughness is about 14.5 MPa·m1/2, but badly decreases to about 8.5 MPa·m1/2, when the Cr contents increase. Vickers hardness of Nbss tends to increase linearly from about 400 to 500, while that of silicides is not sensitive to Cr contents, about 950. The appearance of Cr2Nb phase significantly improves the high temperature oxidation resistance of the alloys with high Cr contents. The isothermal oxidation tests show that the oxidation kinetics of the alloys with various Cr contents follows parabolic oxidation kinetics. 相似文献
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The properties of spontaneous reconnection of a current sheet analyzed via direct three-dimensional simulations are presented. In particular the non-linear dynamics of resistive instabilities has been studied in absence or in presence of velocity shears. It is shown that full three-dimensional simulations allow the inclusion of a rich variety of (ideal) secondary instabilities which, depending on the initial equilibrium magnetic field configuration, determine the final fate of the system in the fully non linear regime. In particular in presence of a guide-field the dynamic is similar to what observed in two-dimensional simulations with energy driven toward both smaller and larger scales and energy spectra anisotropy. For different magnetic field configurations, the final state is characterized by the disruption of the coalesced structure created during the resistive phase and the system is characterized by a more chaotic state. A?discussion on the importance of high-order numerical techniques in numerical simulations of magnetic reconnection is also present. 相似文献
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Solar modulation of galactic cosmic radiation 总被引:1,自引:0,他引:1
U. R. Rao 《Space Science Reviews》1972,12(6):719-809
In this review an attempt is made to present an integrated view of the solar modulation process that cause time variation of cosmic ray particles. After briefly surveying the relevant large and small scale properties of the interplanetary magnetic fields and plasma, the motion of cosmic ray particles in the disordered interplanetary magnetic fields is discussed. The experimentally observed long term variations of different species of cosmic ray particles are summarised and compared with the theoretical predictions from the diffusion-convection model. The effect of the energy losses due to decelaration in the expanding solar wind are clearly brought out. The radial density gradient, the modulation parameter and their long term variation are discussed to understand the dynamics of the modulating region. The cosmic ray anisotropy measurements at different energies are summarised. At high energies (E 1 GeV), the average diurnal anisotropy is shown to be energy independent and along the 18.00 h direction consistent with their undergoing partial corotation with the sun. The average semi-diurnal anisotropy seems to vary with energy as E
+1 and incident from a direction perpendicular to the interplanetary field line, consistent with the semi-diurnal component being produced by latitudinal gradients. Both the diurnal and semi-diurnal components are shown to be practically time invariant. On a day to day basis, however, the anisotropy characteristics such as the exponent of variation, the amplitude and the phase show very high variability which are interpreted in terms of convection and variable field aligned diffusion due to the redistribution of the galactic cosmic ray density following transient changes in the interplanetary medium. The anisotropy observation at low energies (E 100 MeV) are, however, not explained by the theory.The rigidity dependence and the anisotropies during short term variations such as Forbush decreases are discussed in terms of the proposed field models for the interplanetary field structure and are compared with the observed rigidity dependence of long term variations. The data pertaining to the 27 day corotating Forbush decreases and their association with enhanced diurnal variation are also presented. The relationship between the energetic storm particle events which are caused by the acceleration of particles in the shock fronts and the Forbush decreases which are caused by the exclusion of galactic particles by the enhanced field structure in the same fronts are clearly brought out. Thus the recurrent increases at low energies and recurrent decreases at high energies may both be caused by the field structure in the shock front. In conclusion, the properties of the very short period fluctuations (18–25 cph) are summarised. 相似文献
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为了寻求Nb合金的强度和塑性的平衡,设计了以Nb基固溶体Nbss为主导相的Nb-xSi-6Hf-4Zr-2B-yTi(x=4,8;y=10,30;原子分数)合金,研究了Si和Ti对合金组织和室温力学性能的影响。结果表明,合金由Nbss、Nb3Si和Nb5Si3等3相组成。4Si-(10,30)Ti合金铸态组织是Nb枝晶和分布在枝晶间的硅化物(Nb3Si和Nb5Si3),8Si-(10,30)Ti合金Nb枝晶间分布的是Nb/硅化物(Nb5Si3)的共晶和Nb3Si,随着Si和Ti含量的增加,硅化物体积分数增加。1 600 ℃退火50 h可使部分Nb3Si共析分解,改变合金的组织形貌和各相的体积分数。随着Si和Ti含量的增加,合金的硬度和强度增加,但塑性和韧性降低。Nb枝晶的失效方式为解理断裂,而硅化物为脆性断裂。 相似文献
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LIU Fa-min DING Peng SHI Wei-mei WANG Tian-min 《中国航空学报》2007,20(2):162-167
The TiO2-Co-TiO2 sandwich films were successfully grown on glass and silicon substrata making alternate use of radio frequency reactive magnetron sputtering and direct current magnetron sputtering. The structures and properties of these films were identified with X-ray diffraction (XRD), Raman spectra and X-ray photoemission spectra (XPS). It is shown that the sandwich film consists of two anatase TiO2 films with an embedded Co nano-film. The fact that, when the Co nano-film thickens, varied red shifts appear in optical absorption spectra may well be explained by the quantum confinement and tunnel effects. As for magnetic properties, the saturation magnetization, remnant magnetic induction and coercivity vary with the thickness of the Co nano-films. Moreover, the Co nano-film has a critical thickness of about 8.6 nm, which makes the coercivity of the composite film reach the maximum of about 1413 Oe. 相似文献
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磁场辅助激光熔覆铝基金属玻璃覆层 总被引:1,自引:1,他引:0
为提高铝合金的表面性能,采用磁场辅助激光熔覆的方法在5083铝合金表面制备了Al-Ni-Y-Co-La五元金属玻璃熔覆层,并对其进行组织成分及性能分析。实验结果表明:熔覆层主要由非晶相、α-Al相以及Al4NiY等金属间化合物组成,旋转磁场的搅拌作用使熔覆层非晶相含量由10.2%提高到30.7%,且能够有效抑制多道搭接和多层堆积过程中重熔区晶粒的生长,细化了熔覆层晶粒组织,降低了残余应力,提高了显微硬度及韧性,使其平均显微硬度从278 HV0.1提高至335 HV0.1,且波动较小,平均抗拉强度为303 MPa,为基体拉伸件的110.2%,平均伸长率为6.79%,为基体的33.1%。 相似文献
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Fe基非晶合金因强度高、硬度高、软磁性能优异等优势,得到人们极大关注。然而,目前实验室和工业领域利用铜模铸造法所能制备的Fe基非晶合金尺寸仍然较小,这严重制约了Fe基非晶合金作为结构材料在工业领域的实际应用。激光3D打印技术的出现为解决上述问题提供了难得的契机。然而,目前国内外的研究中,利用激光3D打印技术制备Fe基非晶合金存在较为严重的裂纹,所以无法利用该技术成型大尺寸的样品。在Fe基非晶合金中引入塑性较好的第二相来吸收热应力,防止在激光3D打印过程中发生开裂,能成功打印出大尺寸的Fe基非晶合金复合材料。通过上述方法成型的大尺寸Fe基非晶合金复合材料,宏观上没有裂纹发生且成型性良好,但微观上仍在局域发现微小裂纹。由于Cu将Fe基非晶合金包裹在中间,所以这些局域的微裂纹没有扩展,也没有贯穿整个材料,打印的Fe基非晶合金复合材料成型性没有受到较大影响。 相似文献
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LIN Jin-zhao WANG Jin-liang* ZHOU Bo WU Er-xing Department of Physics Beijing University of Aeronautics Astronautics Beijing China 《中国航空学报》2006,19(Z1)
Studies of nanoindentation were performed on nc-Si:H films to evaluate the effects of the fabrication processes on their mechani-cal properties. It is observed that with the decrease of the SiH4 contents, the grain size of the films increases gradually, and as does the crystalline volume fraction. The smaller the grains become, the more homogeneous the films, and the more even the hardness as well as the modulus will be. The hardness and the modulus will increase with the substrate’s temperature rising. The hardness and the modulus of the nc-Si:H films on the Si substrate prove to be higher than those on the glass substrate given the same technology parameters. How-ever, the films on the glass substrate appear to be more homogeneous. 相似文献
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张春基%吕宏军%贾中华%陈道勇%胡国林 《宇航材料工艺》2007,37(6):57-60
为探索铌钨合金在液体火箭发动机上的应用,针对我国研制成功的Nb-5W-2Mo-1Zr铌钨合金进行了高温性能试验及抗高温氧化涂层的研制,铌钨合金及涂层在高温时的组织结构分析及相关工艺试验。结果表明:Nb-5W-2Mo-1Zr铌钨合金及抗氧化涂层可用于液体火箭发动机。 相似文献
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Fe3O4/T-ZnOw composites are fabricated by depositing a layer of Fe3O4 film on the surface of tetrapod-shaped ZnO whisker (T-ZnOw) by ferrite plating method. The morphology, structure and magnetic properties of the composites are characterized by scanning electron microscopy (SEM), X-ray diffractometer (XRD) and vibrating-sample magnetometer (VSM), respectively. The effects of temperature and pH value of ferrite plating on the Fe3O4/T-ZnOw composites and the magnetic properties of composites are studied. It is shown that the chemical environment with pH value at 7.5 is most favorable for the ferrite plating processes by analyzing the main peaks intensity of Fe3O4 in the XRD patterns and the average diameters of the Fe3O4 crystalline. The increase of the ferrite plating temperature with pH value around 7.5 benefits the whole encapsulation of T-ZnOw by the Fe3O4 magnetic films. The composites exhibit ferromagnetic properties and show much lower magnetization intensity than bulk samples at the same magnetic field intensity. 相似文献
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用脉冲激光沉积(PLD)技术制备了掺杂金颗粒的钛酸钡复合薄膜Au/BaTiO3,用透射电镜和X射线光电子能谱对薄膜进行了表征,研究了其线性光吸收特性.结果表明,用复合靶和转靶的方法可以成功地制备金属纳米团簇复合薄膜,并且制备出的薄膜有良好的化学结构和物理特征. 相似文献
18.
TiCxNy
films were formed on 9Cr18 and GCr15 substrates using ion beam assisted deposition and
studied with TEM, AES and XPS. TEM results showed that the films have polycrystalline
structure with preferential growth orientations in (111),(200) and (220) directions. The
AES and XPS results confirmed that the TiCxNy films contain oxygen
coordination. The dry friction test indicated that oxidation resistance of the films is
excellent, formation of the oxide film in the friction process can be effectively
inhibited because of its presence on the steel substrates. At the same time,the wear
properties of substrates were obviously improved because of high hardness and excellent
lubriction of the films. However, the mechanical properties of TiCxNy
films deposited by different N fluence appear different variance rule with the diffrent
substrates. Microhardness and friction properties of TiCxNy films
are relative to its N content and a excessively high N content has a harmful influence on
the hardness and friction properties. 相似文献
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《中国航空学报》2023,36(5):508-521
It is difficult to gain effective Ti-Al fusion welding joints due to their differences in thermal properties and the appearance of brittle Ti-Al Intermetallic Compounds (IMCs). The experiments of laser fusion welding for TC4 titanium and 7075 aluminum alloy were carried out, temperature field and ductility/brittleness, as well as chemical potential of elements, were calculated, and the effect of adding Nb foil on mechanical properties of the weld was also investigated. The results suggested that Nb atoms tend to diffuse toward Al side, which is conducive to the participation of Nb in the metallurgical reaction and contributes to forming the Ti-Nb-Al IMC layer at the interface. As the thickness of Nb foil increases, the tensile-shear force of joint climbs first but then declines, and reaches the highest value of 1663 N with 0.10 mm-thickness Nb foil, representing 58.38% enhancement compared with the non-added one. Adding Nb foil slows down the heat transfer as a blocker, and thus both the melting amount of Al and the mixing area of Ti and Al decrease. In addition, Nb alloying reduces the brittleness of the Ti-Al compound. Hence, the joint properties of titanium/aluminum are improved with the addition of Nb foil. 相似文献